Analytical methods for pesticide residues

Water Environment Research

Volumn 84, Issue 10, 2012, Pages 1979-2000

  Liang, H C ^a   Hay, Michael T ^b   Drake Meneghetti, Abbey M ^a  

^a TETRA TECH INC   (United States)

^b Penn State Beaver ^*  (United States)

Author keywords

Analytical chemistry; Analytical methods; Fluorescence; GC; Immunoassays; LC; MS; Organochlorine; Organophosphate; Organophosphorus; Pesticide residues; Pesticides

Indexed keywords

CHEMICAL ANALYSIS; FLUORESCENCE; MASS SPECTROMETRY;

ANALYTICAL METHOD; IMMUNOASSAYS; ORGANOCHLORINES; ORGANOPHOSPHATE; ORGANOPHOSPHORUS; PESTICIDE RESIDUE;

PESTICIDES;

DIMETHOATE; ETHION; ORGANOCHLORINE DERIVATIVE; ORGANOPHOSPHATE; ORGANOPHOSPHORUS COMPOUND; PARATHION METHYL; PERMETHRIN; PESTICIDE; PESTICIDE RESIDUE;

ANALYTICAL METHOD; BIOASSAY; EXTRACTION; FLUORESCENCE; GAS CHROMATOGRAPHY; LITERATURE REVIEW; MASS SPECTROMETRY; ORGANOCHLORINE; ORGANOPHOSPHATE; PESTICIDE;

ANALYTIC METHOD; ATMOSPHERIC PRESSURE; BIOCHEMICAL COMPOSITION; CHEMISTRY; CONTROLLED STUDY; ELECTRON CAPTURE DETECTION; ELECTROSPRAY; ENVIRONMENTAL PROTECTION; ENZYME LINKED IMMUNOSORBENT ASSAY; EXTRACTION; FLUORESCENCE; GAS CHROMATOGRAPHY; GEL PERMEATION CHROMATOGRAPHY; HOLLOW FIBER; HYDROPHILICITY; IMMUNOASSAY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; LIQUID PHASE MICROEXTRACTION; MASS FRAGMENTOGRAPHY; MASS SPECTROMETRY; PRIORITY JOURNAL; PUBLICATION; REVIEW; SAMPLE; SOLID PHASE EXTRACTION; SOLID PHASE MICROEXTRACTION; SOLVENT EXTRACTION; SPECTROPHOTOMETRY; TANDEM MASS SPECTROMETRY;

EID: 84886734624     PISSN: 10614303     EISSN: 15547531     Source Type: Journal    
DOI: 10.2175/106143012X13407275695959     Document Type: Review

References (106)

1. Acosta-Tejada, G. M.; Medina-Peralta, S.; Moguel-Ordonez, Y. B.; Munoz-Rodriguez, D. (2011) Matrix Solid-Phase Dispersion Extraction of Organophosphorus Pesticides from Propolis Extracts and Recovery Evaluation by GC/MS. Anal. Bioanal. Chem., 400 (3), 885-891.
2. Aguilera-Luiz, M. M.; Plaza-Bolanos, P.; Romero-Gonzalez, R.; Vidal, J. L. M.; Frenich, A. G. (2011) Comparison of the Efficiency of Different Extraction Methods for the Simultaneous Determination of Mycotoxins and Pesticides in Milk Samples by Ultra High-Performance Liquid Chromatography- Tandem Mass Spectrometry. Anal. Bioanal. Chem., 399 (8), 2863-2875.
3. Alves, A. C. H.; Pontes, M. M.; Goncalves, B.; Bernardo, M. M. S.; Mendes, B. S. (2011) Validated Dispersive Liquid-Liquid Microextraction for Analysis of Organophosphorous Pesticides in Water. J. Sep. Sci., 34 (11), 1326-1332.
4. Amendola, G.; Pelosi, P.; Dommarco, R. (2011) Solid-Phase Extraction for Multi-Residue Analysis of Pesticides in Honey. J. Environ. Sci. Health Part B-Pestic. Contam. Agric. Wastes, 46 (1), 24-34.
5. An, E. M.; Shin, H. S. (2011a) Analytical Methods for the Determination of Pesticide Residues Using Gas Chromatography with Nitrogen-Phosphorus Detector. Food Sci. Biotechnol., 20 (2), 395-401.
6. An, E. M.; Shin, H. S. (2011b) Gas Chromatographic Determination of Pesticide Residues Using Electron-Capture Detector and Mass Spectrometry. Food Sci. Biotechnol., 20 (5), 1299-1306.
7. Andrade, G.; Freguglia, R. M. O.; Furlani, R. P. Z.; Torres, N. H.; Tornisielo, V. L. (2011) Determination of Pesticide Residues in Tomato Using Dispersive Solid-Phase Extraction and Gas Chromatography/Ion Trap Mass Spectrometry. J. Braz. Chem. Soc., 22 (9), 1701-1708.
8. Asensio-Ramos, M.; D'Orazio, G.; Hernandez-Borges, J.; Rocco, A.; Fanali, S. (2011) Multi-Walled Carbon Nanotubes-Dispersive Solid-Phase Extraction Combined with Nano-Liquid Chromatography for the Analysis of Pesticides in Water Samples. Anal. Bioanal. Chem., 400 (4), 1113-1123.
9. Aslan, N. (2011) Analysis of Pesticide Residues in Cherries from Afyonkarahisar, Turkey. Fresenius Environ. Bull., 20 (8), 2002-2006.
10. Barletta, J. Y.; Gomes, P.; dos Santos-Neto, A. J.; Lancas, F. M. (2011) Development of a New Stir Bar Sorptive Extraction Coating and Its Application for the Determination of Six Pesticides in Sugarcane Juice. J. Sep. Sci., 34 (11), 1317-1325.
11. Bidari, A.; Ganjali, M. R.; Norouzi, P.; Hosseini, M. R. M.; Assadi, Y. (2011) Sample Preparation Method for the Analysis of Some Organophosphorus Pesticides Residues in Tomato by Ultrasound-Assisted Solvent Extraction Followed by Dispersive Liquid-Liquid Microextraction. Food Chem., 126 (4), 1840-1844.
12. Brondi, S. H. G.; de Macedo, A. N.; Vicente, G. H. L.; Nogueira, A. R. A. (2011) Evaluation of the QuEChERS Method and Gas Chromatography-Mass Spectrometry for the Analysis Pesticide Residues in Water and Sediment. Bull. Environ. Contam. Toxicol., 86 (1), 18-22.
13. Brown, A. N.; Cook, J. M.; Hammack, W. T.; Stepp, J. S.; Pelt, J. V.; Gerard, G. (2011) Analysis of Pesticides Residues in Fresh Produce Using Buffered Acetonitrile Extraction and Aminopropyl Cleanup with Gas Chromatography/Triple Quadrupole Mass Spectrometry, Liquid Chromatography/Triple Quadrupole Mass Spectrometry, Gas Chromatography/Ion Trap Detector Mass Spectrometry, and GC with a Halogen-Specific Detector. J. AOAC Int., 94 (3), 931-941.
14. Cahill, M. G.; Caprioli, G.; Stack, M.; Vittori, S.; James, K. J. (2011) Semi-Automated Liquid Chromatography-Mass Spectrometry (LC-MS/MS) Method for Basic Pesticides in Wastewater Effluents. Anal. Bioanal. Chem., 400 (2), 587-594.
15. Caldas, S. S.; Bolzan, C. M.; Cerqueira, M. B.; Tomasini, D.; Furlong, E. B.; Fagundes, C.; Primel, E. G. (2011) Evaluation of a Modified QuEChERS Extraction of Multiple Classes of Pesticides from a Rice Paddy Soil by LC-APCI-MS/MS. J. Agric. Food Chem., 59 (22), 11918-11926.
16. Caldas, S. S.; Goncalves, F. F.; Primel, E. G.; Prestes, O. D.; Martins, M. L.; Zanella, R. (2011) Modern Techniques of Sample Preparation for Pesticide Residues Determination in Water by Liquid Chromatography with Detection by Diode Array and Mass Spectrometry. Quim. Nova, 34 (9), 1604-1617.
17. Camino-Sanchez, F. J.; Zafra-Gomez, A.; Ruiz-Garcia, J.; Bermudez-Peinado, R.; Ballesteros, O.; Navalon, A.; Vilchez, J. L. (2011) UNE-ENn ISO/IEC 17025:2005 Accredited Method for the Determination of 121 Pesticide Residues in Fruits and Vegetables by Gas Chromatography-Tandem Mass Spectrometry. J. Food Compos. Anal., 24 (3), 427-440.
18. Cappiello, A.; Pierini, E.; Palma, P. (2011) An SPE Method for the Concurrent Extraction of Organochlorine and Phenoxy Acidic Pesticides in River Water. Chromatographia, 73 (7-8), 691-699.
19. Castillo, M.; Gonzalez, C.; Miralles, A. (2011) An Evaluation Method for Determination of Non-Polar Pesticide Residues in Animal Fat Samples by Using Dispersive Solid-Phase Extraction Clean-Up and GC-MS. Anal. Bioanal. Chem., 400 (5), 1315-1328.
20. Chen, G. Q.; Cao, P. Y.; Liu, R. J. (2011) A Multi-Residue Method for Fast Determination of Pesticides in Tea by Ultra Performance Liquid Chromatography-Electrospray Tandem Mass Spectrometry Combined with Modified QuEChERS Sample Preparation Procedure. Food Chem., 125 (4), 1406-1411.
21. Chung, S. W. C.; Chen, B. L. S. (2011) Determination of Organochlorine Pesticide Residues in Fatty Foods: A Critical Review on the Analytical Methods and Their Testing Capabilities. J. Chromatogr. A, 1218 (33), 5555-5567.
22. Cieslik, E.; Sadowska-Rociek, A.; Ruiz, J. M. M.; Surma-Zadora, M. (2011) Evaluation of QuEChERS Method for the Determination of Organochlorine Pesticide Residues in Selected Groups of Fruits. Food Chem., 125 (2), 773-778.
23. Dai, R. H.; Ren, X. D.; He, X.; Huo, Y. S. (2011) Convenient Analytical Method for Quantitative Determination of 23 Pesticide Residues in Herbs by Gas Chromatography-Mass Spectrometry. Bull. Environ. Contam. Toxicol., 86 (6), 559-564.
24. Dasgupta, S.; Banerjee, K.; Dhumal, K. N.; Adsule, P. G. (2011) Optimization of Detection Conditions and Single-Laboratory Validation of a Multiresidue Method for the Determination of 135 Pesticides and 25 Organic Pollutants in Grapes and Wine by Gas Chromatography Time-of-Flight Mass Spectrometry. J. AOAC Int., 94 (1), 273-285.
25. Dasgupta, S.; Banerjee, K.; Utture, S.; Kusari, P.; Wagh, S.; Dhumal, K.; Kolekar, S.; Adsule, P. G. (2011) Extraction of Pesticides, Dioxin-Like PCBs and PAHs in Water Based Commodities Using Liquid-Liquid Microextraction and Analysis by Gas Chromatography-Mass Spectrometry. J. Chromatogr. A, 1218 (38), 6780-6791.
26. Dong, J.; Pan, Y. X.; Lv, J. X.; Sun, J.; Gong, X. M.; Li, K. (2011) Multiresidue Method for the Determination of Pesticides in Fruits and Vegetables Using Gas Chromatography-Negative Chemical Ionization-Triple Quadrupole Tandem Mass Spectrometry. Chromatographia, 74 (1-2), 109-119.
27. Ebrahimi, M.; Es'haghi, Z.; Samadi, F.; Hosseini, M. S. (2011) Ionic Liquid Mediated Sol-Gel Sorbents for Hollow Fiber Solid-Phase Microextraction of Pesticide Residues in Water and Hair Samples. J. Chromatogr. A, 1218 (46), 8313-8321.
28. Edison, S. E.; Lin, L. A.; Gamble, B. M.; Wong, J.; Zhang, K. (2011) Surface Swabbing Technique for the Rapid Screening for Pesticides Using Ambient Pressure Desorption Ionization with High-Resolution Mass Spectrometry. Rapid Commun. Mass Spectrom., 25 (1), 127-139.
29. Edison, S. E.; Lin, L. A.; Parrales, L. (2011) Practical Considerations for the Rapid Screening for Pesticides Using Ambient Pressure Desorption Ionisation with High-Resolution Mass Spectrometry. Food Addit. Contam. Part A-Chem., 28 (10), 1393-1404.
30. Fernandes, V. C.; Domingues, V. F.; Mateus, N.; Delerue-Matos, C. (2011) Organochlorine Pesticide Residues in Strawberries from Integrated Pest Management and Organic Farming. J. Agric. Food Chem., 59 (14), 7582-7591.
31. Ferrer, C.; Martinez-Bueno, M. J.; Lozano, A.; Fernandez-Alba, A. R. (2011) Pesticide Residue Analysis of Fruit Juices by LC-MS/MS Direct Injection. One Year Pilot Survey. Talanta, 83 (5), 1552-1561.
32. Filho, A. M.; dos Santos, F. N.; Pereira, P. A. D. (2011) Multi-Residue Analysis of Pesticide Residues in Mangoes Using Solid-Phase Microextraction Coupled to Liquid Chromatography and UV-Vis Detection. J. Sep. Sci., 34 (21), 2960-2966.
33. Fillatre, Y.; Rondeau, D.; Bonnet, B.; Daguin, A.; Jadas-Hecart, A.; Communal, P. Y. (2011) Multiresidue Analysis of Multiclass Pesticides in Lavandin Essential Oil by LC/MS/MS Using the Scheduled Selected Reaction Monitoring Mode. Anal. Chem., 83 (1), 109-117.
34. Frenich, A. G.; Romero-Gonzalez, R.; Vidal, J. L. M.; Ocana, R. M.; Feria, P. B. (2011) Comparison of Solid Phase Microextraction and Hollow Fiber Liquid Phase Microextraction for the Determination of Pesticides in Aqueous Samples by Gas Chromatography Triple Quadrupole Tandem Mass Spectrometry. Anal. Bioanal. Chem., 399 (6), 2043-2059.
35. Furlani, R. P. Z.; Marcilio, K. M.; Leme, F. M.; Tfouni, S. A. V. (2011) Analysis of Pesticide Residues in Sugarcane Juice Using QuEChERS Sample Preparation and Gas Chromatography with Electron Capture Detection. Food Chem., 126 (3), 1283-1287.
36. Georgakopoulos, P.; Zachari, R.; Mataragas, M.; Athanasopoulos, P.; Drosinos, E. H.; Skandamis, P. N. (2011) Optimisation of Octadecyl (C(18)) Sorbent Amount in QuEChERS Analytical Method for the Accurate Organophosphorus Pesticide Residues Determination in Low-Fatty Baby Foods with Response Surface Methodology. Food Chem., 128 (2), 536-542.
37. Guan, S. X.; Yu, Z. G.; Yu, H. N.; Song, C. H.; Song, Z. Q.; Qin, Z. (2011) Multi-Walled Carbon Nanotubes as Matrix Solid-Phase Dispersion Extraction Adsorbent for Simultaneous Analysis of Residues of Nine Organophosphorus Pesticides in Fruit and Vegetables by Rapid Resolution LC-MS-MS. Chromatographia, 73 (1-2), 33-41.
38. Hu, Y. Y.; Xu, Y. P.; Yao, J.; Han, F.; Zheng, P.; Sheng, X. (2011) On-Column Injection Coupled with Gas Chromatography/Mass Spectrometry for Determination of Thermoliable Carbamates Pesticides in Animal Derived Sample. Chin. J. Anal. Chem., 39 (3), 330-334.
39. Jiang, J.; Li, P. W.; Xie, L. H.; Ding, X. X.; Li, Y.; Wang, X. P.; Wang, X. F.; Zhang, Q.; Guan, D. (2011) Rapid Screening and Simultaneous Confirmation of 64 Pesticide Residues in Vegetable Using Solid Phase Extraction- Comprehensive Two-Dimensional Gas Chromatography Coupled with Time-of-Flight Mass Spectrometer. Chin. J. Anal. Chem., 39 (1), 72-76.
40. Kittlaus, S.; Schimanke, J.; Kempe, G.; Speer, K. (2011) Assessment of Sample Cleanup and Matrix Effects in the Pesticide Residue Analysis of Foods Using Postcolumn Infusion in Liquid Chromatography-Tandem Mass Spectrometry. J. Chromatogr. A, 1218 (46), 8399-8410.
41. Kmellar, B.; Pareja, L.; Ferrer, C.; Fodor, P.; Fernandez-Alba, A. R. (2011) Study of the Effects of Operational Parameters on Multiresidue Pesticide Analysis by LC-MS/MS. Talanta, 84 (2), 262-273.
42. Kobayashi, M.; Otsuka, K.; Tamura, Y.; Tomizawa, S.; Kamijo, K.; Iwakoshi, K.; Sato, C.; Nagayama, T.; Takano, I. (2011) Study on Rapid Analysis Method of Pesticide Contamination in Processed Foods by GC-MS and GC-FPD. Food Hyg. Saf. Sci., 52 (4), 226-236.
43. Koc, F.; Karakus, E. (2011) Determination of Organochlorinated Pesticide Residues by Gas Chromatography - Mass Spectrometry after Elution in a Florisil Column. Kafkas Univ. Vet. Fak. Derg., 17 (1), 65-70.
44. Koesukwiwat, U.; Lehotay, S. J.; Leepipatpiboon, N. (2011) Fast, Low-Pressure Gas Chromatography Triple Quadrupole Tandem Mass Spectrometry for Analysis of 150 Pesticide Residues in Fruits and Vegetables. J. Chromatogr. A, 1218 (39), 7039-7050.
45. Kolberg, D. I.; Prestes, O. D.; Adaime, M. B.; Zanella, R. (2011) Development of a Fast Multiresidue Method for the Determination of Pesticides in Dry Samples (Wheat Grains, Flour and Bran) Using QuEChERS Based Method and GC-MS. Food Chem., 125 (4), 1436-1442.
46. Kruve, A.; Haapala, M.; Saarela, V.; Franssila, S.; Kostiainen, R.; Kotiaho, T.; Ketola, R. A. (2011) Feasibility of Capillary Liquid Chromatography-Microchip-Atmospheric Pressure Photoionization-Mass Spectrometry for Pesticide Analysis in Tomato. Anal. Chim. Acta, 696 (1-2), 77-83.
47. Kruve, A.; Herodes, K.; Leito, I. (2011) Accounting for Matrix Effects of Pesticide Residue Liquid Chromatography/Electrospray Ionisation Mass Spectrometric Determination by Treatment of Background Mass Spectra with Chemometric Tools. Rapid Commun. Mass Spectrom., 25 (9), 1159-1168.
48. Kujawski, M. W.; Namiesnik, J. (2011) Levels of 13 Multi-Class Pesticide Residues in Polish Honeys Determined by LC-ESI-MS/MS. Food Control, 22 (6), 914-919.
49. Lazartigues, A.; Fratta, C.; Baudot, R.; Wiest, L.; Feidt, C.; Thomas, M.; Cren-Olive, C. (2011) Multiresidue Method for the Determination of 13 Pesticides in Three Environmental Matrices: Water, Sediments and Fish Muscle. Talanta, 85 (3), 1500-1507.
50. Lazartigues, A.; Wiest, L.; Baudot, R.; Thomas, M.; Feidt, C.; Cren-Olive, C. (2011) Multiresidue Method to Quantify Pesticides in Fish Muscle by QuEChERS-Based Extraction and LC-MS/MS. Anal. Bioanal. Chem., 400 (7), 2185-2193.
51. Lee, S. W.; Choi, J. H.; Cho, S. K.; Yu, H. A.; Abd El-Aty, A. M.; Shim, J. H. (2011) Development of a New QuEChERS Method Based on Dry Ice for the Determination of 168 Pesticides in Paprika Using Tandem Mass Spectrometry. J. Chromatogr. A, 1218 (28), 4366-4377.
52. Li, J.; Zhang, H. F.; Shi, Y. P. (2011) Monitoring Multi-Class Pesticide Residues in Fresh Grape by Hollow Fibre Sorptive Extraction Combined with Gas Chromatography-Mass Spectrometry. Food Chem., 127 (2), 784-790.
53. Liang, H. C.; Hay, M. T. (2011) Analytical Methods for Pesticides and Herbicides. Water Environ. Res., 83 (10), 956-982.
54. Lin, X. Y.; Chen, X. H.; Huo, X.; Yu, Z. G.; Bi, K. S.; Li, Q. (2011) Dispersive Liquid-Liquid Microextraction Coupled with High-Performance Liquid Chromatography-Diode Array Detection for the Determination of N-Methyl Carbamate Pesticides in Vegetables. J. Sep. Sci., 34 (2), 202-209.
55. 4 Nanoparticle Aggregates as Color Reagents. Anal. Chem., 83 (17), 6778-6784.
56. Liu, D.; Qian, C. F.; Wang, Y. H. (2011) Determination of Organophosphorus Pesticides in Rice by TLC. Asian J. Chem., 23 (5), 2011-2013.
57. Liu, G. Z.; Rong, L.; Guo, B.; Zhang, M. S.; Li, S. J.; Wu, Q.; Chen, J. T.; Chen, B.; Yao, S. Z. (2011) Development of an Improved Method to Extract Pesticide Residues in Foods Using Acetontrile with Magnesium Sulfate and Chloroform. J. Chromatogr. A, 1218 (11), 1429-1436.
58. Martins, J.; Esteves, C.; Simoes, T.; Correia, M.; Delerue-Matos, C. (2011) Determination of 24 Pesticide Residues in Fortified Wines by Solid-Phase Microextraction and Gas Chromatography-Tandem Mass Spectrometry. J. Agric. Food Chem., 59 (13), 6847-6855.
59. Mbaye, M.; Seye, M. D. G.; Aaron, J. J.; Coly, A.; Tine, A. (2011) Application of Flow Injection Analysis-Photo-Induced Fluorescence (FIA-PIF) for the Determination of Alpha-Cypermethrin Pesticide Residues in Natural Waters. Anal. Bioanal. Chem., 400 (2), 403-410.
60. Miyake, S. (2011) Preparation of Monoclonal Antibody for Pesticide and Mycotoxin and Its Application to Food Analysis. Bunseki Kagaku, 60 (5), 389-398.
61. Ng, C. I.; Zhang, X. M. (2011) A Quick Analytical Method Using Direct Solid Sample Introduction and GC-ECD for Pesticide Residues Analysis in Crops. Talanta, 85 (4), 1766-1771.
62. Niell, S.; Pareja, L.; Gonzalez, G.; Gonzalez, J.; Vryzas, Z.; Cesio, M. V.; Papadopoulou-Mourkidou, E.; Heinzen, H. (2011) Simple Determination of 40 Organophosphate Pesticides in Raw Wool Using Microwave-Assisted Extraction and GC-FPD Analysis. J. Agric. Food Chem., 59 (14), 7601-7608.
63. Oellig, C.; Schwack, W. (2011) Planar Solid Phase Extraction-a New Clean-up Concept in Multi-Residue Analysis of Pesticides by Liquid Chromatography-Mass Spectrometry. J. Chromatogr. A, 1218 (37), 6540-6547.
64. Pareja, L.; Cesio, V.; Heinzen, H.; Fernandez-Alba, A. R. (2011) Evaluation of Various QuEChERS Based Methods for the Analysis of Herbicides and Other Commonly Used Pesticides in Polished Rice by LC-MS/MS. Talanta, 83 (5), 1613-1622.
65. Pareja, L.; Fernandez-Alba, A. R.; Cesio, V.; Heinzen, H. (2011) Analytical Methods for Pesticide Residues in Rice. Trac-Trends Anal. Chem., 30 (2), 270-291.
66. Park, J. H.; Mamun, M. I.; Abd El-Aty, A. M.; Na, T. W.; Choi, J. H.; Ghafar, M. W.; Choi, W. J.; Kim, K. S.; Kim, S. D.; Shim, J. H. (2011a) Simultaneous Multiresidue Determination of 48 Pesticides in Yeongsan and Sumjin River Water Using GC-NPD and Confirmation Via GC-MS. Biomed. Chromatogr., 25 (1-2), 155-163.
67. Park, J. H.; Mamun, M. I.; Abd El-Aty, A. M.; Na, T. W.; Choi, J. H.; Ghafar, M. W.; Kim, K. S.; Kim, S. D.; Shim, J. H. (2011b) Development and Validation of a Multiresidue Method for Determination of 37 Pesticides in Soil Using GC-NPD. Biomed. Chromatogr., 25 (9), 1003-1009.
68. Park, J. Y.; Choi, J. H.; Abd El-Aty, A. M.; Kim, B. M.; Oh, J. H.; Do, J. A.; Kwon, K. S.; Shim, K. H.; Choi, O. J.; Shin, S. C.; Shim, J. H. (2011) Simultaneous Multiresidue Analysis of 41 Pesticide Residues in Cooked Foodstuff Using QuEChERS: Comparison with Classical Method. Food Chem., 128 (1), 241-253.
69. Pinheiro, A. D.; da Rocha, G. O.; de Andrade, J. B. (2011) A SDME/GC-MS Methodology for Determination of Organophosphate and Pyrethroid Pesticides in Water. Microchem J., 99 (2), 303-308.
70. Robles-Molina, J.; Gilbert-Lopez, B.; Garcia-Reyes, J. F.; Martos, N. R.; Molina-Diaz, A. (2011) Multiclass Determination of Pesticides and Priority Organic Pollutants in Fruit-Based Soft Drinks by Headspace Solid-Phase Microextraction/Gas Chromatography Tandem Mass Spectrometry. Anal. Methods, 3 (10), 2221-2230.
71. Rodrigues, F. D.; Mesquita, P. R. R.; de Oliveira, L. S.; de Oliveira, F. S.; Menezes, A.; Pereira, P. A. D.; de Andrade, J. B. (2011) Development of a Headspace Solid-Phase Microextraction/Gas Chromatography-Mass Spectrometry Method for Determination of Organophosphorus Pesticide Residues in Cow Milk. Microchem J., 98 (1), 56-61.
72. Rodrigues, S. A.; Caldas, S. S.; Furlong, E. B.; Primel, E. G.; Zanella, R. (2011) Optimization and Validation of a Method Using Modified QuEChERS and LC-ESI-MS/MS for the Determination of Pesticides in Onion. Quim. Nova, 34 (5), 780-U62.
73. Romero-Gonzalez, R.; Frenich, A. G.; Vidal, J. L. M.; Prestes, O. D.; Grio, S. L. (2011) Simultaneous Determination of Pesticides, Biopesticides and Mycotoxins in Organic Products Applying a Quick, Easy, Cheap, Effective, Rugged and Safe Extraction Procedure and Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry. J. Chromatogr. A, 1218 (11), 1477-1485.
74. Sack, C.; Smoker, M.; Chamkasem, N.; Thompson, R.; Satterfield, G.; Masse, C.; Mercer, G.; Neuhaus, B.; Cassias, I.; Chang, E.; Lin, Y.; MacMahon, S.; Wong, J.; Zhang, K.; Smith, R. E. (2011) Collaborative Validation of the QuEChERS Procedure for the Determination of Pesticides in Food by LC-MS/MS. J. Agric. Food Chem., 59 (12), 6383-6411.
75. Sanyal, D.; Rani, A.; Alam, S.; Gujral, S.; Gupta, R. (2011) Development, Validation, and Uncertainty Measurement of Multi-Residue Analysis of Organochlorine and Organophosphorus Pesticides Using Pressurized Liquid Extraction and Dispersive-SPE Techniques. Environ. Monit. Assess., 182 (1- 4), 97-113.
76. Satpathy, G.; Tyagi, Y. K.; Gupta, R. K. (2011) A Novel Optimised and Validated Method for Analysis of Multi-Residues of Pesticides in Fruits and Vegetables by Microwave-Assisted Extraction (MAE)-Dispersive Solid-Phase Extraction (D-SPE)-Retention Time Locked (RTL)-Gas Chromatography-Mass Spectrometry with Deconvolution Reporting Software (DRS). Food Chem., 127 (3), 1300-1308.
77. Seebunrueng, K.; Santaladchaiyakit, Y.; Soisungnoen, P.; Srijaranai, S. (2011) Catanionic Surfactant Ambient Cloud Point Extraction and High-Performance Liquid Chromatography for Simultaneous Analysis of Organophosphorus Pesticide Residues in Water and Fruit Juice Samples. Anal. Bioanal. Chem., 401 (5), 1703-1712.
78. Seiber, J. N.; Kleinschmidt, L. A. (2011) Contributions of Pesticide Residue Chemistry to Improving Food and Environmental Safety: Past and Present Accomplishments and Future Challenges. J. Agric. Food Chem., 59 (14), 7536-7543.
79. Shi, Y.; Chang, J. S.; Esposito, C. L.; Lafontaine, C.; Berube, M. J.; Fink, J. A.; Espourteille, F. A. (2011) Rapid Screening for Pesticides Using Automated Online Sample Preparation with a High-Resolution Benchtop Orbitrap Mass Spectrometer. Food Addit. Contam. Part A-Chem., 28 (10), 1383-1392.
80. Silva, C. F.; Emidio, E. S.; Dorea, H. S. (2011) Solid-Phase Microextraction for Determination of Anilino-Pyrimidine, Dimethylcarbamate and Thiadiazine Pesticides in Irrigation Project Surface Water. J. Braz. Chem. Soc., 22 (7), 1371-1378.
81. Sinha, S. N.; Bhatnagar, V. K.; Doctor, P.; Toteja, G. S.; Agnihotri, N. P.; Kalra, R. L. (2011) A Novel Method for Pesticide Analysis in Refined Sugar Samples Using a Gas Chromatography-Mass Spectrometer (GC-MS/MS) and Simple Solvent Extraction Method. Food Chem., 126 (1), 379-386.
82. Stocka, J.; Tankiewicz, M.; Biziuk, M.; Namiesnik, J. (2011) Green Aspects of Techniques for the Determination of Currently Used Pesticides in Environmental Samples. Int. J. Mol. Sci., 12 (11), 7785-7805.
83. Sun, X. J.; Zhu, F.; Xi, J. B.; Lu, T. B.; Liu, H.; Tong, Y. X.; Ouyang, G. F. (2011) Hollow Fiber Liquid-Phase Microextraction as Clean-Up Step for the Determination of Organophosphorus Pesticides Residues in Fish Tissue by Gas Chromatography Coupled with Mass Spectrometry. Mar. Pollut. Bull., 63 (5-12), 102-107.
84. Tsiropoulos, N. G.; Amvrazi, E. G. (2011) Determination of Pesticide Residues in Honey by Single-Drop Microextraction and Gas Chromatography. J. AOAC Int., 94 (2), 634-644.
85. Uddin, R.; Iqbal, S.; Khan, M. F.; Parveen, Z.; Ahmed, M.; Abbas, M. (2011) Determination of Pesticide Residues in Rice Grain by Solvent Extraction, Column Cleanup, and Gas Chromatography-Electron Capture Detection. Bull. Environ. Contam. Toxicol., 86 (1), 83-89.
86. Valencia, T. M. G.; de Llasera, M. P. G. (2011) Determination of Organophosphorus Pesticides in Bovine Tissue by an on-Line Coupled Matrix Solid-Phase Dispersion-Solid Phase Extraction-High Performance Liquid Chromatography with Diode Array Detection Method. J. Chromatogr. A, 1218 (39), 6869-6877.
87. Walorczyk, S.; Drozdzynski, D.; Gnusowski, B. (2011) Multiresidue Determination of 160 Pesticides in Wines Employing Mixed-Mode Dispersive-Solid Phase Extraction and Gas Chromatography-Tandem Mass Spectrometry. Talanta, 85 (4), 1856-1870.
88. Wang, Y.; Jin, H. Y.; Ma, S. C.; Lu, J.; Lin, R. C. (2011) Determination of 195 Pesticide Residues in Chinese Herbs by Gas Chromatography-Mass Spectrometry Using Analyte Protectants. J. Chromatogr. A, 1218 (2), 334-342.
89. Wang, Y.; Liu, S. B.; Xie, C. M.; Zhang, H. X.; Lu, W. H. (2011) Determination of Organophosphate Pesticide Residues in Salt Fish Using Accelerated Solvent Extraction and Gel Permeation Chromatography/Solid Phase Extraction with Gas Chromatography-Mass Spectrometry. Chin. J. Anal. Chem., 39 (1), 67-71.
90. Wang, Y. Q.; Wang, Z. M.; Zhang, H. H.; Shi, Y. H.; Ren, R. B.; Zhang, H. Q.; Yu, Y. (2011) Application of Pneumatic Nebulization Single-Drop Microextraction for the Determination of Organophosphorous Pesticides by Gas Chromatography-Mass Spectrometry. J. Sep. Sci., 34 (15), 1880-1885.
91. Wiilkowska, A.; Biziuk, M. (2011) Determination of Pesticide Residues in Food Matrices Using the QuEChERS Methodology. Food Chem., 125 (3), 803-812.
92. Witczak, A.; Patrzykat, A. (2011) Comparison of Two Sample Preparation Methods for Analysis of Organochlorine Pesticides Residues in Fish Muscle. J. Environ. Sci. Health Part B-Pestic. Contam. Agric. Wastes, 46 (2), 191-197.
93. Wu, G.; Bao, X. X.; Zhao, S. H.; Wu, J. J.; Han, A. L.; Ye, Q. F. (2011) Analysis of Multi-Pesticide Residues in the Foods of Animal Origin by GC-MS Coupled with Accelerated Solvent Extraction and Gel Permeation Chromatography Cleanup. Food Chem., 126 (2), 646-654.
94. Wu, J.; Liu, Y.; Zhao, R.; Xu, R. (2011) Fast Pesticide Multiresidue Analysis in American Ginseng (Panax quinquefolium L.) by Gas Chromatography with Electron Capture Detection. J. Nat. Med., 65 (2), 406-409.
95. Xie, W.; Han, C.; Qian, Y.; Ding, H. Y.; Chen, X. M.; Xi, J. Y. (2011) Determination of Neonicotinoid Pesticides Residues in Agricultural Samples by Solid-Phase Extraction Combined with Liquid Chromatography-Tandem Mass Spectrometry. J. Chromatogr. A, 1218 (28), 4426-4433.
96. Xu, R.; Wu, J. W.; Liu, Y. G.; Zhao, R. H.; Chen, B.; Yang, M. H.; Chen, J. (2011) Analysis of Pesticide Residues Using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) Pesticide Multiresidue Method in Traditional Chinese Medicine by Gas Chromatography with Electron Capture Detection. Chemosphere, 84 (7), 908-912.
97. Xu, X. M.; Yu, C.; Han, J. L.; Li, J. P.; El-Sepai, F.; Zhu, Y.; Huang, B. F.; Cai, Z. X.; Wu, H. W.; Ren, Y. P. (2011) Multi-Residue Analysis of Pesticides in Tea by Online SEC-GC/MS. J. Sep. Sci., 34 (2), 210-216.
98. Xu, Z. L.; Zeng, D. P.; Yang, J. Y.; Shen, Y. D.; Beier, R. C.; Lei, H. T.; Wang, H.; Sun, Y. M. (2011) Monoclonal Antibody-Based Broad-Specificity Immunoassay for Monitoring Organophosphorus Pesticides in Environmental Water Samples. J. Environ. Monit., 13 (11), 3040-3048.
99. Yang, X.; Wang, J.; Xu, D. C.; Qiu, J. W.; Ma, Y.; Cui, J. (2011) Simultaneous Determination of 69 Pesticide Residues in Coffee by Gas Chromatography-Mass Spectrometry. Food Anal. Meth., 4 (2), 186-195.
100. Yang, X.; Zhang, H.; Liu, Y.; Wang, J.; Zhang, Y. C.; Dong, A. J.; Zhao, H. T.; Sun, C. H.; Cui, J. (2011) Multiresidue Method for Determination of 88 Pesticides in Berry Fruits Using Solid-Phase Extraction and Gas Chromatography-Mass Spectrometry: Determination of 88 Pesticides in Berries Using SPE and GC-MS. Food Chem., 127 (2), 855-865.
101. Zhang, K.; Wong, J. W.; Yang, P.; Tech, K.; DiBenedetto, A. L.; Lee, N. S.; Hayward, D. G.; Makovi, C. M.; Krynitsky, A. J.; Banerjee, K.; Jao, L.; Dasgupta, S.; Smoker, M. S.; Simonds, R.; Schreiber, A. (2011) Multiresidue Pesticide Analysis of Agricultural Commodities Using Acetonitrile Salt-out Extraction, Dispersive Solid-Phase Sample Clean-up, and High-Performance Liquid Chromatography-Tandem Mass Spectrometry. J. Agric. Food Chem., 59 (14), 7636-7646.
102. Zhang, Y. P.; Yang, J.; Shi, R. H.; Su, Q. D.; Gao, Y.; Zhu, X. L. (2011) Development of an Analytical Method Based on Accelerated Solvent Extraction, Solid-Phase Extraction Clean-Up, Then GC-ECD for Analysis of Fourteen Organochlorine Pesticides in Cereal Crops. Chromatographia, 73 (3-4), 385-391.
103. Zhao, W. J.; Sun, X. K.; Deng, X. N.; Huang, L.; Yang, M. M.; Zhou, Z. M. (2011) Cloud Point Extraction Coupled with Ultrasonic-Assisted Back-Extraction for the Determination of Organophosphorus Pesticides in Concentrated Fruit Juice by Gas Chromatography with Flame Photometric Detection. Food Chem., 127 (2), 683-688.
104. Zhao, Y. G.; Shen, H. Y.; Shi, J. W.; Chen, X. H.; Jin, M. C. (2011) Preparation and Characterization of Amino Functionalized Nano-Composite Material and Its Application for Multi-Residue Analysis of Pesticides in Cabbage by Gas Chromatography-Triple Quadrupole Mass Spectrometry. J. Chromatogr. A, 1218 (33), 5568-5580.
105. Zhao, Z. H.; Zhang, L.; Wu, J. L.; Jin, M.; Fan, C. X. (2011) Evaluation of Dispersive Liquid-Liquid Microextraction Coupled with Gas Chromatography-Microelectron Capture Detection (GC-MU ECD) for the Determination of Organochlorine Pesticides in Water Samples. Anal. Sci., 27 (5), 547-553.
106. Zhou, L.; Duan, C. M.; Wang, M. L.; Wang, J. H.; Zhang, R. (2011) Analysis of Residues of 81 Pesticides on Ginkgo Leaves Using QuEChERS Sample Preparation and Gas Chromatography/Mass Spectrometry. J. AOAC Int., 94 (1), 313-321.