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2 and filtered to remove AgCl, and the filtrate was dried under reduced pressure to afford pure product.
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91
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For an example describing α-hydrogen abstraction stemming from a five-coordinate complex see: Schrock, R. R.; Murdzek, J. S.; Bazan, G. C.; Robbins, J.; DiMare, M.; O'Regan, M. J. Am. Chem. Soc. 1990, 112, 3875-3886.
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6e was used as the alkylating reagent.
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97
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