Fast scanning power compensated differential scanning nano-calorimeter: 1. The device

Thermochimica Acta

Volumn 505, Issue 1-2, 2010, Pages 1-13

  Zhuravlev, E ^a   Schick, C ^a  

^a UNIVERSITY OF ROSTOCK   (Germany)

Author keywords

Crystallization; Differential power compensation; Fast scanning nano calorimetry; Metals; Temperature calibration

Indexed keywords

FAST SCANNING; FAST SCANNING NANO-CALORIMETRY; POWER COMPENSATION; TEMPERATURE CALIBRATION;

CALIBRATION; CALORIMETERS; CALORIMETRY; CRYSTALLIZATION; ELECTRIC BATTERIES; METALS; NANOSENSORS; POLYMERS; SAMPLING; SILICON NITRIDE; SMELTING; SPECIFIC HEAT; TEMPERATURE; TEMPERATURE MEASUREMENT; TIN; TITANIUM COMPOUNDS; UNCERTAINTY ANALYSIS;

SCANNING;

EID: 77954243291     PISSN: 00406031     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tca.2010.03.019     Document Type: Article

References (55)

1. M.F.J. Pijpers, V.B.F. Mathot, B. Goderis, R. Scherrenberg, and E. van der Vegte High-speed calorimetry for the analysis of kinetics of vitrification, crystallization and melting of macromolecule Macromolecules 35 2002 3601 3613
2. PerkinElmer-Inc., Technical Specifications Thermal Analysis for the DSC 8000/8500 Differential Scanning Calorimeters http://las.perkinelmer.com/content/ RelatedMaterials/SpecificationSheets/SPC-8000and8500.pdf (2009).
3. N.E. Hager Thin heater calorimeter Rev. Sci. Instrum. 35 1964 618 624
4. L.H. Allen, G. Ramanath, S.L. Lai, Z. Ma, S. Lee, D.D.J. Allman, and K.P. Fuchs 1,000,000 °C/s thin film electrical heater: in situ resistivity measurements of Al and Ti/Si thin films during ultra rapid thermal annealing Appl. Phys. Lett. 64 1994 417 419
5. M.Y. Efremov, E.A. Olson, M. Zhang, F. Schiettekatte, Z. Zhang, and L.H. Allen Ultrasensitive, fast, thin-film differential scanning calorimeter Rev. Sci. Instrum. 75 2004 179 191
6. M. Chonde, M. Brindza, and V. Sadtchenkoa Glass transition in pure and doped amorphous solid water: an ultrafast microcalorimetry study J. Chem. Phys. 125 2006
7. E. León-Gutierrez, G. Garcia, M.T. Clavaguera-Mora, and J. Rodríguez-Viejo Glass transition in vapor deposited thin films of toluene Thermochim. Acta 492 2009 51 54
8. 2 thin film Thermochim. Acta 461 2007 82 87
9. S.A. Adamovsky, A.A. Minakov, and C. Schick Scanning microcalorimetry at high cooling rate Thermochim. Acta 403 2003 55 63
10. A.A. Minakov, S.A. Adamovsky, and C. Schick Non adiabatic thin-film (chip) nanocalorimetry Thermochim. Acta 432 2005 177 185
11. A.A. Minakov, and C. Schick Ultrafast thermal processing and nanocalorimetry at heating and cooling rates up to 1 MK/s Rev. Sci. Instrum. 78 2007 073902 073910
12. A.A. Minakov, A.W. van Herwaarden, W. Wien, A. Wurm, and C. Schick Advanced nonadiabatic ultrafast nanocalorimetry and superheating phenomenon in linear polymers Thermochim. Acta 461 2007 96 106
13. A.W. van Herwaarden Overview of calorimeter chips for various applications Thermochim. Acta 432 2005 192 201
14. A.A. Minakov, D.A. Mordvintsev, and C. Schick Melting and reorganization of poly(ethylene terephthalate) on fast heating (1000 K/s) Polymer 45 2004 3755 3763
15. -1; 5 ms) Faraday Discuss. 128 2005 261 270
16. A.A. Minakov, D.A. Mordvintsev, R. Tol, and C. Schick Melting and reorganization of the crystalline fraction and relaxation of the rigid amorphous fraction of isotactic polystyrene on fast heating (30,000 K/min) Thermochim. Acta 442 2006 25 30
17. A. Gradys, P. Sajkiewicz, A.A. Minakov, S. Adamovsky, C. Schick, T. Hashimoto, and K. Saijo Crystallization of polypropylene at various cooling rates Mater. Sci. Eng. A 413-414 2005 442 446
18. A. Gradys, P. Sajkiewicz, S. Adamovsky, A. Minakov, and C. Schick Crystallization of poly(vinylidene fluoride) during ultra-fast cooling Thermochim. Acta 461 2007 153 157
19. F. De Santis, S. Adamovsky, G. Titomanlio, and C. Schick Scanning nanocalorimetry at high cooling rate of isotactic polypropylene Macromolecules 39 2006 2562 2567
20. F. De Santis, S. Adamovsky, G. Titomanlio, and C. Schick Isothermal nanocalorimetry of isotactic polypropylene Macromolecules 40 2007 9026 9031
21. V.V. Ray, A.K. Banthia, and C. Schick Fast isothermal calorimetry of modified polypropylene clay nanocomposites Polymer 48 2007 2404 2414
22. A. Krumme, A. Lehtinen, S. Adamovsky, C. Schick, J. Roots, and A. Viikna Crystallization behavior of some unimodal and bimodal linear low-density polyethylenes at moderate and high supercooling J. Polym. Sci. Part B: Polym. Phys. 46 2008 1577 1588
23. C. Silvestre, S. Cimmino, D. Duraccio, and C. Schick Isothermal crystallization of isotactic poly(propylene) studied by superfast calorimetry Macromol. Rapid Commun. 28 2007 875 881
24. C. Schick Differential scanning calorimetry (DSC) of semicrystalline polymers Anal. Bioanal. Chem. 2009 1589 1611
25. M. Pyda, E. Nowak-Pyda, J. Heeg, H. Huth, A.A. Minakov, M.L. Di Lorenzo, C. Schick, and B. Wunderlich Melting and crystallization of poly(butylene terephthalate) by temperature-modulated and superfast calorimetry J. Polym. Sci., Part B: Polym. Phys. 44 2006 1364 1377
26. R.T. Tol, A.A. Minakov, S.A. Adamovsky, V.B.F. Mathot, and C. Schick Metastability of polymer crystallites formed at low temperature studied by Ultra fast calorimetry* Polyamide 6 confined in sub-micrometer droplets vs bulk PA6 Polymer 47 2006 2172 2178
27. A. Minakov, A. Wurm, and C. Schick Superheating in linear polymers studied by ultrafast nanocalorimetry Eur. Phys. J. E Soft Matter 23 2007 43 53
28. V. Brucato, S. Piccarolo, and V. La Carrubba An experimental methodology to study polymer crystallization under processing conditions. The influence of high cooling rates Chem. Eng. Sci. 57 2002 4129 4143
29. H. Janeschitz-Kriegl Crystallization Modalities in Polymer Melt Processing, Fundamental Aspects of Structure Formation 2010 Springer Wien, New York
30. W. Chen, D. Zhou, G. Xue, and C. Schick Chip calorimetry for fast cooling and thin films: a review Front. Chem. Chin. 4 2009 229 248
31. S. Adamovsky, and C. Schick Ultra-fast isothermal calorimetry using thin film sensors Thermochim. Acta 415 2004 1 7
32. M.Y. Efremov, E.A. Olson, M. Zhang, S.L. Lai, F. Schiettekatte, Z.S. Zhang, and L.H. Allen Thin-film differential scanning nanocalorimetry: heat capacity analysis Thermochim. Acta 412 2004 13 23
33. E. Zhuravlev, and C. Schick Fast scanning power compensated differential scanning nano-calorimeter: 2. Heat capacity analysis Thermochim. Acta this issue 505 2010 14 21
34. A. Minakov, J. Morikawa, T. Hashimoto, H. Huth, and C. Schick Temperature distribution in a thin-film chip utilized for advanced nanocalorimetry Meas. Sci. Technol. 17 2006 199 207
35. A.F. Lopeandia, J. Valenzuela, and J. Rodríguez-Viejo Power compensated thin film calorimetry at fast heating rates Sens. Actuators A: Phys. 143 2008 256 264
36. A.F. Lopeandia, L.l. Cerdo, M.T. Clavaguera-Mora, L.R. Arana, K.F. Jensen, F.J. Munoz, and J. Rodríguez-Viejo Sensitive power compensated scanning calorimeter for analysis of phase transformations in small samples Rev. Sci. Instrum. 76 2005 065104 065105
37. M. Merzlyakov Method of rapid (100,000 K/s) controlled cooling and heating of thin samples Thermochim. Acta 442 2006 52 60
38. M.J. O'Neill The analysis of a temperature-controlled scanning calorimeter Anal. Chem. 36 1964 1238 1245
39. M.J. O'Neill Measurement of specific heat functions by differential scanning calorimetry Anal. Chem. 38 1966 1331 1336
40. E.S. Watson, M.O. O'Neill, J. Justin, and N. Brenner A differential scanning calorimeter for quantitative differential thermal analysis Anal. Chem. 36 1964 1233 1238
41. E.S. Watson, and M.J. O'Neill Differential Microcalorimeter 1966 The Perskin-Elmer Corporation Norwalk, CN
42. E. Zhuravlev, C. Schick, Patent pending, USA, 2009.
43. Meilhaus ADC/DAC board, 2009. http://www.meilhaus.de/fileadmin/upload/ download/products/manuals/ME-4600%202.0E.pdf.
44. SRS Small Instrumentation Module, 2009. http://www.thinksrs.com/products/ SIM.htm.
45. A.A. Minakov, S.A. Adamovsky, and C. Schick Advanced two-channel AC calorimeter for simultaneous measurements of complex heat capacity and complex thermal conductivity Thermochim. Acta 403 2003 89 103
46. H. Huth, A. Minakov, and C. Schick High sensitive differential AC-chip calorimeter for nanogram samples Netsu Sokutei 32 2005 70 76
47. V.A. Drebushchak Universality of the emf of thermocouples Thermochim. Acta 496 2009 50 53
48. Y.L. Gao, E. Zhuravlev, C.D. Zou, B. Yang, Q.J. Zhai, and C. Schick Calorimetric measurements of undercooling in single micron sized SnAgCu particles in a wide range of cooling rates Thermochim. Acta 482 2009 1 7
49. G.W.H. Hohne, H.K. Cammenga, W. Eysel, E. Gmelin, and W. Hemminger The temperature calibration of scanning calorimeters Thermochim. Acta 160 1990 1 12
50. S.M. Sarge, W. Hemminger, E. Gmelin, G.W.H. Hohne, H.K. Cammenga, and W. Eysel Metrologically based procedures for the temperature, heat and heat flow rate calibration of DSC J. Therm. Anal. 49 1997 1125 1134
51. G. YuLai, Z. ChangDong, Y. Bin, and Z. QiJie Fast calorimetric scanning of micro-sized SnAgCu single droplet at a high cooling rate Sci. China Ser. E-Technol. Sci. 52 2009 1707 1711
52. B. Yang, Y.L. Gao, C.D. Zou, Q.J. Zhai, E. Zhuravlev, and C. Schick Repeated nucleation in an undercooled tin droplet by fast scanning calorimetry Mater. Lett. 63 2009 2476 2478
53. S. Neuenfeld, and C. Schick Verifying the symmetry of differential scanning calorimeters concerning heating and cooling using liquid crystal secondary temperature standards Thermochim. Acta 446 2006 55 65
54. S.M. Sarge, G.W.H. Hohne, H.K. Cammenga, W. Eysel, and E. Gmelin Temperature, heat and heat flow rate calibration of scanning calorimeters in the cooling mode Thermochim. Acta 361 2000 1 20
55. C. Schick, U. Jonsson, T. Vassilev, A. Minakov, J. Schawe, R. Scherrenberg, and D. Lörinczy Applicability of 8OCB for temperature calibration of temperature modulated calorimeters Thermochim. Acta 347 2000 53 61