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Coupling reaction of surface 1 with 1-azidobutane 2a to afford surface 2 was performed with the reaction vessel immersed in a water bath set to 25 °C.
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Coupling reaction of surface 1 with 1-azidobutane 2a to afford surface 2 was performed with the reaction vessel immersed in a water bath set to 25 °C.
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A parallel approach to evaluate reaction yields relied on a comparison between XPS C 1s intensities (integrated area of the corresponding fitted function) ascribed to atoms in different environments. Given that good agreement was generally observed between the two approaches used to quantitate the immobilization of azide species, for clarity, results from only the N/C elemental analysis method are reported in the text.
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34548543101
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105
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34548525003
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5
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29 concerns existed regarding the possibility of an ipso (at the same) substitution reaction at the surfacial silylated olefin, the putative interfacial species, [(a) Cerofolini, G. F.; Galati, C.; Reina, S.; Renna, L. Semicond. Sci. Technol. 2003, 18, 423-429], eventually leading to the complete removal of the entire organic assembly. As a result of the ability of silicon atom to stabilize a positive charge in the beta position, the carbocation originated upon protonation of the double bond affords a weakened carbon-silicon bond that is rapidly cleaved by nucleophiles
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29 concerns existed regarding the possibility of an ipso ("at the same") substitution reaction at the surfacial silylated olefin, the putative interfacial species, [(a) Cerofolini, G. F.; Galati, C.; Reina, S.; Renna, L. Semicond. Sci. Technol. 2003, 18, 423-429], eventually leading to the complete removal of the entire organic assembly. As a result of the ability of silicon atom to stabilize a positive charge in the beta position, the carbocation originated upon protonation of the double bond affords a weakened carbon-silicon bond that is rapidly cleaved by nucleophiles
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x species as indicated by XPS Si 2p narrow scans. (Figure S3). This strongly supports the presence of a densely packed acetylene-terminated monolayer effectively passivating the silicon surface.
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x species as indicated by XPS Si 2p narrow scans. (Figure S3). This strongly supports the presence of a densely packed acetylene-terminated monolayer effectively passivating the silicon surface.
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