Cloud point extraction coupled with ultrasonic-assisted back-extraction for the determination of organophosphorus pesticides in concentrated fruit juice by gas chromatography with flame photometric detection

Food Chemistry

Volumn 127, Issue 2, 2011, Pages 683-688

  Zhao, Wei Jun ^a   Sun, Xiao Ke ^a   Deng, Xiao Ni ^b   Huang, Lin ^c   Yang, Ming Min ^d   Zhou, Zhi Ming ^d  

^a Department of Quality Assurance   (China)

^b Center for Fisheries Environment and Quality of Fishery Products (Xi'an)   (China)

^c XI'AN MODERN CHEMISTRY RESEARCH INSTITUTE   (China)

^d NANJING AGRICULTURAL UNIVERSITY   (China)

Author keywords

Cloud point extraction (CPE); Concentrated fruit juice; Gas chromatography with flame photometric detection (GC FPD); Organophosphorus pesticides (OPPs); Ultrasonic assisted back extraction

Indexed keywords

BACK EXTRACTION; CHLORPYRIFOS; CLOUD POINT EXTRACTIONS; CLOUD-POINT EXTRACTION; CONCENTRATED FRUIT JUICE; DICHLORVOS; DIMETHOATE; ETHYL ACETATES; FLAME PHOTOMETRIC DETECTION; LIMITS OF DETECTION; LIMITS OF QUANTIFICATION; METHAMIDOPHOS; OPTIMUM CONDITIONS; ORGANOPHOSPHORUS PESTICIDE; ORGANOPHOSPHORUS PESTICIDES (OPPS); PARATHION-METHYL; PRE-CONCENTRATION; RELATIVE STANDARD DEVIATIONS;

AGRICULTURAL CHEMICALS; ESTERS; FRUIT JUICES; FRUITS; PESTICIDES; PHOTOMETRY; POLYETHYLENE GLYCOLS; POLYETHYLENE OXIDES; SODIUM; ULTRASONIC APPLICATIONS; ULTRASONICS; VOLATILE FATTY ACIDS;

GAS CHROMATOGRAPHY;

ACEPHATE; ACETIC ACID ETHYL ESTER; CHLORPYRIFOS; DICHLORVOS; DIMETHOATE; DIMPYLATE; MACROGOL 6000; MALATHION; METHAMIDOPHOS; ORGANOPHOSPHATE PESTICIDE; PARATHION; PARATHION METHYL; SODIUM SULFATE;

APPLE; ARTICLE; CLOUD POINT EXTRACTION; EXTRACTION; FRUIT JUICE; GAS CHROMATOGRAPHY; HUMAN; LIMIT OF QUANTITATION; PEAR; PHOTOMETRY; ULTRASOUND;

EID: 79952311090     PISSN: 03088146     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodchem.2010.12.122     Document Type: Article

References (23)

1. Ahmadi, F., Assadi, Y., Milani Hosseini, S. M. R., & Rezaee, M. (2006). Determination of organophosphorus pesticides in water samples by single drop microextraction and gas chromatography-flame photometric detector. Journal of Chromatography A, 1101, 307-312. (Pubitemid 41785563)
2. Barcelo, D., Porte, C., Cid, J., & Albaines, J. (1990). Determination of organophosphorus compounds in mediterranean coastal waters and biota samples using gas chromatography with nitrogen-phosphorus and chemical ionization mass spectrometric detection. International Journal of Environmental Analytical Chemistry, 38, 199-209.
3. Froschl, B., Stangl, G., Niessner & Fresenius, R. (1997). Combination of micellar extraction and GC-ECD for the determination of polychlorinated biphenyls (PCBs) in water. Journal of Analytical Chemistry, 357, 743-746. (Pubitemid 127713821)
4. Ganong, B. R., & Delmore, J. P. (1991). Phase separation temperatures of mixtures of Triton X-114 and Triton X-45: Application to protein separation. Analytical Biochemistry, 193, 35-37.
5. Giokas, D. L., Sakkas, V. A., Albanis, T. A., & Lampropoulou, D. A. (2005). Determination of UV-filter residues in bathing waters by liquid chromatography UV-diode array and gas chromatography-mass spectrometry after micelle mediated extraction-solvent back extraction. Journal of Chromatography A, 1077, 19-27. (Pubitemid 40755101)
6. Gomes, J., Anilal, S. V., & Lloyd, O. (1999). Reproductive and developmental toxicity from organophosphorus pesticide formulations: Litter size and low fetal weight. Journal of Agricultural Safety and Health, 5, 239-248. (Pubitemid 30553263)
7. Hyötyläinen, T., Lüthje, K., Rautiainen-Rämä, M., & Riekkola, M. L. (2004). Determination of pesticides in red wines with on-line coupled microporous membrane liquid-liquid extraction-gas chromatography. Journal of Chromatography A, 1056, 267-271. (Pubitemid 39505135)
8. Jia, G. F., Lv, C. G., Zhu, W. T., Qiu, J., Wang, X. Q., & Zhou, Z. Q. (2008). Applicability of cloud point extraction coupled with microwave-assisted back-extraction to the determination of organophosphorous pesticides in human urine by gas chromatography with flame photometry detection. Journal of Hazardous materials, 159, 300-305.
9. Jin, S. Y., Xu, Z. C., Chen, J. P., Liang, X. M., Wu, Y. N., & Qian, X. H. (2004). Determination of organophosphate and carbamate pesticides based on enzyme inhibition using a pH-sensitive fluorescence probe. Analytica Chimica Acta, 523, 117-123.
10. Lambropolou, D. A., & Albanis, T. A. (2003). Headspace solid-phase microextraction in combination with gas chromatography-mass spectrometry for the rapid screening of organophosphorus insecticide residues in strawberries and cherries. Journal of Chromatography A, 993, 197-203.
11. Lin, T. J., Huang, K. T., & Liu, L. Y. (2006). Determination of organophosphorous pesticides by a novel biosensor based on localized surface plasmon resonance. Biosensors and Bioelectronics, 22, 513-518.
12. Liu, W. P., & Lee, H. K. (1998). Quantitative analysis of pesticides by capillary column high performance liquid chromatography combined with solid-phase extraction. Talanta, 45, 631-639.
13. Martinez, R. C., Gonzalo, E. R., Moran, M. J. A., & Mendez, J. H. (1992). Sensitive method for the determination of organophosphorus pesticides in fruits and surface waters by high-performance liquid chromatography with ultraviolet detection. Journal of Chromatography A, 607, 37-45.
14. Miura, J., Ishii, H., & Watanabe, H. (1976). Extraction and separation of nickel chelate of 1-(2-thiazolylazo)-2-naphthol in nonionic surfactant solution. Bunseki Kagaku, 25, 808-809.
15. Mo, X. R., Zheng, C. H., Chen, J. W., Zhao, D. Y., & Yang, M. M. (2009). Applicability of cloud point extraction coupled with ultrasonic - assisted back - extraction to the determination of pyrethroid pesticides in tea by gas chromatography with electron capture detection. China Journal of Analytical Chemistry, 37, 1178-1182.
16. Pinto, C. G., Pavón, J. L. P., & Cordero, B. M. (1995). Cloud point preconcentration and high-performance liquid chromatographic determination of organophosphorus pesticides with dual electrochemical detection. Corder. Analytical Chemistry, 67, 2606-2612.
17. Rastrelli, L., Totaro, K., & Simone, F. D. (2002). Determination of organophosphorus pesticide residues in Cilento (Campania, Italy) virgin olive oil by capillary gas chromatography. Food Chemistry, 79, 303-305. (Pubitemid 36163362)
18. Sanz, G. P., Halko, R., Ferrera, Z. S., & Rodriguez, J. J. S. (2004). Micellar extraction of organophosphorus pesticides and their determination by liquid chromatography. Analytica Chimica Acta, 524, 265-270. (Pubitemid 39244051)
19. Shen, J. C., & Shao, X. G. (2006). Determination of tobacco alkaloids by gas chromatography-mass spectrometry using cloud point extraction as a preconcentration step. Analytica Chimica Acta, 561, 83-87.
20. Sikalos, T. I., & Paleologos, E. K. (2005). Cloud point extraction coupled with microwave or ultrasonic assisted back extraction as a preconcentration step prior to gas chromatography. Analytical Chemistry, 77, 2544-2549.
21. SN 0334-1995, Method for the determination of 22 organophosphorus pesticides multi-residues in fruits and vegetable for export.
22. Zhu, F., Ruan, W. H., He, M. H., Zeng, F., Luan, T. G., & Tong, Y. X. (2009). Application of solid-phase microextraction for the determination of organophosphorus pesticides in textiles by gas chromatography with mass spectrometry. Analytica Chimica Acta, 650, 202-206.
23. Zygoura, P. D., Paleologos, E. K., Riganakos, K. A., & Kontominas, M. G. (2005). Determination of diethylhexyladipate and acetyltributylcitrate in aqueous extracts after cloud point extraction coupled with microwave assisted back extraction and gas chromatographic separation. Journal of Chromatography A, 1093, 29-35. (Pubitemid 41446944)