Sample Preparation Approaches for the Analysis of Pesticide Residues in Olives and Olive Oils

Olives and Olive Oil in Health and Disease Prevention

Volumn , Issue , 2010, Pages 653-666

  Cunha, Sara C ^a   Lehotay, Steven J ^b   Mastovska, Katerina ^b   Fernandes, José O ^a   Oliveira, M Beatriz P P ^c  

^a UNIVERSITY OF PORTO   (Portugal)

^b EASTERN REGIONAL RESEARCH CENTER   (United States)

^c FEDERAL UNIVERSITY OF JUIZ DE FORA   (Brazil)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84882849252     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1016/B978-0-12-374420-3.00070-X     Document Type: Chapter

References (47)

1. Amvrazi E.G., Albanis T.A. Multiresidue method for determination of 35 pesticides in virgin olive oil by using liquid-liquid extraction techniques coupled with solid-phase extraction clean up and gas chromatography with nitrogen phosphorus detection and electron capture detection. J. Agric. Food Chem. 2006, 54:9642-9651.
2. Anastassiades M., Lehotay S.J., Štajnbaher D., Schenck F.J. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce. J. AOAC Int. 2003, 86:412-431.
3. Arthur C.L., Killam L.M., Buchholz K.D., Pawliszyn J., Berg J.R. Automation and optimization of solid-phase microextraction. Anal. Chem. 1992, 64:1960-1966.
4. Ballesteros E., Sánchez G.A., Martos N.R. Simultaneous multidetermination of residues of pesticides and polycyclic aromatic hydrocarbons in olive and olive-pomace oils by gas chromatography/tandem mass spectrometry. J. Chromatogr. A 2006, 1111:89-96.
5. Barrek S., Paisse O., Grenier-Loustalot M.-F. Determination of residual pesticides in olive oil by GC-MS and HPLC-MS after extraction by size-exclusion chromatography. Anal. Bioanal. Chem. 2003, 376:355-359.
6. Botitsi E., Kormali P., Kontou S., Mourkojanni A., Stavrakaki E., Tsipi D. Monitoring of pesticide residues in olive oil samples: results and remarks between 1999 and 2002. Int. J. Environ. Anal. Chem. 2004, 84:231-239.
7. Caboni P., Cabras M., Angioni A., Russo M., Cabras P. Persistence of azadirachtin residues on olives after field treatment. J. Agric. Food Chem. 2002, 50:3491-3494.
8. Cabras P., Angioni A., Garau V.L., Melis M., Pirisi F.M., Karim M., Minelli E.V. Persistence of insecticide residues in olives and olive oil. J. Agric. Food Chem. 1997, 45:2244-2247.
9. Cabras P., Caboni P., Cabras M., Angioni A., Russo M. Rotenone residues on olives and in olive oil. J. Agric. Food Chem. 2002, 50:2576-2580.
10. Cajka T., Hajslova J., Lacina O., Mastovska K., Lehotay S.J. Rapid analysis of multiple pesticide residues in fruit-based baby food using programmed temperature vaporiser injection-low-pressure gas chromatography-high-resolution time-of-flight mass spectrometry. J. Chromatogr. A 2008, 1186:281-294.
11. Cunha S.C., Fernandes J.O., Oliveira M.B.P.P. Determination of phosmet and its metabolites in olives by matrix solid-phase dispersion and gas-chromatography mass spectrometry. Talanta 2007, 73:514-522.
12. Cunha S.C., Fernandes J.O., Oliveira M.B.P.P. Comparison of matrix-solid phase dispersion and liquid-liquid extraction for the chromatographic determination of fenthion and its metabolites in olives and olive oils. Food Add. Cont. 2007, 24:156-164.
13. Cunha S.C., Lehotay S.J., Mastovska K., Fernandes J.O., Oliveira M.B.P.P. Evaluation of the QuEChERS sample preparation approach for the analysis of pesticide residues in olives. J. Sep. Sci. 2007, 30:620-632.
14. Díaz-Plaza E.M., Cortés J.M., Vázquez A., Villén J. Automated determination of pesticide residues in olive oil by on-line reversed-phase liquid chromatography using the through oven transfer adsorption desorption interface with electron-capture and nitrogen-phosphorus detectors operating simultaneously. J. Chromatogr. A 2008, 1174:145-150.
15. Dugo G., Di Bella G., Torre L., Saitta M. Rapid GC-FPD determination of organophosphorus pesticide residues in Sicilian and Apulian olive oil. Food Control 2005, 16:435-438.
16. Ferrer C., Gomez M.J., Garcia-Reyes J.F., Ferrer I., Thurman E.M., Fernandez-Alba A.R. Determination of pesticide residues in olives and olive oil by matrix solid-phase dispersion followed by gas chromatography/mass spectrometry and liquid chromatography/tandem mass spectrometry. J. Chromatogr. A 2005, 1069:183-194.
17. Fontcuberta M., Arqués J.F., Villalbí J.R., Martínez M., Centrich F., Serrahima E., Pineda L., Duran J., Casas C. Chlorinated organic pesticides in marketed food: Barcelona, 2001-06. Sci. Total Environ. 2008, 389:52-57.
18. Frenich A.G., Moreno J.L.F., Vidal J.L.M., Liébanas F.J.A. Application of gas chromatography coupled to triple quadrupole mass spectrometry for the multiresidue analysis of pesticides in olive oil. J. Agric. Food Chem. 2007, 55:8346-8352.
19. Frenich A.G., Vidal J.L.M., Pastor-Montoro E., Romero-González R. High-throughput determination of pesticide residues in food commodities by use of ultra-performance liquid chromatography-tandem mass spectrometry. Anal. Bioanal. Chem. 2008, 390:947-959.
20. Gimeno E., Fitó M., Lamuela-Raventós R.M., Castellote A.I., Covas M., Farré M. Effect of ingestion of virgin olive oil on human low-density lipoprotein composition. Europ. J. Clin. Nut. 2002, 56:114-120.
21. Guardia-Rubio M., Fernandez-De Cordova M.L., Ayora-Canada M.J., Ruiz-Medina A. Simplified pesticide multiresidue analysis in virgin olive oil by gas chromatography with thermoionic specific, electron-capture and mass spectrometric detection. J. Chromatogr. A 2006, 1108:231-239.
22. Guardia-Rubio M., Marchal-Lopez R.M., Ayora-Canada M.J., Ruiz-Medina A. Determination of pesticides in olives by gas chromatography using different detection systems. J. Chromatogr. A 2007, 1145:195-203.
23. Hernando M.D., Ferrer C., Ulaszewska M., Garcia-Reyes J.F., Molina-Diaz A., Fernandez-Alba A.R. Application of high-performance liquid chromatography-tandem mass spectrometry with a quadrupole/linear ion trap instrument for the analysis of pesticide residues in olive oil. Anal. Bioanal. Chem. 2007, 389:1815-1831.
24. Hiskia A.E., Atmajidou M.E., Tsipi D.F. Determination of organophosphorus pesticide residues in Greek virgin olive oil by capillary gas chromatography. J. Agric. Food Chem. 1998, 46:570-574.
25. Leandro C.C., Hancock P., Fussell R.J., Keely B.J. Ultra-performance liquid chromatography for the determination of pesticide residues in foods by tandem quadrupole mass spectrometry with polarity switching. J. Chromatogr. A 2007, 1144:161-169.
26. Lehotay S.J. Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study. J AOAC Int. 2007, 90:485-520.
27. Lehotay S.J. Multiclass, multiresidue analysis of pesticides, strategies for. Encyclopedia of Analytical Chemistry 2000, 6344-6884. John Wiley and Sons, Chichester, UK. R.A. Meyers (Ed.).
28. Lehotay S.J., Hajšlova J. Application of gas chromatography in food analysis. Trends Anal. Chem. 2002, 21:686-697.
29. Lehotay S.J., Mastovska K., Yun S.J. Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes. J. AOAC Int. 2005, 88:630-638.
30. Lehotay S.J., de Kok A., Hiemstra M., Van Bodegraven P. Validation of a fast and easy method for the determination of residues from 229 pesticides in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection. J. AOAC Int. 2005, 88:595-614.
31. Lehotay S.J., Mastovska K., Lightfield A.R. Use of buffering and other means to improve results of problematic pesticides in a fast and easy method for residue analysis of fruits and vegetables. J. AOAC Int. 2005, 88:615-629.
32. Mastovska K., Lehotay S.J. Rapid sample preparation method for LC-MS/MS or GC-MS analysis of acrylamide in various food matrices. J. Agric. Food Chem. 2006, 54:7001-7008.
33. Nguyen T.D., Lee B.S., Lee B.R., Lee D.M., Lee G.H. A multiresidue method for the determination of 109 pesticides in rice using the quick easy cheap effective rugged and safe (QuEChERS) sample preparation method and gas chromatography/mass spectrometry with temperature control and vacuum concentration. Rap. Commun. Mass Spectrom. 2007, 21:3115-3122.
34. O'Reilly J., Wang Q., Setkova L., Hutchinson J.P., Chen Y., Lord H.L., Linton C.M., Pawliszyn J. Automation of solid-phase microextraction. J. Sep. Sci. 2005, 28:2010-2022.
35. Pawliszyn J. Solid Phase Microextraction Theory and Practice 1997, Wiley-VCH, New York.
36. Payá P., Anastassiades M., Mack D., Sigalova I., Tasdelen B., Oliva J., Barba A. Analysis of pesticide residues using the quick easy cheap effective rugged and safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection. Anal. Bioanal. Chem. 2007, 389:1697-1714.
37. Plössl F., Giera M., Bracher F. Multiresidue analytical method using dispersive solid-phase extraction and gas chromatography/ion trap mass spectrometry to determine pharmaceuticals in whole blood. J. Chromatogr. A 2006, 1135:19-26.
38. Posyniak A., Zmudzki J., Mitrowska K. Dispersive solid-phase extraction for the determination of sulfonamides in chicken muscle by liquid chromatography. J. Chromatogr. A 2005, 1087:259-264.
39. Rastrelli L., Totaro K., De Simone F. Determination of organophosphorus pesticide residues in Cilento (Campania, Italy) virgin olive oil by capillary gas chromatography. Food Chem. 2002, 79:303-305.
40. Rotunno T.C., Argenti R.L. Decay of fenthion in green table olives. J. Agric. Food Chem. 1997, 45:3957-3960.
41. Sanchez R., Vazquez A., Villén-Altamirano J., Villén J. Analysis of pesticide residues by on-line reversed-phase liquid chromatography-gas chromatography in the oil from olives grown in an experimental plot. J. Sci. Food Agric. 2006, 86:129-134.
42. Seiber J.N. Extraction, cleanup, and fractionation methods. Pesticide Residues in Foods: Methods, Technique and Regulations 1999, 17-63. John Wiley and Sons, New York. W.G. Fong, H.A. Moye, J.N. Seiber, J.P. Toth (Eds.).
43. Soler C., Picó Y. Recent trends in liquid chromatography-tandem mass spectrometry to determine pesticides and their metabolites in food. Trends Anal. Chem. 2007, 26:103-115.
44. Tomlin C.D.S. The Pesticide Manual 2003, British Crop Protection Council, Surrey, UK. 14th edn.
45. Tsatsakis A.M., Tsakiris I.N., Tzatzarakis M.N., Agourakis Z.B., Tutudaki M., Alegakis A.K. Three-year study of fenthion and dimethoate pesticides in olive oil from organic and conventional cultivation. Food Addit. Cont. 2003, 20:553-559.
46. Tsoutsi C.S., Albanis T.A. Optimization of headspace solid-phase microextraction conditions for the determination of organophosphorus insecticides in olive oil. Int. J. Environ. Anal. Chem. 2004, 84:3-13.
47. Yagüe C., Bayarri S., Conchello P., Lazaro R., Perez-Arquillué C., Herrera A., Ariño A. Determination of pesticides and PCBs in virgin olive oil by multicolumn solid-phase extraction cleanup followed by GC-NPD/ECD and confirmation by ion-trap GC-MS. J. Agric. Food Chem. 2005, 53:5105-5109.