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X-ray adsorption spectra were recorded at the beam line O1B1 station attached to the Si(311) monochromator at SPring-8 of JASRI, Harima, Japan (prop. No. 2000A0278-NX-np). The detailed procedures for data analysis are described elsewhere: Tanaka, T.; Yamashita, H.; Tsuchitani, R.; Funabiki, T.; Yoshida, S. J. Chem. Soc., Faraday Trans. 1988, 84, 2987.
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0001694565
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2 (R = 1.96 Å), and the Ru-Cl distance of 2.32 Å is close to that found in monochlororuthenium complexes: Joslin, F. L.; Mague, J. T.; Roundhill, D. M. Organometallics 1991, 10, 521.
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19
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0343052158
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note
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When the reaction temperature was raised from 60 to 80 °C, 1-octanoic acid was obtained in 82% yield for 6 h without formation of the corresponding aldehyde.
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20
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0000654853
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2 in the reaction medium could not be detected: Bilgrien, C.; Davis, S.; Drago, R. S. J. Am. Chem. Soc. 1987, 109, 3786.
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