Development of a new QuEChERS method based on dry ice for the determination of 168 pesticides in paprika using tandem mass spectrometry

Journal of Chromatography A

Volumn 1218, Issue 28, 2011, Pages 4366-4377

  Lee, Sung Woo ^a   Choi, Jeong Heui ^b   Cho, Soon Kil ^a   Yu, Hyun A ^a   Abd El Aty, A M ^c   Shim, Jae Han ^b  

^a Ministry of Agriculture and Forestry Korea   (South Korea)

^b Chonnam National University   (South Korea)

^c Cairo University   (Egypt)

Author keywords

Dry ice; Paprika; Pesticides; Problematic pesticides; QuEChERS; Tandem mass spectrometry

Indexed keywords

DRY ICE; PAPRIKA; PROBLEMATIC PESTICIDES; QUECHERS; TANDEM MASS SPECTROMETRY;

ACETONITRILE; AGRICULTURAL CHEMICALS; CARBON DIOXIDE; EXTRACTION; MASS SPECTROMETRY; PESTICIDES; RECOVERY; REFRIGERANTS;

ICE;

ABAMECTIN; ACETONITRILE; ALACHLOR; ALDICARB; AZINPHOS METHYL; BIFENTHRIN; CARBARIL; CARBOFURAN; CARBON DIOXIDE; CARBOSULFAN; CHLORPYRIFOS METHYL; CITRIC ACID; DELTAMETHRIN; DICHLOFLUANID; DICHLORVOS; DIFLUBENZURON; DIMETHOATE; DIMPYLATE; EDIFENPHOS; ETHIOFENCARB; ETHOPROP; ETRIMFOS; FENTHION; FIPRONIL; IMIDACLOPRID; ISOPROCARB; METHOMYL; MOLINATE; PESTICIDE;

ARTICLE; CALIBRATION; CONTROLLED STUDY; EXTRACTION; FOOD ANALYSIS; INTERMETHOD COMPARISON; PEPPER; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PRODUCT RECOVERY; QUICK EASY CHEAP EFFECTIVE RUGGED AND SAFE EXTRACTION; TANDEM MASS SPECTROMETRY;

CAPSICUM; CHEMICAL FRACTIONATION; CHROMATOGRAPHY, LIQUID; DRY ICE; PESTICIDE RESIDUES; TANDEM MASS SPECTROMETRY;

EID: 79959328993     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.05.021     Document Type: Article

References (52)

1. Seiber J.N. Crop Production, Public Health, Environmental Safety 2007, 315. Wiley-VCH, Weinheim, Germany. H. Ohkawa, H. Miyagawa, P.W. Lee (Eds.).
2. Rache K.D. Crop Production, Public Health, Environmental Safety 2007, 29. Wiley-VCH, Weinheim, Germany. H. Ohkawa, H. Miyagawa, P.W. Lee (Eds.).
3. Understanding the Codex Alimentarius 2006, Joint FAO/WHO Food Standards Programme, FAO, Rome, Italy, p. 10 (available at ftp://ftp.fao.org/codex/Publications/understanding/Understanding_EN.pdf). 3rd ed.
4. Tayaputch N. Crop Production, Public Health, Environmental Safety 2007, 341. Wiley-VCH, Weinheim, Germany. H. Ohkawa, H. Miyagawa, P.W. Lee (Eds.).
5. MRLs for Pesticides in Foods 2009, Korea Health Industry Development Institute, Seoul, Republic of Korea, p. 123.
6. Table of MRLs for Agricultural Chemicals, the Japan Food Chemical Research Foundation (available at). http://www.m5.ws001.squarestart.ne.jp/foundation/agrdtl.php?a_inq=65450.
7. Kim H.W. An Extraordinary General Meeting and an Autumn Conference of the Korean Society of Pesticide Science 2009, Book of Abstract, Republic of Korea, p. 15.
8. The Food Code, Part V, No. 4.1.4.111 Flonicamid, Korea Food and Drug Administration (available at). http://www.foodnara.go.kr/portal/site/kfdaportal/infotelegram.
9. Hengel M.J., Miller M. J. Agric. Food Chem. 2007, 55:8033.
10. Cover sheet for Environmental Chemistry Method, Development and validation of analytical method for the determination of IKI-220 residues in soil-report amendment, ISK Biosciences Corporation, 2002 (available at). http://www.epa.gov/opp00001/methods/ecmmethods/458548-14-S.pdf.
11. Anastassiades M., Lehotay S.J., Štajnbaher D., Schenck F.J. J. AOAC Int. 2003, 86:412.
12. Lehotay S.J., De Kok A., Hiemstra M., Van Bodegraven P. J. AOAC Int. 2005, 88:595.
13. Lehotay S.J., Maštovská K., Lightfield A.R. J. AOAC Int. 2005, 88:615.
14. Maštovská K., Lehotay S.J. J. Chromatogr. A 2004, 1040:259.
15. Lehotay S.J., Maštovská K. J. AOAC Int. 2005, 88:630.
16. Lehotay S.J. J. AOAC Int. 2007, 90:485.
17. Chung S.W.C., Chan B.T.P. J. Chromatogr. A 2000, 1217:4815.
18. Lesueur C., Knittl P., Gartner M., Mentler A., Fuerhacker M. Food Contr. 2008, 19:906.
19. Lehotay S.J., Son K.A., Kwon H., Koesukwiwat U., Fu W., Mastovska K., Hoh E., Leepipatpiboon N. J. Chromatogr. A 2010, 1217:2548.
20. European Standard EN 15662 Foods of Plant Origin-Determination of Pesticide Residues using GC-MS and/or LC-MS/MS Following Acetonitrile Extraction/Partitioning and Clean-up by Dispersive SPE-QuEChERS-method 2008, European Committee for Standardization, Brussels.
21. Romero-González R., Frenich A.G., Vidal J.L.M. Talanta 2008, 76:211.
22. Tsiplakou E., Anagnostopoulos C.J., Liapis K., Haroutounian S.A., Zervas G. Chemosphere 2010, 80:504.
23. Lacina O., Urbanova J., Poustka J., Hajslova J. J. Chromatogr. A 2010, 1217:648.
24. Payá P., Anastassiades M., Mack D., Sigalova I., Tasdelen B., Oliva J., Barba A. Anal. Bioanal. Chem. 2007, 389:1697.
25. Takatori S., Okihashi M., Okamoto Y., Kitagawa Y., Kakimoto S., Murata H., Sumimoto T., Tanaka Y. J. AOAC Int. 2008, 91:871.
26. Nguyen T.D., Han E.M., Seo M.S., Kim S.R., Yun M.Y., Lee D.M., Lee G.-H. Anal. Chim. Acta 2008, 619:67.
27. Díez C., Traag W.A., Zommer P., Marinero P., Atienza J. J. Chromatogr. A 2006, 1131:11.
28. Koesukwiwat U., Sanguankaew K., Leepipatpiboon N. Anal. Chim. Acta 2008, 626:10.
29. Koesukwiwat U., Lehotay S.J., Mastovska K., Dorweiler K.J., Leepipatpiboon N. J. Agric. Food Chem. 2010, 58:5950.
30. Mastovska K., Dorweiler K.J., Lehotay S.J., Wegscheid J.S., Szpylka K.A. J. Agric. Food Chem. 2010, 58:5959.
31. Lesueur C., Gartner M., Mentler A., Fuerhacker M. Talanta 2008, 75:284.
32. Cunha S.C., Lehotay S.J., Mastovska K., Fernandes J.O., Beatriz M., Oliveira P.P. J. Sep. Sci. 2007, 30:620.
33. S.J. Lehotay, in: J.L. Martinez Vidal, A. Garrido Frenich (Eds.), Methods in Biotechnology, vol. 19, Pesticide Protocols, Humana Press, Totowa, NJ, 2005, pp. 239-261.
34. QuEChERS, A mini-multiresidue method for the analysis of pesticide residues in low-fat products (available at). http://www.quechers.com/.
35. Jansson C., Pihlström T., Österdahl B.-G., Markides K.E. J. Chromatogr. A 2004, 1023:93.
36. Kruve A., Künnapas A., Herodes K., Leito I. J. Chromatogr. A 2008, 1187:58.
37. Hiemstra M., de Kok A. J. Chromatogr. A 2007, 1154:3.
38. Kanrar B., Mandal S., Bhattacharyya A. J. Chromatogr. A 2010, 1217:1926.
39. Kim W.-J., Kim J.-D., Kim J.K., Oh S.-G., Lee Y.-W. J. Food Eng. 2008, 89:303.
40. Motohashi N., Nagashima H., Párkányi C. J. Biochem. Biophys. Methods 2000, 43:313.
41. Choi J.-H., Mamun M.I.R., Abd El-Aty A.M., Kim K.T., Koh H.-B., Shin H.-C., Kim J.-S., Lee K.B., Shim J.-H. Talanta 2009, 78:348.
42. Anitescu G., Tavlarides L.L. J. Supercrit. Fluids 2006, 38:167.
43. Moore J.W., Stanitski C.L., Jurs P.C. Chapter 11, Liquids, Solids, and Materials, Chemistry, The Molecular Science 2005, Thomson Learning, Inc., CA, USA, p. 487-543. 2nd ed.
44. van Meurs M., Somsen G. J. Solut. Chem. 1993, 22:427.
45. Niessen W.M.A., Manini P., Andreoli R. Mass Spectrum. Rev. 2006, 25:881.
46. Zrostlíková J., Hajšlová J., Poustka J., Begany P. J. Chromatogr. A 2002, 973:13.
47. Kmellár B., Fodor P., Parefa L., Ferrer C., Martínez-Uroz M.A., Valverde A., Fernandez-Alba A.R. J. Chromatogr. A 2008, 1215:37.
48. Koesukwiwat U., Lehotay S.J., Miao S., Leepipatpiboon N. J. Chromatogr. A 2010, 1217:6692.
49. Codex Alimentarius, Guidelines on the use of mass spectrometry (MS) for identification, confirmation and quantitative determination of residues, CAC/GL 56-2005.
50. European Commission, Method validation and quality control procedures for pesticide residues analysis in food and feed, Document No. SANCO/10684/2009.
51. Fussell R.J., Addie K.J., Reynolds S.L., Wilson M.F. J. Agric. Food Chem. 2002, 50:441.
52. Soler C., Mañes J., Picó Y. J. Chromatogr. A 2006, 1109:228.