Dynamics of the temperature distribution in ultra-fast thin-film calorimeter sensors

Thermochimica Acta

Volumn 603, Issue , 2015, Pages 205-217

  Minakov, Alexander A ^a   Schick, Christoph ^a  

^a UNIVERSITY OF ROSTOCK   (Germany)

Author keywords

Fast scanning calorimetry; Nanocalorimetry; Thin film calorimetry; Ultra fast cooling

Indexed keywords

CALORIMETERS; CALORIMETRY; COOLING; GAGES; SILICON NITRIDE; TEMPERATURE DISTRIBUTION;

CONTROLLED COOLING; FAST-SCANNING CALORIMETRIES; NANOCALORIMETRY; PHASE TRANSITION KINETICS; THIN-FILM CALORIMETERS; THIN-FILM CALORIMETRY; ULTRA-FAST COOLING; ULTRA-FAST HEATING;

THIN FILMS;

EID: 85027956493     PISSN: 00406031     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tca.2014.05.030     Document Type: Article

References (55)

1. M.Y. Efremov, E.A. Olson, M. Zhang, S.L. Lai, F. Schiettekatte, Z.S. Zhang, and L.H. Allen Thin-film differential scanning nanocalorimetry: heat capacity analysis Thermochim. Acta 412 2004 13 23
2. E.A. Olson, M.Y. Efremov, M. Zhang, Z.S. Zhang, and L.H. Allen The design and operation of a MEMS differential scanning nanocalorimeter for high-speed heat capacity measurements of ultrathin films J. Microelectromech. Syst. 12 2003 355 364
3. S.L. Lai, J.Y. Guo, V. Petrova, G. Ramanath, and L.H. Allen Size-dependent melting properties of small tin particles: nanocalorimetric measurements Phys. Rev. Lett. 77 1996 99 102
4. 2) Appl. Phys. Lett. 67 1995 1229 1231
5. S.A. Adamovsky, A.A. Minakov, and C. Schick Scanning microcalorimetry at high cooling rate Thermochim. Acta 403 2003 55 63
6. A.A. Minakov, S.A. Adamovsky, and C. Schick Non adiabatic thin-film (chip) nanocalorimetry Thermochim. Acta 432 2005 177 185
7. A. Minakov, J. Morikawa, T. Hashimoto, H. Huth, and C. Schick Temperature distribution in a thin-film chip utilized for advanced nanocalorimetry Meas. Sci. Technol. 17 2006 199 207
8. A.A. Minakov, and C. Schick Ultra-fast thermal processing and nanocalorimetry at heating and cooling rates up to 1 MK/s Rev. Sci. Instrum. 78 2007 073902 073910
9. A.A. Minakov, A.W. van Herwaarden, W. Wien, A. Wurm, and C. Schick Advanced nonadiabatic ultra-fast nanocalorimetry and superheating phenomenon in linear polymers Thermochim. Acta 461 2007 96 106
10. A.W. van Herwaarden Overview of calorimeter chips for various applications Thermochim. Acta 432 2005 192 201
11. K. Xiao, J.M. Gregoire, P.J. McCluskey, D. Dale, and J.J. Vlassak Scanning AC nanocalorimetry combined with in-situ X-ray diffraction J. Appl. Phys. 113 2013 243501 243510
12. 0.16 thin-film sample Appl. Phys. Lett. 102 2013 201902 201904
13. J.M. Gregoire, P.J. McCluskey, D. Dale, S. Ding, J. Schroers, and J.J. Vlassak Combining combinatorial nanocalorimetry and X-ray diffraction techniques to study the effects of composition and quench rate on Au-Cu-Si metallic glasses Scripta Mater. 66 2012 178 181
14. N. Piazzon, M. Rosenthal, A. Bondar, D. Spitzer, and D.A. Ivanov Characterization of explosives traces by the nanocalorimetry J. Phys. Chem. Solid 71 2010 114 118
15. M. Rosenthal, D. Doblas, J.J. Hernandez, Y.I. Odarchenko, M. Burghammer, E. Di Cola, D. Spitzer, A.E. Antipov, L.S. Aldoshin, and D.A. Ivanov High-resolution thermal imaging with a combination of nano-focus X-ray diffraction and ultra-fast chip calorimetry J. Synchrotron. Radiat. 21 2014 223 228
16. E. Zhuravlev, and C. Schick Fast scanning power compensated differential scanning nano-calorimeter: 2. Heat capacity analysis Thermochim. Acta 505 2010 14 21
17. E. Zhuravlev, and C. Schick Fast scanning power compensated differential scanning nano-calorimeter: 1. The device Thermochim. Acta 505 2010 1 13
18. A. Sepúlveda, A.F. Lopeandía, R. Domènech-Ferrer, G. Garcia, F. Pi, J. Rodríguez-Viejo, and F.J. Muñoz Microchip power compensated calorimetry applied to metal hydride characterization Int. J. Hydrogen Energy 33 2008 2729 2737
19. A.F. Lopeandia, J. Valenzuela, and J. Rodríguez-Viejo Power compensated thin film calorimetry at fast heating rates Sens. Actuators A: Phys. 143 2008 256 264
20. A.F. Lopeandia, E. Leon-Gutierrez, J. Rodriguez-Viejo, and F.J. Munoz Design issues involved in the development of a membrane-based high-temperature nanocalorimeter Microelectron. Eng. 84 2007 1288 1291
21. A.F. Lopeandia, J. Rodriguez-Viejo, M. Chacon, M.T. Clavaguera-Mora, and F.J. Munoz Heat transfer in symmetric U-shaped microreactors for thin film calorimetry J. Micromech. Microeng. 16 2006 965 971
22. A.F. Lopeandía, E. Leon-Gutierrez, G. Garcia, F. Pi, A. Bernardi, A.R. Goñi, M.I. Alonso, and J. Rodríguez-Viejo Nanocalorimetric high-temperature characterization of ultrathin films of a-Ge Mater. Sci. Semicon. Process. 9 2006 806 811
23. A.F. Lopeandía, L.I. Cerdó, M.T. Clavaguera-Mora, L.R. Arana, K.F. Jensen, F.J. Muñoz, and J. Rodríguez-Viejoa Sensitive power compensated scanning calorimeter for analysis of phase transformations in small samples Rev. Sci. Instrum. 76 2005 065104
24. B. Yang, J.H. Perepezko, J.W.P. Schmelzer, Y. Gao, and C. Schick Dependence of crystal nucleation on prior liquid overheating by differential fast scanning calorimeter J. Chem. Phys. 140 2014 104513
25. B. Yang, A.S. Abyzov, E. Zhuravlev, Y. Gao, J.W.P. Schmelzer, and C. Schick Size and rate dependence of crystal nucleation in single tin drops by fast scanning calorimetry J. Chem. Phys. 138 2013 054501 054505
26. B. Yang, Y. Gao, C. Zou, Q. Zhai, A. Abyzov, E. Zhuravlev, J. Schmelzer, and C. Schick Cooling rate dependence of undercooling of pure Sn single drop by fast scanning calorimetry Appl. Phys. A: Mater. Sci. Process. 104 2011 189 196
27. B. Yang, Y.L. Gao, C.D. Zou, Q.J. Zhai, E. Zhuravlev, and C. Schick Repeated nucleation in an undercooled tin droplet by fast scanning calorimetry Mater. Lett. 63 2009 2476 2478
28. Y.L. Gao, E. Zhuravlev, C.D. Zou, B. Yang, Q.J. Zhai, and C. Schick Calorimetric measurements of undercooling in single micron sized SnAgCu particles in a wide range of cooling rates Thermochim. Acta 482 2009 1 7
29. E. Zhuravlev, A. Wurm, P. Pötschke, R. Androsch, J.W.P. Schmelzer, and C. Schick Kinetics of nucleation and crystallization of poly(ö-caprolactone)-multiwalled carbon nanotube composites Eur. Polym J. 52 2014 1 11
30. M. Mileva, R. Androsch, E. Zhuravlev, C. Schick, and B. Wunderlich Homogeneous nucleation and mesophase formation in glassy isotactic polypropylene Polymer 53 2012 277 282
31. E. Zhuravlev, J.W.P. Schmelzer, B. Wunderlich, and C. Schick Kinetics of nucleation and crystallization in poly(ε-caprolactone) (PCL) Polymer 52 2011 1983 1997
32. N. Bosq, N. Guigo, E. Zhuravlev, and N. Sbirrazzuoli Nonisothermal crystallization of polytetrafluoroethylene in a wide range of cooling rates J. Phys. Chem. B 117 2013 3407 3415
33. M.F.J. Pijpers, V.B.F. Mathot, B. Goderis, R. Scherrenberg, and E. van der Vegte High-speed calorimetry for the analysis of kinetics of vitrification, crystallization and melting of macromolecule Macromolecules 35 2002 3601 3613
34. E. Hellmuth, and B. Wunderlich Superheating of linear high-polymer polyethylene crystals J. Appl. Phys. 36 1965 3039 3044
35. A. Minakov, A. Wurm, and C. Schick Superheating in linear polymers studied by ultrafast nanocalorimetry Eur. Phys. J. E Soft Matter 23 2007 43 53
36. R.T. Tol, A.A. Minakov, S.A. Adamovsky, V.B.F. Mathot, and C. Schick Metastability of polymer crystallites formed at low temperature studied by ultrafast calorimetry: polyamide 6 confined in sub-micrometer droplets vs. bulk PA6 Polymer 47 2006 2172 2178
37. M. Pyda, E. Nowak-Pyda, J. Heeg, H. Huth, A.A. Minakov, M.L. Di Lorenzo, C. Schick, and B. Wunderlich Melting and crystallization of poly(butylene terephthalate) by temperature-modulated and superfast calorimetry J. Polym. Sci. B: Polym. Phys. 44 2006 1364 1377
38. A.A. Minakov, D.A. Mordvintsev, R. Tol, and C. Schick Melting and reorganization of the crystalline fraction and relaxation of the rigid amorphous fraction of isotactic polystyrene on fast heating (30,000 K/min) Thermochim. Acta 442 2006 25 30
39. -1; 5 ms) Faraday Discuss. 128 2005 261 270
40. A.A. Minakov, D.A. Mordvintsev, and C. Schick Melting and reorganization of poly(ethylene terephthalate) on fast heating (1,000 K/s) Polymer 45 2004 3755 3763
41. P. Cebe, X. Hu, D.L. Kaplan, E. Zhuravlev, A. Wurm, D. Arbeiter, and C. Schick Beating the heat-fast scanning melts silk beta sheet crystals Sci. Report 3 2013 1 7
42. D.W. Denlinger, E.N. Abarra, K. Allen, P.W. Rooney, M.T. Messer, S.K. Watson, and F. Hellman Thin-film microcalorimeter for heat-capacity measurements from 1.5-800 K Rev. Sci. Instrum. 65 1994 946 958
43. S. van Herwaarden, E. Iervolino, F. van Herwaarden, T. Wijffels, A. Leenaers, and V. Mathot Design, performance and analysis of thermal lag of the UFS1 twin-calorimeter chip for fast scanning calorimetry using the Mettler-Toledo Flash DSC 1 Thermochim. Acta 522 2011 46 52
44. http://www.xensor.nl.
45. E. Bich, J. Mlllat, and E. Vogel The viscosity and thermal conductivity of pure monatomic gases from their normal boiling point upto 5000 K in the limit of zero density and at 0. 101325 MPa J. Phys. Chem. Ref. Data 19 1990 1289 1305 DMI
46. D.R. Lide Handbook of Chemistry and Physics 79th ed. 1998 CRC Boca Raton, Boston: London, New York: Washington
47. M.T. Alam, M.P. Manoharan, M.A. Haque, C. Muratore, and A. Voevodin Influence of strain on thermal conductivity of silicon-nitride thin films J. Micromech. Microeng. 22 2012 045001
48. B.L. Zink, and F. Hellman Specific heat and thermal conductivity of low-stress amorphous Si-N membranes Solid State Commun. 129 2004 199 204
49. H. Ftouni, D. Tainoff, J. Richard, K. Lulla, J. Guidi, E. Collin, and O. Bourgeois Specific heat measurement of thin suspended Si-N membrane from 8 K to 300 K using the 3ω-Völklein method Rev. Sci. Instrum. 84 2013 094902
50. B. Revaz, B.L. Zink, D. O'Neil, L. Hull, and F. Hellman Numerical simulation of the heat transfer in amorphous silicon-nitride membrane-based microcalorimeters Rev. Sci. Instrum. 74 2003 4389 4403
51. B. Revaz, B.L. Zink, and F. Hellman Si-N membrane-based microcalorimetry: heat capacity and thermal conductivity of thin films Thermochim. Acta 432 2005 158 168
52. B.L. Zink, B. Revaz, J.J. Cherry, and F. Hellman Measurement of thermal conductivity of thin films with a Si-N membrane-based microcalorimeter Rev. Sci. Instrum. 76 2005 024901 024905
53. C. Baldasseroni, D.R. Queen, D.W. Cooke, K. Maize, A. Shakouri, and F. Hellman Heat transfer simulation and thermal measurements of microfabricated X-ray transparent heater stages Rev. Sci. Instrum. 82 2011 09390401 09390410
54. A.D. Polyanin Handbook of Linear Partial Differential Equations for Engineers Scientists 2002 CHAPMAN & HALL/CRC London, New York: Washington
55. H. Petersen The properties of helium: density, specific heats, viscosity, and thermal conductivity at pressures from 1 to 100 bar and from room temperature to about 1800 K, Danish Atomic Energy Commission RISO Rep. 224 1970 1 42