Use of the 1H nuclear magnetic resonance spectra signals from polyphenols and acids for chemometric characterization of cider apple juices

Journal of Agricultural and Food Chemistry

Volumn 54, Issue 8, 2006, Pages 3095-3100

  Del Campo, Gloria ^a   Santos, J Ignacio ^a   Iturriza, Nuria ^a   Berregi, Iñaki ^a   Munduate, Arantxa ^a  

^a UNIVERSITY OF THE BASQUE COUNTRY UPV EHU   (Spain)

Author keywords

1H NMR; Chemometrics; Cider apple juice; Varietal characterization

Indexed keywords

MALUS X DOMESTICA;

CARBOXYLIC ACID; FLAVONOID; PHENOL DERIVATIVE; POLYPHENOLS;

APPLE; ARTICLE; BEVERAGE; CHEMISTRY; CLASSIFICATION; FRUIT; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

BEVERAGES; CARBOXYLIC ACIDS; FLAVONOIDS; FRUIT; MAGNETIC RESONANCE SPECTROSCOPY; MALUS; PHENOLS;

EID: 33646535829     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf051818c     Document Type: Article

References (34)

1. Lea, A. G. H. Cidermaking. In Fermented Beverage Production; Lea, A. G. H., Piggot, J. R., Eds.; Blackie Academic & Proffesional: London, United Kingdom, 1995; pp 66-96.
2. Van Buren, J. Fruit phenolics. In The Biochemistry of Fruits and Their Products; Hulmes, A. C., Ed.; Academic Press: London, United Kingdom, 1970; Vol. 1, pp 269-304.
3. Lee, H. S.; Wrolstad, R. E. Apple composition: Sugar, non-volatile acid and phenolic profiles. J. Assoc. Off. Anal. Chem. 1988, 71, 789-794.
4. Fuleki, T.; Pelayo, E.; Palabay, R. Sugar composition of varietal juices produced from fresh and stored apples. J. Agric. Food Chem. 1994, 42, 1266-1275.
5. Blanco-Gomis, D.; Herrero-Sánchez, I.; Mangas, J. J. Characterisation of apple cider cultivars by chemometric techniques using data from high-performance liquid chromatography and flow-injection analysis. Analyst 1998, 123, 1187-1191.
6. Fuleki, T.; Pelayo, E.; Palabay, R. Carboxilic acid composition of varietal juices produced from fresh and stored apples. J. Agric. Food Chem. 1995, 43, 598-607.
7. Price, K. R.; Prosser, T.; Richetin, A. M. F.; Rhodes, M. J. C. A comparison of the flavonol content and composition in dessert, cooking and cider-making apples; distribution within the fruit and effect of juicing. Food Chem. 1999, 66, 489-494.
8. Sanoner, P.; Guyot, S.; Marnet, N.; Molle, D.; Drilleau, J. F. Polyphenol profiles of French cider apple varieties. J. Agric. Food Chem. 1999, 47, 4847-4853.
9. Alonso-Salces, R. M.; Korta, E.; Barranco, A.; Berrueta, L. A.; Gallo, B.; Vicente, F. Determination of polyphenolic profiles of Basque cider apple varieties using accelerated solvent extraction. J. Agric. Food Chem. 2001, 49, 3761-3767.
10. Hills, B. P.; Clark, C. J. Quality assessment of horticultural products by NMR. Ann. Rep. NMR Spectrosc. 2003, 75-120.
11. Eads, T. M.; Bryant, R. G. High-resolution proton NMR spectroscopy of milk, orange juice, and apple juice with efficient suppression of the water peak. J. Agric. Food Chem. 1986, 34, 834-837.
12. Bastoni, L.; Bianco, A.; Piccioni, F.; Uccella, N. Biophenolic profile in olives by nuclear magnetic resonance. Food Chem. 2001, 73, 145-151.
13. Košir, I. J.; Kidrič, J. Use of modern nuclear magnetic resonance spectroscopy in wine analysis: Determination of minor compounds. Anal. Chim. Acta 2002, 458, 77-84.
14. Belton, P. S.; Delgadillo, I.; Holmes, E.; Nicholls, A.; Nicholson, J. K.; Spraul, M. Use of high-field NMR spectroscopy for the analysis of liquid foods. J. Agric. Food Chem. 1996, 44, 1483-1487.
15. Belton, P. S.; Delgadillo, I.; Gil, A. M.; Casuscelli, F.; Colquhoun, I. J.; Dennis, M. J.; Spraul, M. High-field proton NMR studies of apple juices. Magn. Reson. Chem. 1997, 35, S52-S60.
16. Gil, A. M.; Duarte, I. F.; Delgadillo, I.; Colquhoun, I. J.; Casuscelli, F.; Humpfer, E.; Spraul, M. Study of the compositional changes of mango during ripening by use of nuclear magnetic resonance spectroscopy. J. Agric. Food Chem. 2000, 48, 1524-1536.
17. Holzgrave, U.; Waber, I.; Diehl, B. W. K. NMR Spectroscopy in Drug Development and Analysis; Wiley-VCH: Weinheim, 1999.
18. Rizzo, V.; Pinciroli, V. Quantitative NMR in synthetic and combinatorial chemistry. J. Pharm. Biomed. Anal. 2005, 38, 851-857.
19. Szantay, C.; Demete, A. In Identification and Determination of Impurities in Drugs; Görög, S., Ed.; Elsevier: Amsterdam, 2000; pp 109-145.
20. 1H NMR spectrometry. Anal. Chim. Acta 2005, 552, 160-165.
21. 1H NMR as a tool for the analysis of mixtures of virgin olive with oils of different botanical origin. Magn. Reson. Chem. 2000, 32, 436-443.
22. Brescia, M. A.; Caldarola, V.; De Giglio, A.; Benedetti, D.; Fanizzi, F. P.; Sacco, A. Characterization of the geographical origin of Italian red wines based on traditional and nuclear magnetic resonance sprectrometric determinations. Anal. Chim. Acta 2002, 458, 177-186.
23. 1H NMR and multivariate statistics for screening complex mixtures: Quality control and authenticity of instant coffee. J. Agric. Food Chem. 2002, 50, 3098-3103.
24. Colquhoun, I. J. High-resolution NMR spectroscopy in food analysis and authentication. Spectrosc. Eur. 1998, 10 (1), 8-18.
25. Fragaki, G.; Spyros, A.; Siragakis, G.; Salivaras, E.; Dais, P. Detection of extra virgin olive oil adulteration with lampante olive oil and refined olive oil using nuclear magnetic resonance spectroscopy and multivariate statistical analysis. J. Agric. Food Chem. 2005, 53, 2810-2816.
26. 1H NMR spectra of apple juices: Discrimination between apple varieties. Food Chem. 1998, 61, 207-213.
27. 1H NMR spectrometry. Anal. Chim. Acta 2003, 486, 269-274.
28. Liu, M.; Mao, X.; He, C.; Huang, H.; Nicholson, J. K.; Lindon, J. C. Water suppression using Watergate W5 pulse sequence with gradients using double echo. J. Magn. Reson. 1998, 132, 125-130.
29. 1H NMR. Talanta 2003, 61, 139-145.
30. Massart, D. L.; Vandeginste, B. G. M.; Buydens, L. M. C.; De Jong, S.; Lewi, P. J.; Smeyers-Verbeke, J. Handbook of Chemometrics and Qualimetrics: Part B; Elsevier: Amsterdam, 1997; pp 57-85, 207-238.
31. Sobolev, A. P.; Segre, A.; Lamanna, R. Proton high-field NMR study of tomate juice. Magn. Reson. Chem. 2003, 41, 237-245.
32. Del Campo, G.; Berregi, I.; Caracena, R.; Santos, J. I. Quantitative analysis of malic and citric acids in fruit juices using proton nuclear magnetic resonance spectroscopy. Anal. Chim. Acta 2006, 556, 462-468.
33. Acree, T. E.; McLellan, M. R. Flavor components and quality attributes. In Processed Apple Products; Downing, D. L., Ed.; Van Nostrand Reinhold: New York, 1989; p 320.
34. Del Campo, G.; Santos, J. I.; Berregi, I.; Munduate, A. Differentiation of Basque cider apple juices from different cultivars by means of chemometric techniques. Food Control 2005, 16, 551-557.