Analysis of Ochratoxin A in Wine by High-Resolution UHPLC-MS

Food Analytical Methods

Volumn 5, Issue 6, 2012, Pages 1506-1513

  Li, Jianhui ^a   Liu, Xin ^a   Han, Shen ^a   Li, Jing ^a   Xu, Qin ^b   Xu, Hong ^c   Wang, Yongwei ^d   Liu, Fei ^d   Zhang, Zhaohui ^a  

^a Beijing Entry Exit Inspection and Quarantine Bureau   (China)

^b Shandong Entry Exit Inspection and Quarantine Bureau   (China)

^c Tianjin Entry Exit Inspection and Quarantine Bureau   (China)

^d Thermo Fisher Scientific   (United States)

Author keywords

HCD; LTQ Orbitrap XL; Ochratoxin A; UHPLC Orbitrap MS; Wine

Indexed keywords

CONCENTRATION LEVELS; FOURIER TRANSFORM MASS SPECTROMETERS; HCD; HIGH RESOLUTION; IONIZATION MODES; LIMIT OF DETECTION; LIMIT OF QUANTIFICATIONS; LTQ-ORBITRAP XL; OCHRATOXIN A; ORBITRAP MS; PACKED COLUMN; PHASE EXTRACTION; RED WINE; SPIKED SAMPLES; UHPLC-ORBITRAP MS; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; WHITE WINES;

LIQUID CHROMATOGRAPHY; RECOVERY;

WINE;

EID: 84867670632     PISSN: 19369751     EISSN: 1936976X     Source Type: Journal    
DOI: 10.1007/s12161-012-9403-9     Document Type: Article

References (36)

1. Alvito PC, Sizoo EA, Almeida CMM, van Egmond JP (2010) Occurrence of aflatoxins and ochratoxin A in baby foods in Portugal. Food Anal Methods 3: 22.
2. AOAC (1995) Official Methods of Analysis of AOAC International. 16th edition. Arlington, VA, USA, AOAC International. 973. 37: 37.
3. Aresta A, Vatinno R, Palmisano F, Zambonin CG (2006) Determination of ochratoxin A in wine at sub ng/mL levels by solid-phase microextraction coupled to liquid chromatography with fluorescence detection. J Chromatogr A 1115: 196.
4. Blesa J, Soriano JM, Molto JC, Manes J (2004) Concentration of ochratoxin A in wines from supermarkets and stores of Valencian Community (Spain). J Chromatogr A 1054: 397.
5. Brera C, Soriano JM, Debegnach F, Miraglia M (2005) Exposure assessment to ochratoxin A from the consumption of Italian and Hungarian wines. Microchem J 79: 109.
6. European Union (2009) Method validation and quality control procedures for pesticide residues analysis in food and feed. Document No. SANCO/10684/2009. 18.
7. European Union (2002) Implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Commission Decision 657/2002/EC. Off J Eur Union L 221: 8.
8. European Union (2006) Setting maximum levels for certain contaminants in foodstuffs. Commission Regulation 1881/2006/EC. Off J Eur Union L 364: 5.
9. Folloni S, Bellocchi G, Kagkli DM, Pastor-Benito S, Aguilera M, Mazzeo A, Querci M, van den Eede G, Ermolli M (2011) Development of an ELISA reverse-based assay to assess the presence of mycotoxins in cereal flour. Food Anal Methods 4: 221.
10. Herebian D, Zuhlke S, Lamshoft M, Spiteller M (2009) Multi-mycotoxin analysis in complex biological matrices using LC-ESI/MS: Experimental study using triple stage quadrupole and LTQ-Orbitrap. J Sep Sci 32: 939.
11. Hernandez MJ, Garcia-Moreno MV, Duran E, Guillen D, Barroso CG (2006) Validation of two analytical methods for the determination of ochratoxin A by reversed-phased high-performance liquid chromatography coupled to fluorescence detection in musts and sweet wines from Andalusia. Anal Chim Acta 566: 117.
12. Hussein HS, Brasel JM (2001) Toxicity, metabolism, and impact of mycotoxins on humans and animals. Toxicology 167: 101.
13. JECFA (2001) Safety Evaluation of Certain Mycotoxins in Food: Fifty-sixth report of the Joint FAO/WHO Expert Committee on Food Additives. WHO technical report series no. 906. World Health Organization, Geneva.
14. Jornet D, Busto O, Guasch J (2000) Solid-phase extraction applied to the determination of ochratoxin A in wines by reversed-phase high-performance liquid chromatography. J Chromatogr A 882: 29.
15. Juan C, Lino CM, Pena A, Molto JC, Manes J, Silveira I (2007) Determination of ochratoxin A in maize bread samples by LC with fluorescence detection. Talanta 73: 246.
16. Kokkonen MK, Jestoi MN (2009) A multi-compound LC-MS/MS method for the screening of mycotoxins in grains. Food Anal Methods 2: 128.
17. Lee HB, Magan N (2000) Impact of environment and interspecific interactions between spoilage fungi and Aspergillus ochraceus on growth and ochratoxin production in maize grain. Int J Food Microbiol 61: 11.
18. Leitner A, Zollner P, Paolillo A, Stroka J, Papadopoulou-Bouraoui A, Jaborek S, Anklam E, Lindner W (2002) Comparison of methods for the determination of ochratoxin A in wine. Anal Chim Acta 453: 33.
19. Li J, Xie H, Yang B, Dong X, Feng L, Chen F, Jiang Y (2010) A comparative identification of ochratoxin A in longan fruit pulp by high performance liquid chromatography-fluorescence detection and electron spray ionization-mass spectrometry. Molecules 15: 680.
20. Liu X, Yang JL, Li JH, Li XL, Li J, Lu XY, Shen JZ, Wang YW, Zhang ZH (2011) Analysis of water-soluble azo dyes in soft drinks by high resolution UPLC-MS. Food Addit Contam A 28: 1315.
21. Maier NM, Buttinger G, Welhartizki S, Gavioli E, Lindner W (2004) Molecularly imprinted polymer-assisted sample clean-up of ochratoxin A from red wine: merits and limitations. J Chromatogr B 804: 103.
22. Markaki P, Delpont-Binet C, Grosso F, Dragacci S (2001) Determination of ochratoxin A in red wine and vinegar by immunoaffinity high-pressure liquid chromatography. J Food Prot 64: 533.
23. Nielen MW, van Engelen MC, Zuiderent R, Ramaker R (2007) Screening and confirmation criteria for hormone residue analysis using liquid chromatography accurate mass time-of-flight, fourier transform ion cyclotron resonance and orbitrap mass spectrometry techniques. Anal Chim Acta 586: 122.
24. Pitt JJ (2009) Principles and applications of liquid chromatography-mass spectrometry in clinical biochemistry. Clin Biochem Rev 30: 19.
25. Pohland AE, Schuller PL, Steyn PS, van Egmond HP (1982) Physicochemical data for some selected mycotoxins. Pure Appl Chem 54: 2219.
26. Ramos AJ, Labernia N, Marin S, Sanchis V, Magan N (1998) Effect of water activity and temperature on growth and ochratoxin production by three strains of Aspergillus ochraceus on a barley extract medium and on barley grains. Int J Food Microbiol 44: 133.
27. Serra R, Mendonça C, Abrunhosa L, Pietri A, Venâncio A (2004) Determination of ochratoxin A in wine grapes: comparison of extraction procedures and method validation. Anal Chim Acta 513: 41.
28. Skrabáková Z, O'Halloran J, van Pelt FNAM, James KJ (2010) Food contaminant analysis at ultra-high mass resolution: application of hybrid linear ion trap-orbitrap mass spectrometry for the determination of the polyether toxins, azaspiracids, in shellfish. Rapid Commun Mass Spectrom 24: 2966.
29. Soleas GJ, Yan J, Goldberg DM (2001) Assay of ochratoxin A in wine and beer by high-pressure liquid chromatography photodiode array and gas chromatography mass selective detection. J Agric Food Chem 49: 2733.
30. Studer-Rohr I, Dietrich DR, Schlatter J, Schlatter C (1995) The occurrence of ochratoxin A in coffee. Food Chem Toxicol 33: 341.
31. van der Heeft E, Bolck YJC, Beumer B, Nijrolder AWJM, Stolker AAM, Nielen MWF (2009) Full-scan accurate mass selectivity of ultra-performance liquid chromatography combined with time-of-flight and orbitrap mass spectrometry in hormone and veterinary drug residue analysis. J Am Soc Mass Spectrom 20: 451.
32. Var I, Kabak B (2007) Occurrence of ochratoxin A in Turkish wines. Microchem J 86: 241.
33. Visconti A, Pascale M, Centonze G (1999) Determination of ochratoxin A in wine by means of immunoaffinity column clean-up and high-performance liquid chromatography. J Chromatogr A 864: 89.
34. Zain ME (2011) Impact of mycotoxins on humans and animals. J Saudi Chem Soc 15: 129.
35. Zimmerli B, Dick R (1996) Ochratoxin A in table wine and grape-juice: Occurrence and risk assessment. Food Addit Contam 13: 655.
36. Zöllner P, Leitner A, Lubda D, Cabrera K, Lidner W (2000) Application of a chromolith speedROD RP-18e HPLC column: Determination of ochratoxin A in different wines by high-performance liquid chromatography-tandem mass spectrometry. Chromatographia 52: 818.