Multiresidue method for determination of 88 pesticides in berry fruits using solid-phase extraction and gas chromatography-mass spectrometry: Determination of 88 pesticides in berries using SPE and GC-MS

Food Chemistry

Volumn 127, Issue 2, 2011, Pages 855-865

  Yang, X ^a,c   Zhang, H ^a   Liu, Y ^b   Wang, J ^c   Zhang, Y C ^a   Dong, A J ^a   Zhao, H T ^a   Sun, C H ^d   Cui, J ^a  

^a HARBIN INSTITUTE OF TECHNOLOGY   (China)

^b Heilongjiang Entry Exit Inspection and Quarantine Bureau   (China)

^c INSTITUTE OF PLANT PROTECTION   (China)

^d Academe of Quality Inspection and Research for Heilongjiang Province   (China)

Author keywords

Berry fruits; GC MS; Multi residue analysis; Pesticides; SPE; Validation

Indexed keywords

BERRY FRUITS; GC-MS; MULTI-RESIDUE ANALYSIS; SPE; VALIDATION;

ACETONITRILE; AGRICULTURAL CHEMICALS; EXTRACTION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PESTICIDES; PROJECTILES; TOLUENE;

FRUITS;

ACETONITRILE; ALACHLOR; ALDRIN; ATRAZINE; BENFLURALIN; CHLOROTHALONIL; CHLORPROPHAM; CHLORPYRIFOS METHYL; DICHLORVOS; DIMETHOATE; DIMPYLATE; DIPHENYLAMINE; ETRIMFOS; FENOBUCARB; HEPTACHLOR; HEXACHLOROBENZENE; PESTICIDE; PESTICIDE RESIDUE; PHORATE; PIRIMICARB; PROMETON; PROPAZINE; QUINTOZENE; SIMAZINE; SULFOTEP; TERBUTRYN; TERBUTYLAZINE; TOLUENE; TRIFLURALIN; UNCLASSIFIED DRUG; VINCLOZOLIN;

ANALYTIC METHOD; ARTICLE; BLUEBERRY; CORRELATION COEFFICIENT; FRUIT; GRAPE; MASS FRAGMENTOGRAPHY; RASPBERRY; SOLID PHASE EXTRACTION; STRAWBERRY; VALIDATION STUDY;

FRAGARIA X ANANASSA; RUBUS GLAUCUS; VACCINIUM; VITACEAE;

EID: 79952316201     PISSN: 03088146     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodchem.2011.01.024     Document Type: Article

References (19)

1. Anastassiades, A., Lehotay, S. J., Štajnbaher, D., & Schenck, F. J. (2003). Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce. Journal of AOAC International, 86, 412-431.
2. Cai, L. S., Xing, J., Dong, L., & Wu, C. Y. (2003). Application of polyphenylmethylsiloxane coated fiber for solid-phase microextraction combined with microwave-assisted extraction for the determination of organochlorine pesticides in Chinese teas. Journal of Chromatography. A, 1015, 11-21. (Pubitemid 37163502)
3. Family Food Annual Reports. (2008). A report on the 2008 Family Food Module of the Living Costs and Food Survey. http://www.defra.gov.uk/evidence/ statistics/foodfarm/food/family food/ index.htm.
4. Fillion, J., Sauvé, F., & Selwyn, J. (2000). Multiresidue method for the determination of residues of 251 pesticides in fruits and vegetables by gas chromatography/mass spectrometry and liquid chromatography with fluorescence detection. Journal of AOAC International, 83, 698-713.
5. Global Berry Congress: 15-16 May 2008: London, UK. http://www.mintel. webbler.co.uk/?lid=982 on 4/05/09.
6. Hernando, M. D., Agüera, A., Fernández-Alba, A. R., Piedra, L., & Contreras, M. (2001). Gas chromatographic determination of pesticides in vegetable samples by sequential positive and negative chemical ionization and tandem mass spectrometric fragmentation using an ion trap analyser. Analyst, 126, 46-51. (Pubitemid 32183361)
7. Jansson, C., Pihlstrom, T., Öterdahl, B. G., & Markides, K. E. (2004). A new multiresidue method for analysis of pesticide residues in fruit and vegetables using liquid chromatography with tandem mass spectrometric detection. Journal of Chromatography. A, 1023(1), 93-104. (Pubitemid 37494816)
8. Perret, D., Gentili, A., Marchese, S., Sergi, M., & D'Ascenzo, G. (2002). Validation of a method for the determination of multiclass pesticide residues in fruit juices by liquid chromatography/tandem mass spectrometry after extraction by matrix solid-phase dispersion. Journal of AOAC International, 85(3), 724-730. (Pubitemid 135691748)
9. Podhorniak, L. V., Negron, J. F., & Griffith, F. D. (2001). Gas chromatography with pulsed flame photometric detection multiresidue method for organophosphate pesticide and metabolite residues at the parts-per-billion level in representative commodities of fruit and vegetable crop groups. Journal of AOAC International, 84, 873-890. (Pubitemid 33615032)
10. SANCO/10684/2009. (2010). Method validation and quality control procedures for pesticide residues analysis in food and feed. Commission of the European Communities, 8, 18.
11. Schenck, F. J., & Howard-King, V. (1999). Rapid solid phase extraction cleanup for pesticide residues in fresh fruits and vegetables. Bulletin of Environmental Contamination and Toxicology, 63, 277-281.
12. Seeram, N. P. (2008). Berry fruits: compositional elements, biochemical activities, and the impact of their intake on human health, performance, and disease. Journal of Agricultural and Food Chemistry, 56, 627-629.
13. Sheridan, R. S., & Meola, J. R. (1999). Analysis of pesticide residues in fruits, vegetables and milk by GC/tandem MS. Journal of AOAC International, 82, 982-990. (Pubitemid 129560962)
14. Specht, W., Pelz, S., & Gilsbach, W. (1995). Gas-chromatographic determination of pesticide residues after clean-up by gel-permeation chromatography and minisilica gel-column chromatography. Fresenius Journal of Analytical Chemistry, 353, 183-190.
15. Štajnbaher, D., & Zupančič-Kralj, L. (2003). Multiresidue method for determination of 90 pesticides in fresh fruits and vegetables using solid-phase extraction and gas chromatography-mass spectrometry. Journal of Chromatography. A, 1015(1), 185-198.
16. Stan, H. J. (2000). Pesticide residue analysis in foodstuffs applying capillary gas chromatography with mass spectrometric detection: State-of-the-art use of modified DFG-multimethod S19 and automated data evaluation. Journal of Chromatography. A, 892, 347-377.
17. Yang, X., Wang, J., Xu, D.C., Qiu, J.W., Ma, Y., & Cui, J. (2010) Simultaneous determination of 69 pesticide residues in coffee by gas chromatography-mass spectrometry. Food Analytical Methods, doi:10.1007/s12161- 010-9155-3.
18. Yang, X., Xu, D. C., Qiu, J. W., Zhang, H., Zhang, Y. C., Dong, A. J., et al. (2009). Simultaneous determination of 118 pesticide residues in china teas by gas chromatography-mass spectrometry. Chemical Papers, 63(1), 39-46.
19. Zambonin, C. G., Quinto, M., De Vietro, N., & Palmisano, F. (2004). Solid-phase microextraction-gas chromatography mass spectrometry: A fast and simple screening method for the assessment of organophosphorus pesticides residues in wine and fruit juices. Food Chemistry, 86(2), 269-274. (Pubitemid 38283582)