On the characterization of environmental nanoparticles

Journal of Environmental Science and Health - Part A Toxic/Hazardous Substances and Environmental Engineering

Volumn 39, Issue 10, 2004, Pages 2707-2753

  Burleson, David J ^a   Driessen, Michelle D ^a   Penn, R Lee ^a  

^a UNIVERSITY OF MINNESOTA   (United States)

Author keywords

Materials characterization; Nanomaterials; Nanoparticles; Particle size; TEM

Indexed keywords

COMPOSITION; ENVIRONMENTAL IMPACT; HEALTH CARE; MICROSTRUCTURE; PARTICLE SIZE ANALYSIS;

ANTHROPOGENY; ENVIRONMENTAL NANOPARTICLES; HUMAN HEALTH;

NANOSTRUCTURED MATERIALS;

NANOPARTICLE;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; CHEMICAL STRUCTURE; DIFFERENTIAL MOBILITY ANALYSIS; ENVIRONMENT; ENVIRONMENTAL IMPACT; IMAGING; MATERIAL STATE; PARTICLE INDUCED X RAY EMISSION; PARTICLE SIZE; PHOTON CORRELATION SPECTROSCOPY; QUANTUM MECHANICS; ROENTGEN SPECTROSCOPY; SCANNING ELECTRON MICROSCOPY; SCANNING PROBE MICROSCOPY; SPECTROSCOPY; STRUCTURE ANALYSIS; TRANSMISSION ELECTRON MICROSCOPY; VIBRATIONAL SPECTROSCOPY; X RAY ABSORPTION SPECTROSCOPY; X RAY DIFFRACTION; X RAY PHOTOELECTRON SPECTROSCOPY;

ENVIRONMENTAL MONITORING; MICROSCOPY, ELECTRON, SCANNING; NANOTECHNOLOGY; PARTICLE SIZE; RISK ASSESSMENT; STRUCTURE-ACTIVITY RELATIONSHIP; X-RAY DIFFRACTION;

EID: 5444253860     PISSN: 10934529     EISSN: None     Source Type: Journal    
DOI: 10.1081/ESE-200027029     Document Type: Article

References (173)

1. Anastasio, C.; Martin, S.T. Atmospheric nanoparticles. Rev. Miner. Geochem. 2001, 44, 293-349.
2. Cass, G.R.; Hughes, L.A.; Bhave, P.; Kleeman, M.J.; Allen, J.O.; Salmon, L.G. The chemical composition of atmospheric ultrafine particles. Philos. Trans. R. Soc. London, Ser. A 2000, 358 (1775), 2581-2592.
3. Banfield, J.F.; Zhang, H. Nanoparticles in the environment. Rev. Miner. Geochem. 2001, 44, 1-58.
4. Cassee, F.R.; Muijser, H.; Duistermaat, E.; Freijer, J.J.; Geerse, K.B.; Marijnissen, J.C.M.; Arts, J.H.E. Particle size-dependent total mass deposition in lungs determines inhalation toxicity of cadmium chloride aerosols in rats. Application of a multiple path dosimetry model. Arch. Toxicol. 2002, 76 (5-6), 277-286.
5. Brown, D.M.; Wilson, M.R.; MacNee, W.; Stone, V.; Donaldson, K. Size-dependent proinflammatory effects of ultrafine polystyrene particles: a role for surface area and oxidative stress in the enhanced activity of ultrafines. Toxicol. Appl. Pharmacol. 2001, 775 (3), 191-199.
6. Anderson, H.R. Differential epidemiology of ambient aerosols. Philos. Trans. R. Soc. London, Ser. A 2000, 358 (1775), 2771-2785.
7. Donaldson, K.; Stone, V.; Clouter, A.; Renwick, L.; MacNee, W. Ultrafine particles. Occup. Environ. Med. 2001, 58 (3), 211-216.
8. Lien, H.L.; Zhang, W.X. Nanoscale iron particles for complete reduction of chlorinated ethenes. Colloid. Surface. A 2001, 191 (1-2), 97-105.
9. Zhang, W.X.; Wang, C.B.; Lien, H.L. Treatment of chlorinated organic contaminants with nanoscale bimetallic particles. Catal. Today 1998, 40 (4), 387-395.
10. Zhang, W.X. Nanoscale iron particles for environmental remediation: an overview. J. Nanopart. Res. 2003, 5 (3-4), 323-332.
11. ATSDR. Toxicological Profile for Chromium; US Department of Health and Human Services, Public Health Service: Atlanta, GA, 2000.
12. Rowbotham, A.L.; Levy, L.S.; Shuker, L.K. Chromium in the environment: an evaluation of exposure of the UK general population and possible adverse health effects. J. Toxicol. Env. Heal. B 2000, 3 (3), 145-178.
13. Murray, C.B.; Kagan, C.R.; Bawendi, M.G: Self-organization of CdSe nanocrystallites into 3-dimensional quantum-dot superlattices. Science 1995, 270 (5240), 1335-1338.
14. Alivisatos, A.P. Semiconductor clusters, nanocrystals, and quantum dots. Science 1996, 277 (5251), 933-937.
15. Alivisatos, A.P. Perspectives on the physical chemistry of semiconductor nanocrystals. J. Phys. Chem. 1996, 100 (31), 13226-13239.
16. Efros, A.L.; Rosen, M. The electronic structure of semiconductor nanocrystals. Annu. Rev. Mater. Sci. 2000, 30, 475-521.
17. Navrotsky, A. Thermochemistry of nanomaterials. Rev. Miner. Geochem. 2001, 44, 73-103.
18. Buffat, P.; Borel, J.P. Size effect on the melting temperature of gold particles. Phys. Rev. A: At. Mol. Opt. Phys. 1976, 13, 2287-2298.
19. Penn, R.L.; Anschutz, A.J.; Burleson, D.; Mostrom, A.P.; Guyodo, Y.; Banerjee, S. Abstracts of Papers, 225th National Meeting of the American Chemical Society, New Orleans, LA, March 23-27, 2003; American Chemical Society: Washington, DC, 2003; GEOC-178.
20. Rao, C.N.R.; Kulkarni, G.U.; Thomas, P.J.; Edwards, P.P. Size-dependent chemistry: properties of nanocrystals. Chem. Eur. J. 2002, 8 (1), 28-35.
21. 2/Si(100): correlation between size, electron structure, and activity in co oxidation. J. Am. Chem. Soc. 2003, 125 (14), 4332-4337.
22. Hochella, M.F.; Banfield, J.F. Chemical Weathering Rates of Silicate Minerals. Reviews in Mineralogy; Mineralogical Society of America: Washington, DC, 1995; Vol. 31, 353-406.
23. Zhang, H.Z.; Gilbert, B.; Huang, F.; Banfield, J.F. Water-driven structure transformation in nanoparticles at room temperature. Nature 2003, 424 (6952), 1025-1029.
24. Penn, R.L.; Burleson, D.J. Two-step growth of goethite nanoparticles from ferrihydrite, in prep.
25. Allen, J.O.; Fergenson, D.P.; Gard, E.E.; Hughes, L.S.; Morrical, B.D.; Kleeman, M.J.; Gross, D.S.; Gaelli, M.E.; Prather, K.A.; Cass, G.R. Particle detection efficiencies of aerosol time of flight mass spectrometers under ambient sampling conditions. Environ. Sci. Technol. 2000, 34 (1), 211-217.
26. Penn, R.L.; Zhu, C.; Xu, H.; Veblen, D.R. Iron oxide coatings on sand grains from the atlantic coastal plain: high-resolution transmission electron microscopy characterization. Geology 2001, 29 (9), 843-846.
27. Williams, D.B.; Carter, C.B. Transmission Electron Microscopy: A Textbook for Materials Science; Plenum Press: New York, 1996.
28. Buseck, P.R.; Cowley, J.M.; Eyring, L. High-Resolution Transmission Electron Microscopy and Associated Techniques; Oxford University Press: New York, 1988.
29. Fultz, B.; Howe, J.M. Transmission Electron Microscopy and Diffractometry of Materials; Spring-Verlag: Berlin, New York, 2001.
30. Wang, Z.L. Transmission electron microscopy of shape-controlled nanocrystals and their assemblies. J. Phys. Chem. B 2000, 104 (6), 1153-1175.
31. Geiss, R.H EDS: Energy-Dispersive X-ray Spectroscopy. In Encyclopedia of Materials Characterization; Brundle, R.C., Evans, C.A., Wilson, S., Eds.; Butterworth-Heinemann: Boston, 1992; 120-134.
32. Joy, D.C.; Alton, D.; Romig, J.; Goldstein, J.I. Principles of Analytical Electron Microscopy; Plenum Press: New York, 1986.
33. Garratt-Reed, A.J.; Bell, D.C. Energy Dispersive X-Ray Analysis in the Electron Microscope; Bios Scientific Publishers, Ltd.: Oxford, U.K., 2003.
34. Egerton, R.F. Electron Energy-Loss Spectroscopy in the Electron Microscope; Plenum Press: New York, 1996.
35. Ahn, C.; Disko, M.; Fultz, B. Transmission Electron Energy Loss Spectrometry in Materials Science; Times of Acadiana Pr Inc., 1992.
36. Lichte, H. Electron image plane off-axis holography of atomic structures. In Advances in Optical and Electron Microscopy; Mulvey, T., Sheppard, C.J.R., Eds.; Academic Press: New York, 1991; Vol. 12, 25.
37. Orchowski, A.; Rau, W.D.; Lichte, H. Electron holography surmounts resolution limit of electron microscopy. Phys. Rev. Lett. 1995, 74, 399-402.
38. Chapman, J.N. The investigation of magnetic domain structures in thin foils by electron microscopy. J. Phys. D: Appl. Phys. 1984, 17, 623-647.
39. Hiemenz, P.C.; Rajagopalan, R. Principles of Colloid and Surface Chemistry, 3rd Ed.; Marcel Dekker: New York, 1997; 566.
40. Park, K. Ph.D thesis, University of Minnesota, Minneapolis, 2003.
41. Delzeit, L.; Blake, D. A characterization of crystalline ice nanoclusters using transmission electron microscopy. J. Geophys. Res. E: Planets 2001, 706 (E12), 33371-33379.
42. Sharma, R. Design and applications of environmental cell transmission electron microscope for in situ observations of gas-solid reactions. Microsc. Microanal. 2001, 7 (6), 494-506.
43. Dragoo, A.L.; Robbins, C.R.; Hsu, S.M. A critical assessment of requirements for ceramic powder characterization. Adv. Ceram. 1987, 21 (Ceram. Powder Sci.), 711-720.
44. Maurice, P.A. Applications of atomic-force microscopy in environmental colloid and surface chemistry. Colloid Surf. A-Physicochem. Eng. Asp. 1996, 707, 57-75.
45. Friedbacher, G.; Fuchs, H. Classification of scanning probe microscopies - (technical report). Pure Appl. Chem. 1999, 71 (7), 1337-1357.
46. Sarid, D. Scanning Force Microscopy: with Applications to Electric, Magnetic and Atomic Forces, Rev. Ed.; Oxford University Press: New York, 1994.
47. Nagy, K.L.; Cygan, R.T.; Hanchar, J.M.; Sturchio, N.C. Gibbsite growth kinetics on gibbsite, kaolinite, and muscovite substrates: atomic force microscopy evidence for epitaxy and an assessment of reactive surface area. Geochim. Cosmochim. Acta 1999, 63 (16), 2337-2351.
48. Sutheimer, S.H.; Maurice, P.A.; Zhou, Q.H. Dissolution of well and poorly crystallized kaolinites: A1 speciation and effects of surface characteristics. Am. Miner. 1999, 84 (4), 620-628.
49. Teng, H.H.; Dove, P.M.; DeYoreo, J.J. Reversed calcite morphologies induced by microscopic growth kinetics: insight into biomineralization. Geochim. Cosmochim. Acta 1999, 63 (17), 2507-42512.
50. Frisbie, C.D.; Rozsnyai, L.F.; Noy, A.; Wrighton, M.S.; Lieber, C.M. Functional group imaging by chemical force microscopy. Science 1994, 265 (5181), 2071-2074.
51. 2 secondary submicroparticles by hydrothermal sol-gel method. Chem. Lett. 2000, (1), 70-71.
52. McRendry, R.; Theoclitou, M.E.; Abell, C.; Rayment, T. How much chemistry is there in chemical force microscopy? Jpn. J. Appl. Phys. Part 1 - Regul. Pap. Short Notes Rev. Pap. 1999, 38 (6B), 3901-3907.
53. Proksch, R.B.; Schaffer, T.E.; Moskowitz, B.M.; Dahlberg, E.D.; Bazylinski, D.A.; Frankel, R.B. Magnetic force microscopy of the submicron magnetic assembly in a magnetotactic bacterium. Appl. Phys. Lett. 1995, 66 (19), 2582-2584.
54. Chen, X.; Davies, M.C.; Roberts, C.J.; Tendler, S.J.B.; Williams, P.M.; Burnham, N.A. Optimizing phase imaging via dynamic force curves. Surf. Sci. 2000, 460 (1-3), 292-300.
55. Wiesendanger, R. Scanning Probe Microscopy Analytical Methods; Springer: Berlin, 1998.
56. Kirstein, S. Scanning near-field optical microscopy. Curr. Opin. Colloid Interface Sci. 1999, 4 (4), 256-264.
57. Heinzelmann, H.; Pohl, D.W. Scanning near-field optical microscopy. Appl. Phys. A 1994, A59 (2), 89-101.
58. Betzig, E.; Trautman, J.K. Near-field optics: microscopy, spectroscopy, and surface modification beyond the diffraction limit. Science 1992, 257 (5067), 189-195.
59. Eggleston, C.M. Scanning Probe Microscopy of Clay Minerals; Clay Minerals Society, 1994; Vol. 7.
60. Bickmore, B.R.; Hochella, M.F.; Bosbach, D.; Charlet, L. Methods for performing atomic force microscopy imaging of clay minerals in aqueous solutions. Clays Clay Miner. 1999, 47 (5), 573-581.
61. Goldstein, J.I.; Newbury, D.E.; Echlin, P.; Joy, D.C.; Romig, A.D., Jr. Scanning Electron Microscopy and X-Ray Microanalysis, 2nd Ed.; Plenum Press: New York, 1992.
62. Newbury, D.E.; Williams, D.B. The electron microscope: the materials characterization tool of the millennium. Acta Metall. 2000, 48 (1), 323-346.
63. Scott, J.H.J. Analytical advances in the sem. Anal. Bioanal. Chem. 2003, 375 (1), 38-40.
64. Maynard, A.D. Overview of methods for analyzing single ultrafine particles. Philos. Trans. R. Soc. London, Ser. A 2000, 358 (1775), 2593-2610.
65. Humphreys, F.J. Grain and subgrain characterization by electron backscatter diffraction. J. Mater. Sci. 2001, 36 (16), 3833-3854.
66. Randle, V.; Caul, M. Representation of electron backscatter diffraction data. Mater. Sci. Technol. 1996, 12 (10), 844-850.
67. Field, D.P. Recent advances in the application of orientation imaging. Ultramicroscopy 1997, 67 (1-4), 1-9.
68. Dingley, D.J.; Randle, V. Microtexture determination by electron back-scatter diffraction. J. Mater. Sci. 1992, 27 (17), 4545-4566.
69. Goetze, J. Potential of cathodoluminescence (cl) microscopy and spectroscopy for the analysis of minerals and materials. Anal. Bioanal. Chem. 2002, 374 (4), 703-708.
70. Petruk, W. Imaging of minerals, ores and related products to determine mineral characteristics. Miner. Metall. Process 2002, 19 (1), 50-56.
71. Strausser, Y.E. AES: Auger Electron Spectroscopy. In Encyclopedia of Materials Characterization; Brundle, R.C., Evans, C.A., Wilson, S., Eds.; Butterworth-Heinemann: Boston, 1992; 310-323.
72. Berube, K.A.; Jones, T.P.; Williamson, B.J.; Winters, C.; Morgan, A.J.; Richards, R.J. Physicochemical characterization of diesel exhaust particles: factors for assessing biological activity. Atmos. Environ. 1999, 33 (10), 1599-1614.
73. Ebert, M.; Inerle-Hof, M.; Weinbruch, S. Environmental scanning electron microscopy as a new technique to determine the hygroscopic behaviour of individual aerosol particles. Atmos. Environ. 2002, 36 (39-40), 5909-5916.
74. Schleicher, B.; Tapper, U.; Kauppinen, E.I.; Martin, M.; Roschier, L.; Paalanen, M.; Wernsdorfer, W.; Benoit, A. Magnetization reversal measurements of size-selected iron oxide particles produced via an aerosol route. Appl. Organomet. Chem. 1998, 12 (5), 315-320.
75. Weinbruch, S.; van Aken, P.; Ebert, M.; Thomassen, Y.; Skogstad, A.; Chashchin, V.P.; Nikonov, A. The heterogeneous composition of working place aerosols in a nickel refinery: a transmission and scanning electron microscope study. J. Environ. Monit. 2002, 4 (3), 344-350.
76. Laskin, A.; Cowin, J.P. Automated single-particle SEM/EDX analysis of submicrometer particles down to 0.1 mm. Anal. Chem. 2001, 73 (5), 1023-1029.
77. Kasparian, J.; Frejafon, E.; Rambaldi, P.; Yu, J.; Vezin, B.; Wolf, J.P.; Ritter, P.; Viscardi, P. Characterization of urban aerosols using sem-microscopy, X-ray analysis and lidar measurements. Atmos. Environ. 1998, 32 (17), 2957-2967.
78. Swietlicki, E.; Martinsson, B.G.; Kristiansson, P. The use of PIXE and complementary ion beam analytical techniques for studies of atmospheric aerosols. Nucl. Instrum. Methods Phys. Res., Sect. B 1996, 109/110, 385-394.
79. Johansson, S.A.E.; Campbell, J.L.; Malmqvist, K.G. Particle-Induced X-Ray Emission Spectroscopy (Pixe). In Chemical Analysis; Winefordner, J.D., Ed.; John Wiley & Sons, Inc.: New York, 1995; Vol. 133.
80. Miranda, J. Studies of atmospheric aerosols in large urban areas using pixe: an overview. Nucl. Instrum. Methods Phys. Res., Sect. B 1996, 109/110, 439-444.
81. Maenhaut, W.; Cafmeyer, J. Long-term atmospheric aerosol study at urban and rural sites in belgium using multi-elemental analysis by particle-enduced X-ray emission spectrometry and short-irradiation instrumental neutron activation analysis. X-Ray Spectrom. 1998, 27 (4), 236-246.
82. Malmqvist, K.G. Particle-induced X-ray emission - a quantitative technique suitable for microanalysis. Mikrochim. Act. Suppl. 1996, 13 (Microbeam and Nanobeam Analysis), 117-133.
83. Malmqvist, K. The nuclear, microprobe - Advances in micro PIXE and complementary techniques. X-Ray Spectrom. 1995, 24 (5), 226-234.
84. Campbell, J.L.; Higuchi, D.; Maxwell, J.A.; Teesdale, W.J. Quantitative PIXE microanalysis of thick specimens. Nucl. Instrum. Methods Phys. Res., Sect. B 1993, B77 (1-4), 95-109.
85. Maura de Miranda, R.; Andrade, M.D.F.; Worobiec, A.; van Grieken, R. Characterisation of aerosol particles in the Sao Paulo metropolitan area. Atmos. Environ. 2002, 36 (2), 345-352.
86. Salma, I.; Maenhaut, W.; Zaray, G. Comparative study of elemental mass size distributions in urban atmospheric aerosol. J. Aerosol Sci. 2001, 33 (2), 339-356.
87. Eleftheriadis, K.; Colbeck, I. Coarse atmospheric aerosol: size distributions of trace elements. Atmos. Environ. 2001, 35 (31), 5321-5330.
88. Briggs, D.; Seah, M.P. Practical Surface Analysis, 2nd Ed.; John Wiley & Sons: Chichester, 1992; Vol. 1 - Auger and X-ray Photoelectron Spectroscopy.
89. Anschutz, A.J.; Penn, R.L. Reduction of crystalline iron(III) oxyhydroxides using hydroquinone: influence of phase and particle size, in prep.
90. Gunther, S.; Kaulich, B.; Gregoratti, L.; Kiskinova, M. Photoelectron microscopy and applications in surface and materials science. Progress in Surface Science 2002, 70 (4-8), 187-260.
91. Hoenig, M. Preparation steps in environmental trace element analysis-facts and traps. Talanta 2001, 54, 1021-1038.
92. Ford, R.G. Rates of hydrous ferric oxide crystallization and the influence on coprecipitated arsenate. Environ. Sci. Technol. 2002, 36, 2459-2463.
93. Ford, R.G.; Kemner, K.M.; Bertsch, P.M. Influence of sorbate-sorbent interactions on the crystallization kinetics of nickel- and lead-ferrihydrite coprecipitates. Geochim. Cosmochim. Acta 1999, 63 (1), 39-48.
94. Cornell, R.M.; Schneider, W. Formation of goethite from ferrihydrite at physiological pH under the influence of cysteine. Polyhedron 1989, 8 (2), 149-155.
95. Van Loon, J.C. Analytical Atomic Absorption Spectroscopy: Selected Methods; Academic Press: New York, 1980.
96. Welz, B.; Sperling, M. Atomic Absorption Spectrometry, 3rd Ed.; Wiley-VCH: Weinheim, 1999.
97. Balaram, V. Recent trends in the inorganic analysis of environmental materials. Res. J. Chem. Environ. 2002, 6 (2), 69-79.
98. Taylor, V.F.; Toms, A.; Longerich, H.P. Acid digestion of geological and environmental samples using open-vessel focused microwave digestion. Anal. Bioanal. Chem. 2002, 372, 360-365.
99. Ridley, I.W. The ICP-MS laser microprobe: a new geochemical tool. Trends in Geochemistry 2000, 1, 1-14.
100. Hill, S.J.; Arowolo, T.A.; Butler, O.T.; Cook, J.M.; Cresser, M.S.; Harrington, C.; Miles, D.L. Atomic spectrometry update. Environmental analysis. J. Anal. At. Spectrom. 2003, 18, 170-202.
101. Kurfurst, U. Solid Sample Analysis; Springer-Verlag: Berlin Heidelberg, 1998.
102. Dean, J.R. Atomic Absorption and Plasma Spectroscopy, 2nd Ed.; John Wiley & Sons: Chichester, 1997.
103. Ebdon, L.; Evans, E.H.; Fisher, A.; Hill, S.J. An Introduction to Analytical Atomic Spectrometry; John Wiley & Sons: Chichester, 1998.
104. Jarvis, K.E.; Gray, A.L.; Houk, R.S. Handbook of Inductively Coupled Plasma Mass Spectrometry; Blackie: Glasgow & London, 1992.
105. Gomez, D.; Smichowski, P.; Polla, G.; Ledesma, A.; Resnizky, S.; Rosa, S. Fractionation of elements by particle size of ashes ejected from copahue volcano, argentina. J. Environ. Monit. 2002, 4, 972-977.
106. Skoog, D.A.; Holler, F.J.; Nieman, T.A. Principles of Instrumental Analysis, 5th Ed.; Brooks/Cole, 1997.
107. Cullity, B.D.; Stock, S.R. Elements of X-Ray Diffraction, 3rd Ed.; Prentice Hall: Upper Saddle River, 2001.
108. Toney, M.F. XRD: X-ray diffraction. In Encyclopedia of Materials Characterization; Brundle, R.C., Evans, C.A., Wilson, S., Eds.; Butterworth-Heinemann: Boston, 1992; 198-213.
109. Huber, C. X-ray diffraction characterization of nanophase materials. In Handbook of Nanophase Materials; Goldstein, A.N., Ed.; Marcel Dekker: New York, 1997; 317-336.
110. Tarassov, M.; Mihailova, B.; Tarassova, E.; Konstantinov, L. Chemical composition and vibrational spectra of tungsten-bearing goethite and hematite from western rhodopes, Bulgaria. Eur. J. Mineral. 2002, 14, 977-986.
111. Matyi, R.J.; Schwart, L.H.; Butt, J.B. Partice size, particle size distribution, and related measurements of supported metal catalysts. Cat. Rev. -Sci. Eng. 1987, 29, 41-99.
112. Zanchet, D.; Hall, B.D.; Ugarte, D. X-ray characterization of nanoparticles. In Characterization of Nanophase Materials; Wang, Z.L., Ed.; Wiley-VCH: Weinheim, New York, 2000; 13-36.
113. Davis, B.L.; Jenkins, R.; McCarthy, G.J.; Smith, D.K.; Wong-Ng, W. Specimen preparation in X-ray diffraction. In A Practical Guide for the Preparation of Specimens for X-Ray Fluorescence and X-Ray Diffraction Analysis; Buhrke, V.E., Jenkins, R., Smith, D.K., Eds.; John Wiley & Sons: New York, 1998; 123-170.
114. Blanton, T.N.; Hamilton, R.F.; Iyenger, S.S.; Jenkins, R.; McMurdie, H.F.; Nelson, D.E.; Rasmussen, S.E.; Rendle, D.F.; Roach, G.I.D.; Ryba, E.R.; Smith, D.K.; Wong-Ng, W. Specific areas of specimen preparation in X-ray powder diffraction. In A Practical Guide for the Preparation of Specimens for X-Ray Fluorescence and X-Ray Diffraction Analysis; Buhrke, V.E., Jenkins, R., Smith, D.K., Eds.; John Wiley & Sons: New York, 1998; 171-216.
115. Antonio, M.R. EXAFS: Extended X-ray absorption fine structure. In Encyclopedia of Materials Characterization; Brundle, R.C., Evans, C.A., Wilson, S., Eds.; Butterworth-Heinemann: Boston, 1992; 214-226.
116. Fendorf, S.E.; Sparks, D.L.; Lamble, G.M.; Kelley, M.J. Applications of X-ray adsorption fine-structure spectroscopy to soils. Soil Sci. Soc. Am. J. 1994, 55, 1583-1595.
117. Waychunas, G.A. Structure, aggregation and characterization of nanoparticles. In Nanoparticles and the Environment; Banfield, J.F., Navrotsky, A., Eds.; Mineralogical Society of America: Washington, D.C., 2001; Vol. 44, 105-166.
118. Waychunas, G.A.; Fuller, C.C.; Davis, J.A. Surface complexation and precipitate geometry for aqueous Zn(II) sorption on ferrihydrite I: X-ray absorption extended fine structure spectroscopy analysis. Geochim. Cosmochim. Acta 2002, 66 (7), 1119-1137.
119. Waychunas, G.A.; Fuller, C.C.; Rea, B.A.; Davis, J.A. Wide angle X-ray scattering (WAXS) study of "two-line" ferrihydrite structure: effect of arsenate sorption and counterion variation and comparison with EXAFE results. Geochim. Cosmochim. Acta 1996, 60 (40), 1765-1781.
120. 2+ incorporated at the calcite surface. An X-ray standing wave and sexafs study. Phys. Rev. B: Condens. Matter 2000, 61 (7), 4877-4883.
121. Lagarde, P. Surface X-ray absorption spectroscopy principles and some examples of applications. Ultramicroscopy 2001, 86 (3/4), 255-263.
122. Norman, D. SEXAFS/NEXAFS: Surface Extended X-Ray Absorption Fine Structure and Near Edge X-Ray Absorption Fine Structure. In Encyclopedia of Materials Characterization; Brundle, R.C., Evans, C.A., Wilson, S., Eds.; Butterworth-Heinemann: Boston, 1992; 227-239.
123. Stor, J. SEXAFS: Everything You Always Wanted to Know about SEXAFS but Were Afraid to Ask. In X-Ray Absorption: Principles, Applications Techniques of EXAFS, SEXAFS and XANES; Koningsberger, D.C., Prins, R., Eds.; John Wiley & Sons: New York, 1988; Vol. 92, 443-572.
124. Ingle, J., James D.; Crouch, S. Spectrochemical Analysis; Prentice-Hall: Upper Saddle River, NJ, 1988.
125. Schwertmann, U.; Friedl, J.; Stanjek, H.; Murad, E.; Bender Koch, C. Iron oxides and smectites in sediments from the Atlantis II deep, red sea. Eur. J. Mineral. 1998, 10 (5), 953-967.
126. Woolridge, M.S.; Danczyk, S.A.; Wu, J. Demonstration of gas-phase combustion synthesis of nanosized particles using a hybrid burner. Nanostruct. Mater. 1999, 11 (7), 955-964.
127. Lyon, L.A.; Keating, C.D.; Fox, A.P.; Baker, B.E.; He, L.; Nicewarner, S.R.; Mulvaney, S.P.; Natan, M.J. Raman spectroscopy. Anal. Chem. 1998, 70, 341R-361R.
128. Pelletier, M.J. Analytical Applications of Raman Spectroscopy; Blackwell Science: Oxford, 1999.
129. Weber, W.H.; Merlin, R. Raman Scattering in Materials Science; Springer-Verlag: Berlin, 2000.
130. Mulvaney, S.P.; Keating, C.D. Raman spectroscopy. Anal. Chem. 2000, 72, 145R-157R.
131. de Faria, D.L.A.; Silva, S.V.; de Oliveira, M.T. Raman microspectroscopy of some iron oxides and oxyhydroxides. J. Raman Spectrosc. 1997, 28, 873-878.
132. 2 and ZnO: influence of trichloroethylene pressure, oxygen pressure, and the photocatalyst surface on the product distribution. J. Phys. Chem. B 1998, 702 (3), 549-556.
133. 2. J. Phys. Chem. 1995, 99 (45), 16519-16522.
134. Driessen, M.D.; Grassian, V.H. A comprehensive study of the reactions of methyl fragments from methyl iodide dissociation on reduced and oxidized silica-supported copper nanoparticles. J. Am. Chem. Soc. 1997, 119 (7), 1697-1707.
135. 4 by high surface-area aluminum oxide. Environ. Sci. Technol. 2002, 36 (7), 1620-1624.
136. Rancourt, D.G. Magnetism of Earth, Planetary, and Environmental Nanomaterials. In Nanoparticles and the Environment; Banfield, J.F., Navrotsky, A., Eds.; Mineralogical Society of America: Washington, D.C., 2001; Vol. 44, 217-292.
137. Sorenson, C.M. Magnetism. In Nanoscale Materials in Chemistry; Klabunde, K.J., Ed.; John Wiley & Sons, Inc.: New York, 2001; 169-221.
138. Mulay, L.N.; Mulay, I.L. Magnetometry: instrumentation and analytical applications including catalysis, bioscience, geoscience, and amorphous materials. Anal. Chem. 1982, 54, 216R-227R.
139. Kopcewicz, B.; Kopcewicz, M. Mossbauer study of the structure of iron-containing atmospheric aerosols. In Analytical Chemistry of Aerosols; Spurny, K.R., Ed.; Lewis Publishers, CRC, Press LLC: Boca Raton, 1999; 185-196.
140. Stevens, J.G.; Bowen, L.H. Mossbauer spectroscopy. Anal. Chem. 1984, 56, 199R-212R.
141. Dollimore, D.; Spooner, P.; Turner, A. The BET method of analysis of gas adsorption data and its relevance to the calculation of surface areas. Surf. Technol. 1976, 4 (2), 121-160.
142. Brunauer, S.; Emmett, P.H.; Teller, E. Adsorption of gases in multimolecular layers. J. Am. Chem. Soc. 1938, 60, 309-319.
143. 2 nanoparticles. J. Solid State Chem. 2003, 174 (2), 241-248.
144. 3 powders during g- to a-phase transformation. Nano Lett. 2002, 2 (3), 245-252.
145. Mogyorosi, K.; Dekany, I.; Pendler, J.H. Preparation and characterization of clay mineral intercalated titanium dioxide nanoparticles. Langmuir 2003, 19 (7), 2938-2946.
146. Muller, R.H.; Mehnert, W. Particle and Surface Characterisation Methods; Medpharm Scientific Publishers: Stuttgart, 1997.
147. De Jaeger, N.; Demeyere, H.; Finsy, R.; Sneyers, R.; Vanderdeelen, J.; Van der Meeren, P.; Van Laethem, M. Particle sizing by photon correlation spectroscopy. Part I. Monodisperse latices: influence of scattering angle and concentration of dispersed material. Part. Part. Syst. Char. 1991, 8 (3), 179-186.
148. Finsy, R.; De Jaeger, N. Particle sizing by photon correlation spectroscopy. Part II. Average values. Part. Part. Syst. Char. 1991, 8 (3), 187-193.
149. Finsy, R.; De Jaeger, N.; Sneyers, R.; Gelade, E. Particle sizing by photon correlation spectroscopy. Part III. Mono and bimodal distributions and data analysis. Part. Part. Syst. Char. 1992, 9 (2), 125-137.
150. Finsy, R. Particle sizing by quasi-elastic light scattering. Adv. Colloid Interface Sci. 1994, 52, 79-143.
151. Chu, B.; Liu, T. Characterization of nanoparticles by scattering techniques. J. Nanopart. Res. 2000, 2 (1), 29-41.
152. Cecere, D.; Bruno, A.; Minutolo, P.; D'Alessio, A. DLS measurements on nanoparticles produced in laminar premixed flames. Synth. Met. 2003, 139 (3), 653-656.
153. Sipos, P.; Berkesi, O.; Tombiez, E.; St. Pierre, T.G.; Webb, J. Formation of spherical iron(III) oxyhydroxide nanoparticles sterically stabilized by chitosan in aqueous solutions. J. Inorg. Biochem. 2003, 95 (1), 55-63.
154. Jeevanandam, P.; Klabunde, K.J. Redispersion and reactivity studies on surfactant-coated magnesium oxide nanoparticles. Langmuir 2003, 19 (13), 5491-5495.
155. Fergenson, D.P.; Song, X.-H.; Ramadan, Z.; Allen, J.O.; Hughes, L.S.; Cass, G.R.; Hopke, P.K.; Prather, K.A. Quantification of ATOFMS data by multivariate methods. Anal. Chem. 2001, 73 (15), 3535-3541.
156. Gard, E.; Mayer, J.E.; Morrical, B.D.; Dienes, T.; Fergenson, D.P.; Prather, K.A. Real-time analysis of individual atmospheric aerosol particles: design and performance of a portable atofms. Anal. Chem. 1997, 69 (20), 4083-4091.
157. Hughes, L.S.; Allen, J.O.; Kleeman, M.J.; Johnson, R.J.; Cass, G.R.; Gross, D.S.; Gard, E.E.; Gaelli, M.E.; Morrical, B.D.; Fergenson, D.P.; Dienes, T.; Noble, C.A.; Liu, D.-Y.; Silva, P.J.; Prather, K.A. Size and composition distribution of atmospheric particles in southern California. Environ. Sci. Technol. 1999, 33 (20), 3506-3515.
158. Galli, M.; Guazzotti, S.A.; Prather, K.A. Improved lower particle size limit for aerosol time-of-flight mass spectrometry. Aerosol Sci. Technol. 2001, 34 (4), 381-385.
159. Gard, E.E.; Kleeman, M.J.; Gross, D.S.; Hughes, L.S.; Allen, J.O.; Morrical, B.D.; Fergenson, D.P.; Dienes, T.; Galli, M.E.; Johnson, R.J.; Cass, G.R.; Prather, K.A. Direct observation of heterogeneous chemistry in the atmosphere. Science 1998, 279 (5354), 1184-1187.
160. Gross, D.S.; Warren, B.S.; Barron, A.R.; Liu, D.-Y.; Wenzel, R.J.; Prather, K.A. Book of Abstracts, 219th ACS National Meeting, San Francisco, CA, March 26-30, 2000; CHED-237.
161. Liu, D.-Y.; Wenzel, R.J.; Prather, K.A. Aerosol time-of-flight mass spectrometry during the atlanta supersite experiment: 1. Measurements. J. Geophys. Res. D: Atmos. 2003, 108 (D7), SOS 14/1-SOS 14/16.
162. Middlebrook, A.M.; Murphy, D.M.; Lee, S.-H.; Thomson, D.S.; Prather, K.A.; Wenzel, R.J.; Liu, D.-Y.; Phares, D.J.; Rhoads, K.P.; Wexler, A.S.; Johnston, M.V.; Jimenez, J.L.; Jayne, J.T.; Worsnop, D.R.; Yourshaw, I.; Seinfeld, J.H.; Flagan, R.C. A comparison of particle mass spectrometers during the 1999 Atlanta supersite project. J. Geophys. Res. D: Atmos. 2003, 108 (D7), SOS 12/1-SOS 12/13.
163. Wenzel, R.J.; Liu, D.-Y.; Edgerton, E.S.; Prather, K.A. Aerosol time-of-flight mass spectrometry during the Atlanta supersite experiment: 2. Scaling procedures. J. Geophys. Res. D: Atmos. 2003, 108 (D7), SOS 15/1-SOS 15/8.
164. Knutson, E.O.; Whitby, K.T. Aerosol classification by electric mobility: apparatus, theory, and applications. J. Aerosol Sci. 1975, 6 (6), 443-451.
165. Hinds, W.C. Aerosol Technology: Properties, Behavior, and Measurement of Airborne Particles, 2nd Ed.; John Wiley & Sons, Inc.: New York, 1999.
166. Friedlander, S.K. Smoke, Dust, and Haze, 2nd Ed.; Oxford University Press: New York, 2000.
167. Weber, A.P.; Baltensperger, U.; Gaeggeler, H.W.; Schmidt-Ott, A. In situ characterization and structure modification of agglomerated aerosol particles. J. Aerosol Sci. 1996, 27 (6), 915-929.
168. Tobias, H.J.; Beving, D.E.; Ziemann, P.J.; Sakurai, H.; Zuk, M.; McMurry, P.H.; Zarling, D.; Waytulonis, R.; Kittelson, D.B. Chemical analysis of diesel engine nanoparticles using a nano-dma/thermal desorption particle beam mass spectrometer. Environ. Sci. Technol. 2001, 35 (11), 2233-2243.
169. Higgins, K.J.; Jung, H.; Kittelson, D.B.; Roberts, J.T.; Zachariah, M.R. Kinetics of diesel nanoparticle oxidation. Environ. Sci. Technol. 2003, 37 (9), 1949-1954.
170. 2 addition to diesel engine exhaust gas and its effect on particles. J. Aerosol Sci. 2000, 31 (4), 415-426.
171. McMurry, P.H.; Litchy, M.; Huang, P.-F.; Cai, X.; Turpin, B.J.; Dick, W.D.; Hanson, A. Elemental composition and morphology of individual particles separated by size and hygroscopicity with the TDMA. Atmos. Environ. 1996, 30 (1), 101-108.
172. Rader, D.J.; McMurry, P.H. Application of the tandem differential mobility analyzer to studies of droplet growth or evaporation. J. Aerosol Sci. 1986, 17 (5), 771-787.
173. Higgins, K.J.; Jung, H.; Kittelson, D.B.; Roberts, J.T.; Zachariah, M.R. Size-selected nanoparticle chemistry: kinetics of soot oxidation. J. Phys. Chem. A 2002, 106 (1), 96-103.