Solid-phase extraction for multi-residue analysis of pesticides in honey

Journal of Environmental Science and Health - Part B Pesticides, Food Contaminants, and Agricultural Wastes

Volumn 46, Issue 1, 2011, Pages 24-34

  Graziella, Amendola ^a   Pelosi, Patrizia ^a   Dommarco, Roberto ^a  

^a ISTITUTO SUPERIORE DI SANITÀ   (Italy)

Author keywords

Food analysis; Gas chromatography (GC); Honey; Liquid chromatography (LC); Pesticides multi residue analysis; Solid phase extraction (SPE)

Indexed keywords

ACCURACY AND PRECISION; ALDICARB; ANALYTICAL PROCEDURE; DERIVATIZATIONS; EUROPEAN UNION; FLAME PHOTOMETRIC DETECTORS; FOOD ANALYSIS; HONEY; LIMIT OF DETECTION; LIMIT OF QUANTIFICATIONS; LOW CONCENTRATIONS; MULTI-RESIDUE ANALYSIS; ORGANOCHLORINES; PESTICIDE RESIDUE; PYRETHROIDS; RELATIVE STANDARD DEVIATIONS; REPRODUCIBILITIES; SOLID-PHASE EXTRACTION; SOLID-PHASE EXTRACTION (SPE); SPECTROFLUORIMETRIC; SULPHOXIDE;

ACETONE; AGRICULTURAL CHEMICALS; CHEMICAL CONTAMINATION; DETECTORS; DICHLOROMETHANE; ESTERS; EXTRACTION; INSECTICIDES; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; RECOVERY;

GAS CHROMATOGRAPHY;

ACCURACY ASSESSMENT; ACETONE; AQUEOUS SOLUTION; CONCENTRATION (COMPOSITION); EUROPEAN UNION; GAS CHROMATOGRAPHY; HONEY; LINEARITY; MASS SPECTROMETRY; PERFORMANCE ASSESSMENT; PESTICIDE; PHOTOMETER; QUANTITATIVE ANALYSIS;

EID: 78650087714     PISSN: 03601234     EISSN: 15324109     Source Type: Journal    
DOI: 10.1080/03601234.2010.515170     Document Type: Article

References (29)

1. Ben ́ech, A.; Wolff, A.L. Natural delights. Food Ingredients & Analysis International 2006, June, 21-22.
2. Wallner, K. Varroacides and their residues in bee products. Apidologie 1999, 30, 235-248.
3. Koch, H.; Weißer, P. Exposure of honey bees during pesticide application under field conditions. Apidologie 1997, 28, 439-447.
4. Ferńandez, M.; Pic ́ o, Y.; Ma ̃nes, J. Analytical methods for pesticide residue determination in bee products. Journal of Food Protection 2002, 65, 1502-1511.
5. Korta, E.; Bakkali, A.; Berrueta, L.A.; Gallo, B.; Vicente, F. Study of semi-automated solid-phase extraction for the determination of acaricide residues in honey by liquid chromatography. J. Chromatogr. A, 2001, 930, 21-29.
6. Blasco, C.; Fern ́andez, M.; Pena, A.; Lino, C.; Silveira, M.I.; Font, G.; Pic ́ o, Y. Assessment of pesticide residues in honey samples from Portugal and Spain. J. Agric. Food Chem. 2003, 51, 8132-8138.
7. Albero, B.; S ́anchez-Brunete, C.; Tadeo, J.L. Analysis of pesticides in honey by solid phase extraction and gas chromatography-mass spectrometry. J. Agric. Food Chem. 2004, 52, 5828-5835.
8. Herrera, A.; P ́erez-Arquillu ́e, C.; Conchello P.; Bayarri S.; L ́azaro R.; Yag̈ue C.; Ari ̃no A. Determination of pesticides and PCBs in honey by solid-phase extraction cleanup followed by gas chromatography with electron-capture and nitrogen-phosphorus detection. Anal. Bioanal. Chem. 2005, 381, 695-701.
9. Barakat, A.A.; Badawy, H.M.A.; Salama, E.; Attallah, E.; Maatook, G. Simple and rapid method of analysis for the determination of pesticide residues in honey using dispersive solid-phase extraction and GC determination. J. Food Agr. Environ. 2007, 5, 97-100.
10. Jiḿenez J.J.; Bernal J.L.; del Nozal M.J.; Mart ́in M.T.; Mayorga A.L. Solid-phase microextraction applied to the analysis of pesticide residues in honey using gas chromatography with electron-capture detection. J. Chromatogr. A 1998, 829, 269-277.
11. Blasco, C.; Font, G.; Pic ́ o, Y. Solid-phase microextraction-liquid chromatography-mass spectrometry applied to the analysis of insecticides in honey. Food Addit. Contam. Part A 2008, 25, 56-69.
12. Campillo, N.; Pe ̃nalver, R.; Aguinaga, N.; Hern ́andez-C ́ordoba,M. Solid-phase microextraction and gas chromatography with atomic emission detection for multiresidue determination of pesticides in honey. Analytica Chimica Acta 2006, 562, 9-15.
13. Albero, B.; S ́anchez-Brunete, C.; Tadeo, J.L. Multiresidue determination of pesticides in honey by matrix solid-phase dispersion and gas chromatography with electron-capture detection. J. AOAC Int. 2001, 84, 1165-1171.
14. Śanchez-Brunete, C.; Albero, B.; Miguel, E.; Tadeo, J.L. Determination of insecticides in honey bymatrix solid-phase dispersion and gas chromatography with nitrogen-phosphorus detection and mass spectrometry confirmation. J. AOAC Int. 2002, 85,128-133.
15. Rissato, S.R.; Galhiane, M.S.; Knoll, F.R.N.; Apon, B.M. Supercritical fluid extraction for pesticide multiresidue analysis in honey: determination by gas chromatography with electron-capture and mass spectrometry detection. J. Chromatogr. A 2004, 1048, 153- 159.
16. Korta, E.; Bakkali, A.; Berrueta, L.A.; Gallo, B.; Vicente, F. Study of accelerated solvent extraction procedure for the determination of acaricide residues in honey by high performance liquid chormatography-diode array detector. J. Food Protection 2002, 65, 161-166.
17. Ferńandez, M.; Pic ́ o, Y.; Girotti, S.; Ma ̃nes, J. Analysis of organophosphorus pesticides in honeybee by liquid chromatography-atmospheric pressure chemical ionization mass spectrometry. J. Agric. Food. Chem. 2001, 49, 3540-3547.
18. Martel, A. C.; Zeggane, S. Determination of acaricides in honey by high-performance liquid chromatogaphy with photodiode array detection. J. Chromatogr. A 2002, 954, 173 180.
19. Blasco, C.; Lino, C.M.; Pic ́ o, Y.; Pena, A.; Font,G.; Silveira,M.I.N. Determination of organochlorine pesticide residues in honey from the central zone of Portugal and the Valencian community of Spain. J. Chromatogr. A 2004, 1049, 155-160.
20. Tahboub, Y.R.; Zaater, M.F.; Barri, T.A. Simultaneous identification and quantitation of selected organochlorine pesticide residues in honey by full-scan gas chromatography-mass spectrometry. Analytica Chimica Acta 2006, 558, 61-68.
21. Pang, G.F.; Fan, C.L.; Liu, Y.M.; Cao, Y.Z.; Zhang, J.J.; Fu, B.L.; Li, X.M.; Li, Z.Y.; Wu, Y.P. Multi-residue method for the determination of 450 pesticide residues in honey, fruit juice and wine by double-cartridge solid-phase extraction/gas chromatography-mass spectrometry and liquid chromatography-tandem mass spectrometry. Food Additives Contaminants 2006, 23, 777-810.
22. European Commission. Regulation (EC) n.396/2005 of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC. Official Journal of the European Union L 70, 2005, 1-16.
23. European Commission. DG SANCO. Document No. SANCO/ 10684/2009. Method validation and quality control procedures for pesticide residues analysis in food and feed. 2009, 1-53. http://ec. europa.eu/food/plant/protection/resources/publications en.htm (accessed Sept 2010).
24. Jiḿenez, J.J.; Bernal, J.L.; del Nozal, M.J.; Toribio, L.; Mart́in, M.T. Gas chromatography with electron-capture and nitrogenphosphorus detection in the analysis of pesticides in honey after elution from a Florisil column. Influence of the honey matrix on the quantitative results. J. Chromatogr. A 1998, 823, 381-387.
25. Di Muccio, A.; Ausili, A.; Camoni, I.; Dommarco, R.; Rizzica,M.; Vergori,F. Single-step solid-matrix clean-up of vegetable extracts for organo-phosphorus pesticide residue determination. J. Chromatogr. A 1988, 456, 149-153.
26. Di Muccio, A.; Dommarco, R.; Attard Barbini, D.; Santilio, A.; Girolimetti, S.; Ausili, A.; Ventriglia, M.; Generali, T.; Vergori, L. Application of solid-phase partition cartridges in the determination of fungicide residues in vegetable samples. J. Chromatogr. 1993, 643, 363-368.
27. Di Muccio, A.; Attard Barbini, D.; Generali, T.; Pelosi, P.; Ausili, A.; Vergori, F.; Camoni, I. Clean-up of aqueous acetone vegetable extracts by solid-matrix partition for pyrethroid residue determination by gas chromatography-electron-capture detection. J. Chromatogr. A 1997, 765, 39-49.
28. Di Muccio, A.;Girolimetti, S.; Attard Barbini,D.; Pelosi, P.;Generali, T.; Vergori, L.; De Merulis, G.; Leonelli, A.; Stefanelli, P. Selective clean-up applicable to aqueous acetone extracts for the determination of carbendazim and thiabendazole in fruits and vegetables by high-performance liquid chromatography with UV detection. J. Chromatogr. A 1999, 833, 61-65.
29. Fidente, P.; Seccia, S.; Vanni, F.; Morrica, P. Analysis of nicotinoid insecticides residues in honey by solid matrix partition cleanup and liquid chromatography-electrospray mass spectrometry. J. Chromatogr. A 2005, 1094, 175-178.