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The byproducts are 4-methoxybenzoic acid and 4-methoxybenzyl 4-methoxybenzoate.
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81
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33845187927
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note
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1H NMR analysis, and then purified by flash chromatography (n-pentane/diethyl ether = 8:1) to afford 4-methoxybenzaldehyde (colorless oil, 247 mg, yield 91%).
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note
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6 is immiscible with n-pentane.
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