Extraction of pesticides, dioxin-like PCBs and PAHs in water based commodities using liquid-liquid microextraction and analysis by gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1218, Issue 38, 2011, Pages 6780-6791

  Dasgupta, Soma ^a,b   Banerjee, Kaushik ^a   Utture, Sagar ^a,c   Kusari, Parijat ^d   Wagh, Sameer ^a   Dhumal, Kondiba ^b   Kolekar, Sanjay ^c   Adsule, Pandurang G ^a  

^a NATIONAL RESEARCH CENTRE FOR GRAPES   (India)

^b UNIVERSITY OF PUNE   (India)

^c SHIVAJI UNIVERSITY   (India)

^d KIIT UNIVERSITY   (India)

Author keywords

Dioxin like polychlorinated biphenyls; Gas chromatography time of flight mass spectrometry; Measurement uncertainty; Method validation; Microextraction; Pesticide residues; Polyaromatic hydrocarbons

Indexed keywords

DIOXIN-LIKE POLYCHLORINATED BIPHENYLS; MEASUREMENT UNCERTAINTY; METHOD VALIDATION; MICROEXTRACTION; PESTICIDE RESIDUES; POLYAROMATIC HYDROCARBONS;

BEVERAGES; CENTRIFUGATION; CHLORINE COMPOUNDS; FRUITS; GAS CHROMATOGRAPHY; HYDROCARBONS; ISOTOPES; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETERS; MASS SPECTROMETRY; ORGANIC POLLUTANTS; PESTICIDES; POLYCHLORINATED BIPHENYLS; POLYCYCLIC AROMATIC HYDROCARBONS; POTABLE WATER; TRACE ANALYSIS; UNCERTAINTY ANALYSIS;

SOLVENT EXTRACTION;

4,4' ISOPROPYLIDENEDIPHENOL; ACETIC ACID ETHYL ESTER; ANTHRACENE; ATRAZINE; CARBARIL; CARBOFURAN; CARBOSULFAN; CHLOROFORM; CYCLOHEXANE; DIMETHOATE; DIMPYLATE; DIOXIN; ETRIMFOS; FENOBUCARB; FLUORENE; METALAXYL; METRIBUZIN; MEVINPHOS; NAPHTHALENE; PESTICIDE; PHENANTHRENE; PHORATE; PHOSPHAMIDON; POLYCHLORINATED BIPHENYL; POLYCYCLIC AROMATIC HYDROCARBON; PROPANIL; PROPOXUR; SOLVENT; THIOMETON;

APPLE; ARTICLE; EXTRACTION; GRAPE; LEMON; LIQUID LIQUID MICROEXTRACTION; MASS FRAGMENTOGRAPHY; PINEAPPLE; POMEGRANATE JUICE; PRIORITY JOURNAL; PROCESS OPTIMIZATION; SEPARATION TECHNIQUE; TIME OF FLIGHT MASS SPECTROMETRY; VALIDATION STUDY; WATER SAMPLING;

CHEMICAL FRACTIONATION; DIOXINS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; PESTICIDES; POLYCHLORINATED BIPHENYLS; POLYCYCLIC HYDROCARBONS, AROMATIC; WATER POLLUTANTS, CHEMICAL;

ANANAS COMOSUS; CITRUS LIMON; LYTHRACEAE; MALUS X DOMESTICA; VITACEAE;

EID: 80052078231     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.07.043     Document Type: Article

References (31)

1. FAO/WHO (World Health Organization). Guidelines for Predicting Dietary Intake of Pesticide Residues, 24. Geneva, 1989.
2. Tariq M.I., Afzal S., Hussain I. Environ. Int. 2004, 30:471.
3. Fernandez-Alvarez M., Llompart M., Lamas J.P., Lores M., Garcia-Jares C., Cela R., Dagnac T. J. Chromatogr. A 2008, 1188:154.
4. Xue N., Xu X., Jin Z. Chemosphere 2005, 61:1594.
5. Harner T., Shoeib M., Kozma M., Gobas F.A., Li S.M. Environ. Sci. Technol. 2005, 39:724.
6. 2010 (accessed 30.07.10.). http://www.who.int/water_sanitation_health/dwq/guidelines/en/.
7. US Environmental Protection Agency, National Survey of Pesticides in Drinking Water Wells, Phase II Report, EPA 570/9-91-020, National Technical Information Service, Springfield, VA, 1992.
8. Fatoki O.S., Awofolu R.O. J. Chromatogr. A 2003, 983:225.
9. Rial-Otero R., Cancho-Grande B., Simal-Gándara J. J. Chromatogr. A 2003, 992:121.
10. Pose-Juan E., Cancho-Grande B., Rial-Otero R., Simal-Gándara J. Food Control 2006, 17:1012.
11. Aguilar C., Borrull F., Marce R.M. J. Chromatogr. A 1997, 771:221.
12. López-Blanco M.C., Cancho-Grande B., Simal-Gándara J. J. Chromatogr. A 2002, 963:117.
13. García-Falcón M.S., Pérez-Lamela C., Simal-Gándara J. Anal. Chim. Acta 2004, 508:177.
14. García-Falcón M.S., Pérez-Lamela M., Simal-Gándara J. J. Agric. Food Chem. 2004, 52:6897.
15. López-Blanco C., Gómez-Álvarez S., Rey-Garrote M., Cancho-Grande B., Simal-Gándara J. Anal. Bioanal. Chem. 2006, 384:1002.
16. Dong C., Zeng Z., Yang M. Water Res. 2005, 39:4204.
17. Psillakis E., Kalogerakis N. Trends Anal. Chem.: TRAC 2003, 22:565.
18. Rial-Otero R., Yagüe-Ruiz C., Cancho-Grande B., Simal-Gándara J. J. Chromatogr. A 2002, 942:41.
19. Rezaeea M., Assadia Y., Hosseinia M.M., Aghaeea E., Ahmadia F., Berijania S. J. Chromatogr. A 2006, 1116:1.
20. Regueiro J., Llompart M., Garcia-Jares C., Garcia-Monteagudo J.C., Cela R. J. Chromatogr. A 2008, 1190:27.
21. Insecticides Registered Under Section 9(3) of the Insecticide Act, 1968 as on 14/09/2010, New Delhi, India. 2010 (accessed 03.11.10.). http://www.cibrc.nic.in/reg_products.htm.
22. US EPA, Method 3510C, Separatory Funnel Liquid-Liquid Extraction (Revision 3 - December). SW846 CH 4.2.1, 1996.
23. Aydin M.E., Wichmann H., Bahadir M. Fresenius Environ. Bull. 2004, 13:118.
24. Thompson M., Ellison S.L., Wood R. Pure Appl. Chem. 2002, 74:835.
25. Horwitz W., Albert R. J. AOAC Int. 2006, 89:1095.
26. Horwitz W., Kamps L.R., Boyer K.W. J. Assoc. Off. Anal. Chem. 1980, 63:1344.
27. Guide CG 4, Quantifying Uncertainty in Analytical Measurement, EURACHEM [UK]/CITAC [UK], 2nd ed. 2000. http://www.measurementuncertainty.org/.
28. Banerjee K., Oulkar D.P., Dasgupta S., Patil S.B., Patil S.H., Savant R., Adsule P.G. J. Chromatogr. A 2007, 1173:98.
29. Banerjee K., Patil S.H., Dasgupta S., Oulkar D.P., Patil S.B., Savant R., Adsule P.G. J. Chromatogr. A 2008, 1190:350.
30. Wu Q.H., Xin Z., Li Y.M., Zang X.H., Wang C., Wang Z. Anal. Bioanal. Chem. 2009, 393:1755.
31. Method Validation and Quality Control Procedures for Pesticide Residues Analysis in Food and Feed, Document No. SANCO/10684/2009.