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Volumn 7, Issue 5, 2005, Pages 673-681

Synthesis of a library of complex macrodiolides employing cyclodimerization of hydroxy esters

Author keywords

[No Author keywords available]

Indexed keywords

HYDROXYACID; KAPPA OPIATE RECEPTOR; MACROLIDE;

EID: 27744456130     PISSN: 15204766     EISSN: None     Source Type: Journal    
DOI: 10.1021/cc050064b     Document Type: Article
Times cited : (39)

References (91)
  • 39
    • 0036603599 scopus 로고    scopus 로고
    • For recent reviews of microwave-accelerated synthesis, see: (a) Kappe, O. C. Curr. Opin. Chem. Biol. 2002, 6, 314.
    • (2002) Curr. Opin. Chem. Biol. , vol.6 , pp. 314
    • Kappe, O.C.1
  • 59
  • 69
    • 33751500481 scopus 로고
    • For insight regarding the mechanism of tin-catalyzed trans- esterification, see: Otera, J.; Dan-oh, N.; Nozaki, H. J. Org. Chem. 1991, 56, 5307.
    • (1991) J. Org. Chem. , vol.56 , pp. 5307
    • Otera, J.1    Dan-oh, N.2    Nozaki, H.3
  • 70
    • 28844493347 scopus 로고    scopus 로고
    • note
    • See Supporting Information for further details.
  • 71
    • 0035813242 scopus 로고    scopus 로고
    • For examples and discussion of microwave power effects, see: (a) Perreux, L.; Loupy, A. Tetrahedron 2001, 57, 9199.
    • (2001) Tetrahedron , vol.57 , pp. 9199
    • Perreux, L.1    Loupy, A.2
  • 82
    • 28844457852 scopus 로고    scopus 로고
    • note
    • A standard HPLC gradient (5% acetonitrile → 45% acetonitrile (0.01% formic acid) over 5 min) was used for all compounds and adjusted for cases that did not show satisfactory separation.
  • 88
    • 28844478672 scopus 로고    scopus 로고
    • note
    • Preparative HPLC was accomplished using LC gradients based on successful analytical methods for each sample. Criteria for fraction collection was a mixed trigger involving both ELSD intensity and mass identity.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.