A new and improved strategy combining a dispersive-solid phase extraction-based multiclass method with ultra high pressure liquid chromatography for analysis of low molecular weight polyphenols in vegetables

Journal of Chromatography A

Volumn 1260, Issue , 2012, Pages 154-163

  Silva, Catarina L ^a   Haesen, Nathaly ^b   Câmara, José S ^a  

^a UNIVERSITY OF MADEIRA   (Portugal)

^b Thomas More University College   (Belgium)

Author keywords

DSPE QuEChERS; Free low molecular weight polyphenols; UHPLC PDA; Vegetables

Indexed keywords

ANALYTICAL COLUMNS; CONCENTRATION LEVELS; CONCENTRATION RANGES; DETECTION SYSTEM; DSPE-QUECHERS; EXTRACTION EFFICIENCIES; EXTRACTION TECHNIQUES; FIGURES OF MERITS; FOOD QUALITY; GREEN PEPPER; HIGH STRENGTH; LIMIT OF DETECTION; LIMIT OF QUANTIFICATIONS; LINEAR DYNAMIC RANGES; LOW MOLECULAR WEIGHT POLYPHENOLS; MATRIX EFFECTS; MOBILE PHASE; MULTICLASS METHODS; PHASE EXTRACTION; POLAR COMPOUNDS; POLYPHENOLS; RED PEPPERS; RELATIVE STANDARD DEVIATIONS; REPRODUCIBILITIES; SALT SOLUTION; SILICA CAPILLARY; SYRINGIC ACID; TRANS-RESVERATROL; UHPLC-PDA; ULTRA HIGH PRESSURE LIQUID CHROMATOGRAPHY (UHPLC); ULTRAHIGH-PRESSURE LIQUID CHROMATOGRAPHIES; VALIDATION PARAMETERS; VEGETABLE EXTRACTS; VEGETABLE SAMPLES;

CHROMATOGRAPHY; FLAVONOIDS; FORMIC ACID; HIGH PRESSURE LIQUID CHROMATOGRAPHY; METHANOL; MOLECULAR WEIGHT; ORGANIC COMPOUNDS; ORGANIC SOLVENTS; PHENOLS; SILICA; VEGETABLES;

EXTRACTION;

CATECHIN; CINNAMIC ACID; COUMARIC ACID; EPICATECHIN; FERULIC ACID; GENTISIC ACID; KAEMPFEROL; ORGANIC SOLVENT; POLYPHENOL; PROTOCATECHUIC ACID; RESVERATROL; SERINGALDEHYDE; SILICON DIOXIDE; SODIUM CHLORIDE; SYRINGIC ACID; UNCLASSIFIED DRUG;

ANALYTICAL EQUIPMENT; ARTICLE; BEETROOT; BROCCOLI; CAPILLARY CHROMATOGRAPHY; CARROT; CONCENTRATION (PARAMETERS); DESICCATION; DISPERSIVE SOLID PHASE EXTRACTION; DYNAMICS; FEASIBILITY STUDY; FOOD ANALYSIS; FOOD QUALITY; GARLIC; HOMOGENATE; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MOLECULAR WEIGHT; NONHUMAN; ONION; PHOTODIODE ARRAY DETECTION SYSTEM; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; RELIABILITY; SOLID PHASE EXTRACTION; SUPERNATANT; SWEET PEPPER; TOMATO; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; VALIDATION PROCESS; VEGETABLE;

ACETONITRILES; ANALYSIS OF VARIANCE; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; LEAST-SQUARES ANALYSIS; LIMIT OF DETECTION; MAGNESIUM SULFATE; MOLECULAR WEIGHT; POLYPHENOLS; REPRODUCIBILITY OF RESULTS; SODIUM CHLORIDE; SOLID PHASE EXTRACTION; VEGETABLES;

ALLIUM CEPA; ALLIUM SATIVUM; BRASSICA OLERACEA VAR. ITALICA; CAPSICUM ANNUUM VAR. ANNUUM; DAUCUS CAROTA; LYCOPERSICON ESCULENTUM;

EID: 84866531760     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.08.082     Document Type: Article

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