Analysis of multi-pesticide residues in the foods of animal origin by GC-MS coupled with accelerated solvent extraction and gel permeation chromatography cleanup

Food Chemistry

Volumn 126, Issue 2, 2011, Pages 646-654

  Wu, Gang ^a,b   Bao, Xiaoxia ^b   Zhao, Shanhong ^b   Wu, Jianjian ^b   Han, Ailiang ^a   Ye, Qingfu ^a  

^a ZHEJIANG UNIVERSITY   (China)

^b Zhejiang Academy of Science and Technology for Inspection and Quarantine   (China)

Author keywords

Accelerated solvent extraction; Food of animal origin; GC MS; Gel permeation chromatography; Pesticides multi residues

Indexed keywords

ACCELERATED SOLVENT EXTRACTION; ANALYTES; ANALYTICAL METHOD; AVERAGE RECOVERY; CHLORPYRIFOS; FOOD OF ANIMAL ORIGIN; FOODS OF ANIMAL ORIGIN; GC-MS; GEL PERMEATION; INTERNAL STANDARDS; LIMIT OF DETECTION; PESTICIDE RESIDUE; RELATIVE STANDARD DEVIATIONS; SELECTED ION MONITORING;

ACETONITRILE; AGRICULTURAL CHEMICALS; ANIMALS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; GEL PERMEATION CHROMATOGRAPHY; GELS; ISOMERS; ORGANIC SOLVENTS; PESTICIDES; SOLVENT EXTRACTION;

CHEMICAL CONTAMINATION;

ACETONITRILE; CHLORPYRIFOS; PESTICIDE RESIDUE;

ACCELERATED SOLVENT EXTRACTION; ACCURACY; ARTICLE; CHEMICAL ANALYSIS; DISPERSION; GEL PERMEATION CHROMATOGRAPHY; HUMAN; ION MONITORING; MASS FRAGMENTOGRAPHY; NONHUMAN; QUALITATIVE ANALYSIS; SOLVENT EXTRACTION;

ANIMALIA;

EID: 78650679655     PISSN: 03088146     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodchem.2010.10.105     Document Type: Article

References (17)

1. F.E. Ahmed Analyses of pesticides and their metabolites in foods and drinks Trends in Analytical Chemistry 20 2001 649 661
2. M. Anastassiades, S.J. Lehotay, D. Stajnbaher, and F.J. Schenck Fast and easy multiresidue method employing acetonitrile extraction/partitioning and dispersive solid-phase extraction for the determination of pesticide residues in produce Journal of AOAC International 86 2003 412 431
3. A.G. Frenich, J.L.M. Vidal, A.D.C. Sicilia, M.J.G. Rodríguez, and P.P. Bolaños Multiresidue analysis of organochlorine and organophosphorus pesticides in muscle of chicken, pork and lamb by gas chromatography-triple quadrupole mass spectrometry Analytica Chimica Acta 558 2006 42 52
4. Hogsette, J. A., Koehler, P. G., Kaufman, P. E. (2006). Pesticide safety around animals. .
5. M.L. Hopper Automated gel permeation system for rapid separation of industrial chemicals and organophosphate and chlorinated pesticides from fats Journal of Agricultural Food Chemistry 30 1982 1038 1041
6. M.L. Hopper Automated one-step supercritical fluid extraction and cleanup system for the analysis of pesticide residues in fatty matrices Journal of Chromatography A 840 1999 93 105
7. M. Kirchner, R. Húšková, E. Matisová, and J. Mocák Fast gas chromatography for pesticide residues analysis using analyte protectants Journal of Chromatography A 1186 2008 271 280
8. S.J. Lehotay, A. de Kok, M. Hiemstra, and P. van Bodegraven Validation of a fast and easy method for the determination of 229 pesticide residues in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection Journal of AOAC International 88 2005 595 614
9. Lin W. X. (2002). The compilation of residue limits standards for pesticides and veterinary drugs in foodstuffs in the world (pp. 3-1288). Dalian: Dalian Maritime University Press.
10. G.F. Pang, Y.Z. Cao, J.J. Zhang, C.L. Fan, Y.M. Liu, and X.M. Li Validation study on 660 pesticide residues in animal tissues by gel permeation chromatography cleanup/gas chromatography-mass spectrometry and liquid chromatography-tandem mass spectrometry Journal of Chromatography A 1125 2006 1 30
11. L.V. Podhorniak, J.R. Negron, and F.D. Griffith Jr. Gas chromatography with pulsed flame photometric detection multiresidue method for organophosphate pesticide and metabolite residues at the parts-per-billion level in representative commodities of fruit and vegetable crop groups Journal of AOAC International 84 2001 873 890
12. B.E. Richter, B.A. Jones, J.L. Ezzell, and N.L. Porter ASE: A technique for sample preparation Analytical Chemistry 68 1996 1033 1039
13. D.L. Stalling, R.C. Tindle, and J.L. Johnson Cleanup of pesticide and polychlorinated biphenyl residues in fish extracts by gel permeation chromatography Journal of AOAC International 55 1972 32 38
14. H.J. Stan Pesticide residue analysis in foodstuffs applying capillary gas chromatography with mass spectrometric detection state-of-the-art use of modified DFG-multimethod S19 and automated data evaluation Journal of Chromatography A 892 2000 347 377
15. E. Ueno, H. Oshima, I. Saito, and H. Matsumoto Determination of nitrogen-and phosphorus-containing pesticide residues in vegetables by gas chromatography with nitrogen-phosphorus and flame photometric detection after gel permeation chromatography and a two-step minicolumn cleanup Journal of AOAC International 86 2003 1241 1251
16. E. Ueno, H. Oshima, I. Saito, and H. Matsumoto Multiresidue analysis of pesticides in vegetables and fruits by gas chromatography/mass spectrometry after gel permeation chromatography and graphitised carbon column cleanup Journal of AOAC International 87 2004 1003 1015
17. US Environmental Protection Agency (EPA). SW-846 test methods for evaluating solid waste, Method 3545. US EPA, Washington, DC; July 18, 2002.