Nuclear magnetic resonance: Methodologies and applications

Handbook of Olive Oil: Analysis and Properties

Volumn , Issue , 2013, Pages 395-430

  Dais, Photis ^a  

^a UNIVERSITY OF CRETE   (Greece)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84988817432     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1007/978-1-4614-7777-8_11     Document Type: Chapter

References (82)

1. Agiomyrgianaki A, Petrakis PV, Dais P (2010) Detection of refined olive oil adulteration with refined hazelnut oil by employing NMR spectroscopy and multivariate statistical analysis. Talanta 80:2165-2171
2. Alonso-Salces RM, Moreno-Rojas JM, Holland MV, Reniero F, Guillou C et al (2010) Virgin olive oil authentication by multivariate analyses of 1H NMR fingerprints and δ 13C and δ 1H data. J Agric Food Chem 59:5586-5596
3. Aparicio R, Aparicio-Ruiz R (2000) Authentication of vegetable oils by chromatographic techniques. J Chromatogr A 881:93-104
4. Berger S, Braun S (2004) 200 and more experiments: a practical course. Wiley VCH, Weinheim
5. Brescia MA, Alviti G, Liuzzi V, Antonio Sacco A (2003) Chemometric classification of olive cultivars based on compositional data of oils. J Am Oil Chem Soc 80:945-950
6. Brescia MA, Sacco A (2008a) High-resolution 1H nuclear magnetic resonance in the study of oils. In: Webb GA (ed) Modern magnetic resonance. Part III. Springer, Dordrect, pp 1645-1650
7. Brescia MA, Sacco A (2008b) High-resolution 13C nuclear magnetic resonance in the study of oils. In: Webb GA (ed) Modern magnetic resonance. Part III. Springer, Dordrecht, pp 1637-1643
8. Ceci LN, Carelli AA (2007) Characterization of monovarietal argentinian olive oils from new productive zones. J Am Oil Chem Soc 84:1125-1136
9. Christophoridou S, Dais P (2006) Novel approach to the detection and quantification of phenolic compounds in olive oil based on 31P nuclear magnetic resonance spectroscopy. J Agric Food Chem 54:656-664
10. Christophoridou S, Dais P (2009) Detection and quantification of phenolic compounds in olive oil by high resolution 1H nuclear magnetic resonance spectroscopy. Anal Chim Acta 633:283-292
11. Christophoridou S, Dais P, Tseng L-H, Spraul M (2005) Separation and identification of phenolic compounds in olive oil by coupling high-performance liquid chromatography with postcolumn soli-phase extraction to nuclear magnetic resonance spectroscopy (LC-SPE-NMR). J Agric Food Chem 53:4667-4679
12. Corcoran O, Wilkinson PS, Godejohann M, Braumann U, Hofmann M et al (2002) Advancing sensitivity for flow NMR spectroscopy: LC-SPE-NMR and capillary-scale LC-NMR. Am Lab 5:18-21
13. Cotte JF, Casabianca H, Lhéritier J, Perrucchietti JC, Sanglar C et al (2007) Study and validity of 13C stable carbon isotopic ratio analysis by mass spectrometry and 2H site-specific natural isotopic fractionation by nuclear magnetic resonance isotopic measurements to characterize and control the authenticity of honey. Anal Chim Acta 582:125-136
14. D'Imperio M, Mannina L, Capitani D, Bidet O, Rossi E et al (2007) NMR and statistical study of olive oils from Lazio: a geographical, ecological and agronomic characterization. Food Chem 105:1256-1267
15. Dais P, Spyros A (2007) 31P NMR spectroscopy in the quality control and authentication of virgin olive oil. An account of recent results. Magn Reson Chem 45:367-377
16. Dais P, Spyros A, Christophoridou S, Hatzakis E, Fragaki G et al (2007) Comparison of analytical methodologies based on 1H and 31P NMR spectroscopy with conventional methods of analysis for the determination of some olive oil constituents. J Agric Food Chem 55:577-584
17. Exarchou V, Krucker M, van Beek T, Vervoort J, Gerothanassis I et al (2005) LC-NMR coupling technology: recent advancements and applications in natural products analysis. Magn Reson Chem 43:681-687
18. Fauhl C, Reniero F, Guillou C (2000) 1H.NMR as a tool for the analysis of mixtures of virgin olive oils of different botanical origin. Magn Reson Chem 38:436-443
19. Fragaki G, Spyros A, Siragakis G, Salivaras E, Dais P (2005) Detection of extra virgin olive oil adulteration with lampante olive oil and refined olive oil using nuclear magnetic resonance spectroscopy and multivariate statistical analysis. J Agric Food Chem 53:2810-2816
20. Fronimaki P, Spyros A, Christophoridou S, Dais P (2002) Determination of the diglyceride content in Greek virgin olive oils and some commercial olive oils by employing 31P NMR spectroscopy. J Agric Food Chem 50:2207-2213
21. Gambhir PN (1992) Applications of low-resolution pulsed NMR to the determination of oil and moisture in oilseeds. Trends Food Sci Technol 3:191-196
22. Gao L, Sedman J, García-González DL, Ehsan S, Sprules T et al (2009) 13C NMR as a primary method for determining saturates, cis and trans-monounsaturates and polyunsaturates in fats and oils for nutritional labeling purposes. Eur J Lipid Sci Technol 11:612-622
23. García-González DL, Mannina L, D'Imperio M, Segre AL, Aparicio R (2004) Using 1H and 13C NMR techniques and artificial neural networks to detect the adulteration of olive oil with hazelnut oil. Eur Food Res Technol 219:545-548
24. Goulas V, Exarchou V, Troganis AN, Psomiadou E, Fotsis T et al (2009) Phytochemicals in olive-leaf extracts and their antiproliferative activity against cancer and endothelial cells. Mol Nutr Food Res 53:600-608
25. Guillen MD, Ruiz A (2003) Edible oils: discrimination by 1H nuclear magnetic resonance. J Sci Food Agric 83:338-346
26. Guillen MD, Ruiz A (2006) Study by means of 1H nuclear magnetic resonance of the oxidation process undergone by edible oils of different natures submitted to microwave action. Food Chem 96:665-674
27. Hatzakis E, Dais P (2008) Determination of water content in olive oil by 31P NMR spectroscopy. J Agric Food Chem 56:1866-1872
28. Hatzakis E, Koidis A, Boskou D, Dais P (2008) Determination of phospholipids in olive oil by 31P NMR spectroscopy. J Agric Food Chem 56:6232-6240
29. Hatzakis E, Dagounakis G, Agiomyrgianaki A, Dais P (2010a) A facile NMR method for the quantification of total, free and esterified sterols in virgin olive oil. Food Chem 122:346-352
30. Hatzakis E, Agiomyrgianaki A, Dais P (2010b) Detection and quantification of free glycerol in virgin olive oil by 31P-NMR spectroscopy. J Am Oil Chem Soc 87:29-34
31. Hidalgo FJ, Zamora R (2003) Edible oil analysis by high-resolution nuclear magnetic resonance spectroscopy: recent advances and future perspectives. Trends Food Sci Technol 14:499-506
32. Hidalgo FJ, Gómez G, Navarro JL, Zamora RZ (2002) Oil stability prediction by high-resolution 13C nuclear magnetic resonance spectroscopy. J Agric Food Chem 50:5825-5831
33. International Olive Council (IOC) (2003) COI/T.15/NC no 3-25. Madrid, Spain
34. Lercker G, Frega N, Bocci F, Servidio G (1994) Veiled extravirgin olive oils: dispersion response related to oil stability. J Am Oil Chem Soc 71:657-658
35. Lui A, Casu M, Saba G, Corongiu FP, Dessi MA (1995) NMR investigation of the intramolecular distribution of deuterium nuclei in natural ttiacylglycerols. Magn Reson Chem 33:165-166
36. Mannina L, Segre A (2002) High resolution nuclear magnetic resonance: from chemical structure to food authenticity. Grasas Aceites 53:22-33
37. Mannina L, Luchinat C, Emanuele MC, Segre AL (1999a) Acyl positional distribution of glycerol tri-esters in vegetable oils: a 13C NMR study. Chem Phys Lipids 103:47-55
38. Mannina L, Patumi M, Fiordiponti P, Emanuele MC, Segre AL (1999b) Olive and hazelnut oils: a study by high 1H NMR and gas chromatography. Ital J Food Sci 11:139-149
39. Mannina L, Fontanazza G, Patumi M, Ansanelli G, Segre AL (2001a) Italian and Argentine olive oils: a NMR and gas chromatography study. Grasas Aceites 6:380-388
40. Mannina L, Patumi M, Proietti N, Segre AL (2001b) PDO (Protected Designation of Origin): geographical characterization of Tuscan extra virgin olive oils using high-field H-1 NMR spectroscopy. Ital J Food Sci 13:53-63
41. Mannina L, Luchinat C, Patumi M, Emanuele MC, Rossi E et al (2002) Concentration dependence of 13C NMR spectra of triglycerides: implications for the NMR analysis of olive oils. Magn Reson Chem 38:886-890
42. Mannina L, Sobolev AP, Segre A (2003a) Olive oil as seen by NMR and chemometrics. Spectr Eur 15:6-14
43. Mannina L, Dugo G, Salvo F, Cicero L, Ansanelli G et al (2003b) Study of the cultivar-composition relationship in Sicilian olive oils by GC, NMR, and statistical methods. J Agric Food Chem 51:120-127
44. Mannina L, D'Imperio M, Lava R, Schievano E, Mammi S (2005) Caratterizzazione NMR e analisi statistica di oli di oliva DOP Veneti. Riv Ital Sostanze Grasse 82:59-63
45. Mannina L, D'Imperio M, Capitani D, Rezzi S, Guillou C et al (2009) 1H NMR-based protocol for the detection of adulterations of refined olive oil with refined hazelnut oil. J Agric Food Chem 57:11550-11556
46. Mannina L, Marini F, Gobbino M, Sobolev AP, Capitani D (2010) NMR and chemometrics in tracing European olive oils: the case study of Ligurian samples. Talanta 80:2141-2148
47. Mannina L, Sobolev AP (2011) High resolution NMR characterization of olive oils in terms of quality, authenticity and geographical origin. Magn Reson Chem 49:S3-S11
48. Martin ML, Martin GJ (1990) Deuterium NMR in the study of site-specific natural isotope fractionation (SNIF-NMR). NMR Basic Princ Prog 23:1-61
49. Martin ML, Martin GJ (1995) Stable Isotope analysis of food and beverages by nuclear magnetic resonance. Ann Rep NMR Spectrosc 31:81-104
50. Mavromoustakos T, Zervou M, Theodoropoulou E, Panagiotopoulos D, Bonas G et al (1997) 13C NMR analysis of the triacyglycerol composition of Greek virgin olive oils. Magn Reson Chem 35:S3-S7
51. Mavromoustakos T, Zervou M, Bonas G, Kolocouris A, Petrakis P (2000) A novel analytical method to detect adulteration of virgin olive oil by other oils. J Am Oil Chem Soc 77:405-411
52. Medina I, Sacchi R, Giudicianni I, Aubourg S (1998) Oxidation in fish lipids during thermal stress as studied by 13C nuclear magnetic resonance spectroscopy. J Am Oil Chem Soc 75:147-154
53. Miyake Y, Yokomizo K, Matsuzaki N (1998) Rapid determination of iodine value by 1H Nuclear magnetic resonance spectroscopy. J Am Oil Chem Soc 75:15-19
54. Montedoro G, Servili M, Baldioli M, Selvaggini R, Miniati E (1992) Simple and hydrolysable compounds in virgin olive oil. 1. Their extraction, separation and semiquantitative evaluation by HPLC. J Agric Food Chem 40:1571-1576
55. Morelló JR, Romero MP, Motilva MJ (2006) Influence of seasonal conditions on the composition and quality parameters of monovarietal virgin olive oils. J Am Oil Chem Soc 83:683-690
56. Morris KF, Johnson CS (1992) Diffusion-ordered two-dimensional nuclear magnetic resonance spectroscopy. J Am Oil Chem Soc 114:3139-3141
57. Official Journal of the Commission of the European Communities (EC) (1991) Regulation No. 2568/91, L248, Sept 5
58. Official Journal of the Commission of the European Communities (EC) (1995) Regulation No. 656/95, L69, Mar 29
59. Petrakis PV, Agiomyrgianaki A, Christophoridou S, Spyros A, Dais P (2008) Geographical characterization of Greek virgin olive oils (Cv. Koroneiki) using 1H and 31P NMR fingerprinting with canonical discriminant analysis and classification binary trees. J Agric Food Chem 56:3200-3207
60. Rezzi S, Axelso DE, Héberger K, Reniero F, Mariani C et al (2005) Classification of olive oils using throughput flow 1H NMR fingerprinting with principal component analysis, linear discriminant analysis and probabilistic neural network. Anal Chim Acta 552:13-24
61. Royer A, Nauler N, Mabon F, Lees M, Martin CJ (1999) Stable isotope characterization of olive oils. II-Deuterium distribution in fatty acids studied by nuclear magnetic resonance. J Am Oil Chem Soc 76:365-373
62. Sacchi R, Addeo F, Paolillo L, Giudicianni I (1997) 1H and 13C NMR of virgin olive oil. An overview. Magn Reson Chem 35:S133-S145
63. Sacco A, Brescia MA, Liuzzi V, Reniero F, Guillou C et al (2000) Characterization of Italian olive oils based on analytical and nuclear magnetic resonance determinations. J Am Oil Chem Soc 77:619-625
64. Schievano E, Arosio I, Lava R, Simionato V, Mammi S et al (2006) Olio di oliva DOP del lago di Garda: uno studio NMR e analisi statistica multivariata. Riv Ital Sostanze Grasse 83:14-17
65. Sedman J, Gao L, García-González DL, Ehsan S, van de Voort FR (2010) Determining nutritional labeling data for fats and oils by 1H NMR. Eur J Lipid Sci Technol 112:439-451
66. Shaw AD, di Camillo A, Vlahov G, Jones A, Bianchi G et al (1997) Discrimination of the variety and region of origin of extra virgin olive oils using 13C NMR and multivariate calibration with variable reduction. Anal Chim Acta 348:357-374
67. Simonova S, Ivanova G, Spassov SL (2003) Alternative NMR method for quantitative determination of acyl positional distribution in triacylglycerols and related compounds. Chem Phys Lipids 126:167-176
68. Šmejkalová D, Piccolo A (2010) High-power gradient diffusion NMR spectroscopy for rapid assessment of extra-virgin olive oil adulteration. Food Chem 118:153-158
69. Spyros A, Dais P (2000) Application of 31P NMR spectroscopy in food analysis. Quantitative determination of the monoand diglyceride composition of olive oils. J Agric Food Chem 48:802-805
70. Spyros A, Philippidis A, Dais P (2004) Kinetics of diglyceride formation and isomerization in virgin olive oils by employing 31P NMR spectroscopy. Formulation of a quantitative measure to assess olive oil storage history. J Agric Food Chem 52:157-164
71. Stilbs P (1987) Fourier transform pulsed-gradient spin-echo studies of molecular diffusion. Prog NMR Spectrosc 19:1-45
72. Van Duynhoven J, Voda A, Witek M, Van As H (2010) Time-domain NMR applied food products. Ann Rep NMR Spectrosc 69:145-197
73. Vigli G, Philippidis A, Spyros A, Dais P (2003) Classification of edible oils by employing 31P and 1H NMR spectroscopy in combination with multivariate statistical analysis. A proposal for detection of seed oil adulteration in virgin olive oils. J Agric Food Chem 51:5715-5722
74. Vlahov G (1997) Quantitative 13C NMR method using the DEPT pulse sequence for the detection of olive oil adulteration with soybean oil. Magn Reson Chem 35:S8-S12
75. Vlahov G (1999) Application of NMR to study of olive oils. Prog NMR Spectrosc 35:341-357
76. Vlahov G, Shaw AD, Kell DB (1999) Use of 13C nuclear magnetic resonance distortionless enhancement by polarization transfer pulse sequence and multivariate analysis to discriminate olive oil cultivars. J Am Oil Chem Soc 76:1223-1231
77. Vlahov G, Schiavone C, Simone N (2001) Quantitative 13C NMR method using the DEPT pulse sequence for the determination of the geographical origin (DOP) of olive oils. Magn Reson Chem 39:689-695
78. Vlahov G, Del Re P, Simone N (2003) Determination of geographical origin of olive oils using 13C nuclear magnetic resonance spectroscopy. I-Classification of olive oils of the Puglia region with denomination of protected origin. J Agric Food Chem 51:5612-5615
79. Zamora R, Navarro JL, Hidalgo FJ (1994) Identification and classification of olive oils by high-resolution 13C nuclear magnetic resonance. J Am Oil Chem Soc 71:361-464
80. Zamora R, Gómez G, Hidalgo FJ (2002) Classification of vegetable oils by high-resolution 13C NMR spectroscopy using chromatographically obtained oil fractions. J Am Oil Chem Soc 79:267-272
81. Zamora R, Gómez G, Hidalgo FJ (2003) Quality control of vegetable oils by 13C NMR spectroscopy. In: Webb GA, Belton PS, Gill AM, Rutledge DN (eds) Magnetic resonance in food science latest developments. The Royal Society of Chemistry, Cambridge, UK, pp 231-238
82. Zamora R, Alba V, Hidalgo FJ (2001) Use of high-resolution 13C nuclear magnetic resonance spectroscopy for screening of virgin olive oils. J Am Oil Chem Soc 78:89-94