Transmission electron microscopy finds plenty of room on the surface

Physical Chemistry Chemical Physics

Volumn 17, Issue 22, 2015, Pages 14461-14469

  Zhang, Wei ^a   Zheng, Wei Tao ^a  

^a JILIN UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84930646627     PISSN: 14639076     EISSN: None     Source Type: Journal    
DOI: 10.1039/c5cp01705j     Document Type: Article

References (94)

1. E. Ruska Z. Tech. Phys. 1931 12 389
2. E. Ruska, Student project thesis, The High Voltage Laboratory of the Technische Hochschule Berlin, 1929
3. P. A. Midgley J. M. Thomas Multi-Dimensional Electron Microscopy Angew. Chem., Int. Ed. 2014 53 8614 8617
4. K. W. Urban Studying atomic structures by aberration-corrected transmission electron microscopy Science 2008 321 506 510
5. C. L. Jia K. Urban Atomic-resolution measurement of oxygen concentration in oxide materials Science 2004 303 2001 2004
6. N. Erdman K. R. Poeppelmeier M. Asta O. Warschkow D. E. Ellis L. D. Marks The structure and chemistry of the TiO2-rich surface of SrTiO3 (001) Nature 2002 419 55 58
7. G. Ertl Reactions at surfaces: From atoms to complexity (Nobel lecture) Angew. Chem., Int. Ed. 2008 47 3524 3535
8. W. Weiss W. Ranke Surface chemistry and catalysis on well-defined epitaxial iron-oxide layers Prog. Surf. Sci. 2002 70 1 151
9. W. Zhang W. Zheng Exsolution-Mimic Heterogeneous Surfaces: Towards Unlimited Catalyst Design ChemCatChem 2015 7 48 50
10. W. Zhang M. Chen L. TheilKuhn J. R. Bowen J. J. Bentzen Electrochemistry Unlocks Wettability: Epitaxial Growth of Oxide Nanoparticles on Rough Metallic Surfaces ChemElectroChem 2014 1 520 523
11. L. D. Marks Direct Imaging of Carbon-Covered and Clean Gold (110) Surfaces Phys. Rev. Lett. 1983 51 1000 1002
12. L. D. Marks D. J. Smith Direct surface imaging in small metal particles Nature 1983 303 316 317
13. L. D. Marks Direct atomic imaging of solid surfaces: I. Image simulation and interpretation Surf. Sci. 1984 139 281 298
14. L. D. Marks D. J. Smith Direct atomic imaging of solid surfaces: II. Gold (111) surfaces during and after in situ carbon etching Surf. Sci. 1984 143 495 508
15. D. J. Smith L. D. Marks Direct atomic imaging of solid surfaces: III. Small particles and extended Au surfaces Ultramicroscopy 1985 16 101 113
16. K. Takayanagi and K. Yagi, in Dynamic Processes on Solid Surfaces, ed., K. Tamaru, Springer Science+Business Media, New York, 1994, ch. 4
17. K. Takayanagi Surface structure imaging by electron microscopy J. Microsc. 1984 136 287 298
18. K. Yamazaki K. Takayanagi Y. Tanishiro K. Yagi Transmission electron microscope study of the reconstructed Au(001) surface Surf. Sci. 1988 199 595 608
19. K. Rajan P. Sewell Surface Analysis in the TEM J. Met. 1986 38 34 35
20. R. Yu L. H. Hu Z. Y. Cheng Y. D. Li H. Q. Ye J. Zhu Direct Subangstrom Measurement of Surfaces of Oxide Particles Phys. Rev. Lett. 2010 105 226101
21. W. Zhan R. Yu S. Lu Y. Li H. Chen J. Zhu Surface structure of alpha-Fe2O3 J. Chin. Electron Microsc. Soc. 2012 31 375
22. M. R. He R. Yu J. Zhu ubangstrom Profile Imaging of Relaxed ZnO(10-10) Surfaces Nano Lett. 2012 12 704 708
23. N. Lu Q. H. Wan J. Zhu Surface Structure of Zigzag SnO2 Nanobelts J. Phys. Chem. Lett. 2010 1 1468 1471
24. Y. Y. Lin Z. L. Wu J. G. Wen K. R. Poeppelmeier L. D. Marks Imaging the Atomic Surface Structures of CeO2 Nanoparticles Nano Lett. 2014 14 191 196
25. Y. Y. Lin J. G. Wen L. H. Hu R. M. Kennedy P. C. Stair K. R. Poeppelmeier L. D. Marks Synthesis-Dependent Atomic Surface Structures of Oxide Nanoparticles Phys. Rev. Lett. 2013 111 156101
26. W. Zhang A. Trunschke R. Schlogl D. S. Su Real-Space Observation of Surface Termination of a Complex Metal Oxide Catalyst Angew. Chem., Int. Ed. 2010 49 6084 6089
27. A. C. Sanfiz T. W. Hansen A. Sakthivel A. Trunschke R. Schlogl A. Knoester H. H. Brongersma M. H. Looi S. B. A. Hamid How important is the (001) plane of M1 for selective oxidation of propane to acrylic acid? J. Catal. 2008 258 35 43
28. Y. H. Zhu Q. X. Wang L. Zhao Y. Han Direct Observation of Surface Reconstruction and Termination on a Complex Metal Oxide Catalyst by Electron Microscopy Angew. Chem., Int. Ed. 2012 51 4176 4180
29. T. Lunkenbein J. Schumann M. Behrens R. Schlögl M. G. Willinger Formation of a ZnO Overlayer in Industrial Cu/ZnO/Al2O3 Catalysts Induced by Strong Metal-Support Interaction Angew. Chem., Int. Ed. 2015 54 4544 4548
30. H. M. Zheng J. B. Rivest T. A. Miller B. Sadtler A. Lindenberg M. F. Toney L. W. Wang C. Kisielowski A. P. Alivisatos Observation of Transient Structural-Transformation Dynamics in a Cu2S Nanorod Science 2011 333 206 209
31. M. R. He R. Yu J. Zhu Reversible Wurtzite-Tetragonal Reconstruction in ZnO(10-10) Surfaces Angew. Chem., Int. Ed. 2012 51 7744 7747
32. U. M. Bhatta I. M. Ross T. X. T. Sayle D. C. Sayle S. C. Parker D. Reid S. Seal A. Kumar G. Mobus Cationic Surface Reconstructions on Cerium Oxide Nanocrystals: An Aberration-Corrected HRTEM Study ACS Nano 2012 6 421 430
33. Y. Lin J. Wen L. Hu J. A. McCarthy S. Wang K. R. Poeppelmeier L. D. Marks Electron-induced Ti-rich surface segregation on SrTiO3 nanoparticles Micron 2015 68 152 157
34. M. Haruta Chance and Necessity: My Encounter with Gold Catalysts Angew. Chem., Int. Ed. 2014 53 52 56
35. B. S. Zhang D. Wang W. Zhang D. S. Su R. Schlogl Structural Dynamics of Low-Symmetry Au Nanoparticles Stimulated by Electron Irradiation Chem.-Eur. J. 2011 17 12877 12881
36. B. Song J. Jansen F. D. Tichelaar H. W. Zandbergen G. Gajewski C. W. Pao D. J. Srolovitz In-situ transmission electron microscopy and first-principles study of Au (100) surface dislocation dynamics Surf. Sci. 2013 608 154 164
37. A. Surrey D. Pohl L. Schultz B. Rellinghaus Quantitative Measurement of the Surface Self-Diffusion on Au Nanoparticles by Aberration-Corrected Transmission Electron Microscopy Nano Lett. 2012 12 6071 6077
38. G. Ertl Molecules at Surfaces: 100 Years of Physical Chemistry in Berlin-Dahlem Angew. Chem., Int. Ed. 2013 52 52 60
39. X. Bao M. Muhler B. Pettinger R. Schlögl G. Ertl On the nature of the active state of silver during catalytic oxidation of methanol Catal. Lett. 1993 22 215 225
40. X. Bao M. Muhler R. Schlögl G. Ertl Oxidative coupling of methane on silver catalysts Catal. Lett. 1995 32 185 194
41. D. S. Su T. Jacob T. W. Hansen D. Wang R. Schlogl B. Freitag S. Kujawa Surface chemistry of Ag particles: Identification of oxide species by aberration-corrected TEM and by DFT calculations Angew. Chem., Int. Ed. 2008 47 5005 5008
42. H. Yoshida Y. Kuwauchi J. R. Jinschek K. J. Sun S. Tanaka M. Kohyama S. Shimada M. Haruta S. Takeda Visualizing Gas Molecules Interacting with Supported Nanoparticulate Catalysts at Reaction Conditions Science 2012 335 317 319
43. S. E. Donnelly R. C. Birtcher C. W. Allen I. Morrison K. Furuya M. H. Song K. Mitsuishi U. Dahmen Ordering in a fluid inert gas confined by flat surfaces Science 2002 296 507 510
44. A. A. Herzing C. J. Kiely A. F. Carley P. Landon G. J. Hutchings Identification of active gold nanoclusters on iron oxide supports for CO oxidation Science 2008 321 1331 1335
45. V. Ortalan A. Uzun B. C. Gates N. D. Browning Direct imaging of single metal atoms and clusters in the pores of dealuminated HY zeolite Nat. Nanotechnol. 2010 5 506 510
46. B. T. Qiao A. Q. Wang X. F. Yang L. F. Allard Z. Jiang Y. T. Cui J. Y. Liu J. Li T. Zhang Single-atom catalysis of CO oxidation using Pt1/FeOx Nat. Chem. 2011 3 634 641
47. T. Y. Chang Y. Tanaka R. Ishikawa K. Toyoura K. Matsunaga Y. Ikuhara N. Shibata Direct Imaging of Pt Single Atoms Adsorbed on TiO2 (110) Surfaces Nano Lett. 2014 14 134 138
48. D. Alloyeau B. Freitag S. Dag L. W. Wang C. Kisielowski Atomic-resolution three-dimensional imaging of germanium self-interstitials near a surface: aberration-corrected transmission electron microscopy Phys. Rev. B: Condens. Matter Mater. Phys. 2009 80 014114
49. K. L. Kavanagh Are we seeing atoms diffuse? Physics 2009 2 63
50. Y. Zhu H. Inada K. Nakamura J. Wall Imaging single atoms using secondary electrons with an aberration-corrected electron microscope Nat. Mater. 2009 8 808 812
51. J. C. Meyer C. Kisielowski R. Erni M. D. Rossell M. F. Crommie A. Zettl Direct Imaging of Lattice Atoms and Topological Defects in Graphene Membranes Nano Lett. 2008 8 3582 3586
52. N. R. Wilson P. A. Pandey R. Beanland R. J. Young I. A. Kinloch L. Gong Z. Liu K. Suenaga J. P. Rourke S. J. York J. Sloan Graphene Oxide: Structural Analysis and Application as a Highly Transparent Support for Electron Microscopy ACS Nano 2009 3 2547 2556
53. U. Kaiser J. Biskupek J. C. Meyer J. Leschner L. Lechner H. Rose M. Stoger-Pollach A. N. Khlobystov P. Hartel H. Muller M. Haider S. Eyhusen G. Benner Transmission electron microscopy at 20 kV for imaging and spectroscopy Ultramicroscopy 2011 111 1239 1246
54. B. S. Zhang D. S. Su Transmission Electron Microscopy and the Science of Carbon Nanomaterials Small 2014 10 222 229
55. C. O. Girit J. C. Meyer R. Erni M. D. Rossell C. Kisielowski L. Yang C. H. Park M. F. Crommie M. L. Cohen S. G. Louie A. Zettl Graphene at the Edge: Stability and Dynamics Science 2009 323 1705 1708
56. A. Chuvilin J. C. Meyer G. Algara-Siller U. Kaiser From graphene constrictions to single carbon chains New J. Phys. 2009 11 083019
57. A. Chuvilin U. Kaiser E. Bichoutskaia N. A. Besley A. N. Khlobystov Direct transformation of graphene to fullerene Nat. Chem. 2010 2 450 453
58. F. R. Eder J. Kotakoski U. Kaiser J. C. Meyer A journey from order to disorder-Atom by atom transformation from graphene to a 2D carbon glass Sci. Rep. 2014 4 4060
59. Z. Q. Yang L. C. Yin J. Lee W. C. Ren H. M. Cheng H. Q. Ye S. T. Pantelides S. J. Pennycook M. F. Chisholm Direct Observation of Atomic Dynamics and Silicon Doping at a Topological Defect in Graphene Angew. Chem., Int. Ed. 2014 53 8908 8912
60. A. W. Robertson B. Montanari K. He J. Kim C. S. Allen Y. M. A. Wu J. Olivier J. Neethling N. Harrison A. I. Kirkland J. H. Warner Dynamics of Single Fe Atoms in Graphene Vacancies Nano Lett. 2013 13 1468 1475
61. J. C. Meyer A. Chuvilin G. Algara-Siller J. Biskupek U. Kaiser Selective Sputtering and Atomic Resolution Imaging of Atomically Thin Boron Nitride Membranes Nano Lett. 2009 9 2683 2689
62. H. P. Komsa J. Kotakoski S. Kurasch O. Lehtinen U. Kaiser A. V. Krasheninnikov Two-Dimensional Transition Metal Dichalcogenides under Electron Irradiation: Defect Production and Doping Phys. Rev. Lett. 2012 109 035503
63. S. Van Aert K. J. Batenburg M. D. Rossell R. Erni G. Van Tendeloo Three-dimensional atomic imaging of crystalline nanoparticles Nature 2011 470 374 377
64. I. Arslan T. J. V. Yates N. D. Browning P. A. Midgley Embedded nanostructures revealed in three dimensions Science 2005 309 2195 2198
65. D. Van Dyck J. R. Jinschek F. R. Chen 'Big Bang' tomography as a new route to atomic-resolution electron tomography Nature 2012 486 243 246
66. C. C. Chen C. Zhu E. R. White C. Y. Chiu M. C. Scott B. C. Regan L. D. Marks Y. Huang J. W. Miao Three-dimensional imaging of dislocations in a nanoparticle at atomic resolution Nature 2013 496 74 77
67. B. S. Zhang D. S. Su Electron Tomography: Three-Dimensional Imaging of Real Crystal Structures at Atomic Resolution Angew. Chem., Int. Ed. 2013 52 8504 8506
68. C. L. Jia S. B. Mi J. Barthel D. W. Wang R. E. Dunin-Borkowski K. W. Urban A. Thust Determination of the 3D shape of a nanoscale crystal with atomic resolution from a single image Nat. Mater. 2014 13 1044 1049
69. L. J. Allen Electron microscopy: Shape of a crystal from one image Nat. Mater. 2014 13 1000 1001
70. K. Takayanagi Y. Tanishiro S. Takahashi M. Takahashi Structure analysis of Si(111)-7 × 7 reconstructed surface by transmission electron diffraction Surf. Sci. 1985 164 367 392
71. K. Yagi, RHEED and REM, in Electron Diffraction Techniques II, ed., J. M. Cowley, Oxford University Press, 1993
72. N. Osakabe Y. Tanishiro K. Yagi G. Honjo Reflection electron microscopy of clean and gold deposited (111) silicon surfaces Surf. Sci. 1980 97 393 408
73. K. Yagi Reflection electron microscopy J. Appl. Crystallogr. 1987 20 147 160
74. O. Nobuyuki T. Yasumasa Y. Katsumichi H. Goro Image contrast of dislocations and atomic steps on (111) silicon surface in reflection electron microscopy Surf. Sci. 1981 102 424 442
75. S. Lee M. F. Toney W. Ko J. C. Randel H. J. Jung K. Munakata J. Lu T. H. Geballe M. R. Beasley R. Sinclair H. C. Manoharan A. Salleo Laser-Synthesized Epitaxial Graphene ACS Nano 2010 4 7524 7530
76. H. Minoda K. Hatano H. Yazawa Development of a surface conductivity measurement system for ultrahigh vacuum transmission electron microscope Rev. Sci. Instrum. 2009 80 113702
77. M. G. Willinger W. Zhang O. Bondarchuk S. Shaikhutdinov H. J. Freund R. Schlogl A Case of Strong Metal-Support Interactions: Combining Advanced Microscopy and Model Systems to Elucidate the Atomic Structure of Interfaces Angew. Chem., Int. Ed. 2014 53 5998 6001
78. K. Suenaga Elemental analysis down to the single atom with electron beams C. R. Phys. 2014 15 151 157
79. K. Suenaga T. Okazaki E. Okunishi S. Matsumura Detection of photons emitted from single erbium atoms in energy-dispersive X-ray spectroscopy Nat. Photonics 2012 6 545 548
80. Q. M. Ramasse C. R. Seabourne D.-M. Kepaptsoglou R. Zan U. Bangert A. J. Scott Probing the Bonding and Electronic Structure of Single Atom Dopants in Graphene with Electron Energy Loss Spectroscopy Nano Lett. 2012 13 4989 4995
81. W. Zhou M. D. Kapetanakis M. P. Prange S. T. Pantelides S. J. Pennycook J.-C. Idrobo Direct Determination of the Chemical Bonding of Individual Impurities in Graphene Phys. Rev. Lett. 2012 109 206803
82. T. C. Lovejoy Q. M. Ramasse M. Falke A. Kaeppel R. Terborg R. Zan N. Dellby O. L. Krivanek Single atom identification by energy dispersive x-ray spectroscopy Appl. Phys. Lett. 2012 100 154101
83. A. V. Krasheninnikov F. Banhart Engineering of nanostructured carbon materials with electron or ion beams Nat. Mater. 2007 6 723 733
84. W. Zhang L. TheilKuhn Strong Metal-Support Interaction: Growth of Individual Carbon Nanofibers from Amorphous Carbon Interacting with an Electron Beam ChemCatChem 2013 5 2591 2594
85. W. Zhang B. Zhang T. Wolfram L. Shao R. Schlögl D. S. Su Probing a Redox Behavior of TiO2/SBA-15 Supported VxOy Catalyst Using an Electron Beam in a 200 kV Transmission Electron Microscope J. Phys. Chem. C 2011 115 20550 20554
86. F. Krause Naturwissenschaften 1937 25 817 825
87. E. Driest H. O. Mueller Z. Wiss. Mikrosk. 1935 52 53 57
88. D. Beischer F. Krause Naturwissenschaften 1937 25 825 829
89. S. Iijima High-Resolution Electron Microscopy of Crystal Lattice of Titanium-Niobium Oxide J. Appl. Phys. 1971 42 5891 5893
90. M. Haider S. Uhlemann E. Schwan H. Rose B. Kabius K. Urban Electron microscopy image enhanced Nature 1998 392 768 769
91. O. H. Kwon A. H. Zewail 4D Electron Tomography Science 2010 328 1668 1673
92. D. S. Su Electron Tomography: From 3D Statics to 4D Dynamics Angew. Chem., Int. Ed. 2010 49 9569 9571
93. S. Uhlemann H. Muller P. Hartel J. Zach M. Haider Thermal Magnetic Field Noise Limits Resolution in Transmission Electron Microscopy Phys. Rev. Lett. 2013 111 046101
94. L. Marks What Are the Resolution Limits in Electron Microscopes? Physics 2013 6 82