Optimization of ultrasound assisted-emulsification-dispersive liquid-liquid microextraction by experimental design methodologies for the determination of sulfur compounds in wines by gas chromatography-mass spectrometry

Analytica Chimica Acta

Volumn 683, Issue 1, 2010, Pages 126-135

  Jofré, Viviana P ^a   Assof, Mariela V ^a   Fanzone, Martín L ^a   Goicoechea, Héctor C ^b,d   Martínez, Luis D ^b,c   Silva, María F ^b  

^a INSTITUTO NACIONAL DE TECNOLOGÍA AGROPECUARIA INTA   (Argentina)

^b Facultad de Ciencias Naturales e Instituto M Lillo   (Argentina)

^c UNIVERSIDAD NACIONAL DE SAN LUIS   (Argentina)

^d UNIVERSIDAD NACIONAL DEL LITORAL   (Argentina)

Author keywords

Experimental design; Sulfur compound; Ultrasound assisted emulsification dispersive liquid liquid microextraction gas chromatography mass spectrometry; Wine

Indexed keywords

4-METHYL-2-PENTANONE; ANALYTES; ANALYTICAL METHOD; CALIBRATION GRAPHS; CENTRAL COMPOSITE DESIGNS; DESIRABILITY FUNCTION; DISPERSIVE LIQUID-LIQUID MICROEXTRACTION; EXPERIMENTAL CONDITIONS; EXPERIMENTAL DESIGN; EXTRACTANTS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIMITS OF QUANTITATIONS; MATRIX; METHOD DETECTION LIMITS; MINIMUM INTERFERENCE; MULTIPLE RESPONSE; OPERATIONAL CONDITIONS; POSITIVE EFFECTS; SAMPLE VOLUME; SCREENING DESIGN; SIMULTANEOUS DETERMINATIONS; SIMULTANEOUS OPTIMIZATION; ULTRASOUND ASSISTED-EMULSIFICATION-DISPERSIVE LIQUID-LIQUID MICROEXTRACTION/GAS CHROMATOGRAPHY-MASS SPECTROMETRY; WHITE WINES; WINE SAMPLE;

CAVITATION; CENTRIFUGATION; CENTRIFUGES; DESIGN; EMULSIFICATION; GAS CHROMATOGRAPHY; IONIC STRENGTH; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; OPTIMIZATION; SODIUM CHLORIDE; SOLVENT EXTRACTION; STATISTICS; SULFUR; SULFUR COMPOUNDS; SULFUR DETERMINATION; ULTRASONIC APPLICATIONS; ULTRASONICS; WINE;

LIQUIDS;

SOLVENT; SULFUR DERIVATIVE;

ACCURACY; ANALYTIC METHOD; ARTICLE; CALIBRATION; CENTRIFUGATION; CHEMICAL COMPOSITION; CONTROLLED STUDY; EMULSION; EXPERIMENTAL DESIGN; FOOD ANALYSIS; GAS CHROMATOGRAPHY; IONIC STRENGTH; LIQUID LIQUID EXTRACTION; MASS SPECTROMETRY; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION; QUANTITATIVE ANALYSIS; ULTRASOUND; WINE;

EID: 78649323290     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2010.10.010     Document Type: Article

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