Detection of hazelnut oil in extra-virgin olive oil by analysis of polar components bymicro-solid phase extraction based on hydrophilic liquid chromatography and MALDI-ToF mass spectrometry

Journal of Mass Spectrometry

Volumn 45, Issue 9, 2010, Pages 981-988

  Calvano, Cosima D ^a   Aresta, Antonella ^a   Zambonin, Carlo G ^a  

^a UNIVERSITY OF BARI   (Italy)

Author keywords

Extra virgin olive oil; Hazelnut oil; HILIC SPE; MALDI ToF MS; Polar fraction

Indexed keywords

CAPILLARY LIQUID CHROMATOGRAPHY; FATTY ACID PROFILES; HAZELNUT OIL; LYSOPHOSPHATIDYLCHOLINE; MALDI TOF MS; MALDI-TOF MASS SPECTROMETRY; MALDI-TOF-MS ANALYSIS; MATRIX-ASSISTED LASER DESORPTION IONIZATION; MICROSOLIDPHASE EXTRACTION; POLAR COMPONENTS; POLAR COMPOUNDS; POLAR FRACTION; QUADRUPOLES; QUALITATIVE ANALYSIS; SELECTIVE EXTRACTION; SOLID-PHASE EXTRACTION; TIME OF FLIGHT MASS SPECTROMETRY; TRIACYLGLYCEROLS; VIRGIN OLIVE OIL;

DESORPTION; ELECTROSPRAY IONIZATION; FATTY ACIDS; GLYCEROL; HYDROPHILICITY; INDUCTIVELY COUPLED PLASMA; IONIZATION; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; PARTICLE DETECTORS; POLYACRYLATES; SOLVENT EXTRACTION; VEGETABLE OILS;

QUALITY CONTROL;

ARACHIS OIL; DAIDZEIN; EXTRA VIRGIN OLIVE OIL; FATTY ACID; HAZELNUT OIL; LYSOPHOSPHATIDYLCHOLINE; OLIVE OIL; STEROL; TRIACYLGLYCEROL; UNCLASSIFIED DRUG;

ARTICLE; BIOCHEMICAL COMPOSITION; HAZELNUT; HYDROPHILICITY; LIQUID CHROMATOGRAPHY; MATRIX ASSISTED LASER DESORPTION IONIZATION TIME OF FLIGHT MASS SPECTROMETRY; NONHUMAN; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; SOLID PHASE EXTRACTION;

CHROMATOGRAPHY, LIQUID; CORYLUS; FOOD CONTAMINATION; HYDROPHOBIC AND HYDROPHILIC INTERACTIONS; PLANT OILS; SOLID PHASE MICROEXTRACTION; SPECTROMETRY, MASS, MATRIX-ASSISTED LASER DESORPTION-IONIZATION;

CORYLUS;

EID: 77956843446     PISSN: 10765174     EISSN: 10969888     Source Type: Journal    
DOI: 10.1002/jms.1753     Document Type: Article

References (38)

1. European Union Commission Regulation EEC/1989/2003. J. Eur. Union 2003, L295.
2. European Union Commission Regulation 1513/2001 of 23 July 2001 amending Regulations No. 136/66/EEC. J. Eur. Union 2001, L201.
3. M.D. Medeiros. The Handbook of Nutraceutical sand Functional Foods, R. E. C. Wildman (Ed.). CRC Press: Boca Raton, 2001.
4. E. Gimeno, M. Fito, R. M. Lamuela-Raventos, A. I. Castellote, M. Covas, M. Farre. Effect of ingestion of virgin olive oil on human low-density lipoprotein composition. Eur. J. Clin.Nutr. 2002, 56, 114.
5. J. Parcerisa, D. G. Richardson, M. Rafecas, R. Codony, J. Boatella. Fatty acid distribution in polar and non-polar lipid classes of hazelnut oil (Corylus avellana L.). J. Agric. Food Chem. 1997, 45, 3887.
6. R. Aparicio, R. Aparicio-Ruiz. Authentication of vegetable oils by chromatographic techniques. J. Chromatogr. A 2000, 881, 93.
7. K. Papadopoulos, T. Triantis, C. H. Tzikis, A. Nikokavoura, D. Dimotikali. Investigations of the adulteration of extra virgin olive oils with seed oils using their weak chemiluminescence. Anal. Chim. Acta 2002, 464, 135.
8. G. G. Bortoleto, L. C.M. Pataca, M. I.M. S. Bueno. A new application of X-ray scattering using principal component analysis - classification of vegetable oils. Anal. Chim. Acta 2005, 539, 283.
9. F. Guimet, J. Ferre, R. Boque. Rapid detection of olive-pomace oil adulteration in extra virgin olive oils from the protected denomination of origin "Siurana" using excitation-emission fluorescence spectroscopy and three-way methods of analysis. Anal. Chim. Acta 2005, 544, 143.
10. S. Azadmard-Damirchi, P. C. Dutta. Novel solid-phase extraction method to separate 4-desmethyl-, 4-monomethyl-, and 4,4′-dimethylsterols in vegetable oils. J. Chromatogr. A 2006, 1108, 183.
11. K. I. Poulli, G. A. Mousdis, C. A. Georgiou. Synchronous fluorescence spectroscopy for quantitative determination of virgin olive oil adulteration with sunflower oil. Anal. Bioanal. Chem. 2006, 386, 1571.
12. N. Vlachos, Y. Skopelitis, M. Psaroudaki, V. Konstantinidou, A. Chatzilazarou, E. Tegou. Applications of Fourier transform-infrared spectroscopy to edible oils. Anal. Chim. Acta 2006, 573-574(,), 459.
13. K. I. Poulli, G. A. Mousdis, C. A. Georgiou. Rapid synchronous fluorescence method for virgin olive oil adulteration assessment. Food Chem. 2007, 105, 369.
14. G. Gurdeniz, B. Ozen. Detection of adulteration of extra-virgin olive oil by chemometric analysis of mid-infrared spectral data. Food Chem. 2009, 116, 519.
15. H. Lizhi, K. Toyoda, I. Ihara. Discrimination of olive oil adulterated with vegetable oils using dielectric spectroscopy. J. Food Eng. 2010, 96, 167.
16. D. Smejkalova, A. Piccolo. High-power gradient diffusion NMR spectroscopy for the rapid assessment of extra-virgin olive oil adulteration. Food Chem. 2010, 118, 153.
17. I. Marcos-Lorenzo, J. L. Perez-Pavon, M. E. Fernandez-Laespada, C. Garcia-Pinto, B. Moreno-Cordero. Detection of adulterants in olive oil by headspace-mass spectrometry. J. Chromatogr. A 2002, 945, 221.
18. C. D. Calvano, A. Aresta, F. Palmisano, C. G. Zambonin. A laser desorption ionization time-of-flight mass spectrometry investigation into triacylglycerols oxidation during thermal stressing of edible oils. Anal. Bioanal. Chem. 2007, 389, 2075.
19. C. D. Calvano, F. Palmisano, C. G. Zambonin. Laser desorption/ ionization time-of-flight mass spectrometry of triacylglycerols in oils. Rapid Commun.Mass Spectrom. 2005, 19, 1315.
20. R. R. Catharino, R. Haddad, L. Girotto Cabrini, I. B. S. Cunha, A. C. H. F. Sawaya, M. N. Eberlin. Characterization of vegetable oils by electrospray ionization mass spectrometry fingerprinting: classification, quality, adulteration, and aging. Anal. Chem. 2005, 77, 7429.
21. J. L. Gomez-Ariza, A. Arias-Borrego, T. Garcia-Barrera, R. Beltran. Comparative study of electrospray and photospray ionization sources coupled to quadrupole time-of-flight mass spectrometer for olive oil authentication. Talanta 2006, 70, 859.
22. L. Vaclavik, T. Cajka, V. Hrbek, J. Hajslova. Ambient mass spectrometry employing direct analysis in real time (DART) ion source for olive oil quality and authenticity assessment. Anal. Chim. Acta 2009, 645, 56.
23. D. Zabaras, M. H. Gordon. Detection of pressed hazelnut oil in virgin olive oil by analysis of polar components: improvement and validation of the method. Food Chem. 2004, 84, 475.
24. E. Christopouloua, M. Lazarakia, M. Komaitisb, K. Kaselimis. Effectiveness of determinations of fatty acids and triglycerides for the detection of adulteration of olive oils with vegetable oils. Food Chem. 2004, 84, 463.
25. G. Flores, M. L. Castillo, G. P. Blanch, M. Herraiz. Detection of the adulteration of olive oils by solid phase microextraction and multidimensional gas chromatography. Food Chem. 2006, 97, 336.
26. F. Priego-Capote, J. Jimenez, M. D. de Castro. Sequential (step-by-step) detection, identification and quantitation of extra virgin olive oil adulteration by chemometric treatment of chromatographic profiles. Anal. Bioanal. Chem. 2007, 388, 1859.
27. M. Jafari,M. Kadivar, J. Keramat. Detection of adulteration in iranian olive oils using instrumental (GC, NMR, DSC) methods. J Am. Oil Chem. Soc. 2009, 86, 103.
28. L. Cercaci, M. T. Rodriguez-Estrada, G. Lercker. Solid-phase extraction-thin-layer chromatography-gas chromatography method for the detection of hazelnut oil in olive oils by determination of esterified sterols. J. Chromatogr. A 2003, 985, 211.
29. G. Flores, M. L. del Castillo, M Herraiz, G. P. Blanch. Study of the adulteration of olive oil with hazelnut oil by on-line coupled high performance liquid chromatographic and gas chromatographic analysis of filbertone. Food Chem. 2006, 97, 742.
30. S. Mildner-Szkudlarz, H. H. Jelen. The potential of different techniques for volatile compounds analysis coupled with PCA for the detection of the adulteration of olive oil with hazelnut oil. Food Chem. 2008, 110, 751.
31. M. Arlorio, J. D. Coisson, M. Bordiga, F. Travaglia, C. Garino, L. Zuidmeer, R. Van Ree, M. G. Giuffrida, A. Conti, A. Martelli. Olive oil adulterated with hazelnut oils: simulation to identify possible risks to allergic consumers. Food Addit. Contam. A 2010, 27, 11.
32. E.Chiavaro, E.Vittadini, M.T. Rodriguez-Estrada, L. Cerretani, A Bendini. Differential scanning calorimeter application to the detection of refined hazelnut oil in extra virgin olive oil. Food Chem. 2008, 110, 248.
33. S. Azadmard-Damirchi. Review of the use of phytosterols as a detection tool for adulteration of olive oil with hazelnut oil. Food Addit. Contam. A 2010, 27, 1.
34. C. G. Zambonin, C. D. Calvano, L. D'Accolti, F. Palmisano. Laser desorption/ionization time-of flight mass spectrometry of squalene in oil samples. Rapid Commun.Mass Spectrom. 2006, 20, 325.
35. S. Fu, A. Segura-Carretero, D. Arrez-Romn, J. A. Menndez, A. De La Torre, A. Fernndez-Gutirrez. Tentative characterization of novel phenolic compounds in extra virgin olive oils by rapid-resolution liquid chromatography coupled with mass spectrometry. J. Agric. Food Chem. 2009, 57, 11140.
36. C. D. Calvano, C. G. Zambonin, O. N. Jensen. Assessment of lectin and HILIC based enrichment protocols for characterization of serum glycoproteins bymass spectrometry. J. Proteomics 2008, 71, 304.
37. B. Brugger, G. Erben, R. Sandhoff, F. T. Wieland, W. D. Lehmann. Quantitative analysis of biological membrane lipids at the low picomole level by nano-electrospray ionization tandem mass spectrometry. Proc. Natl. Acad. Sci. USA 1997, 94, 2339.
38. F. Xu, L. Zou, Q. Lin, C. N. Ong. Use of liquid chromatography/ tandem mass spectrometry and online databases for identification of phosphocholines and lysophosphatidylcholines in human red blood cells. Rapid Commun.Mass Spectrom. 2009, 23, 3243.