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Ahmad, M.U., Xu, X., Polar lipids, biology, chemistry, and technology. 2015, AOCS Press, Urbana IL.
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On the combined application of iatroscan TLC-FID and GC-FID to identify total, neutral, and polar lipids and their fatty acids extracted from foods
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Article ID 859024
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Sinanoglou, V.J., Strati, I.F., Bratakos, S.M., Proestos, C., Zoumpoulakis, P., Miniadis-Meimaroglou, S., On the combined application of iatroscan TLC-FID and GC-FID to identify total, neutral, and polar lipids and their fatty acids extracted from foods. ISRN Chromatography, 2013, 10.1155/2013/859024 Article ID 859024.
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ISRN Chromatography
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Sinanoglou, V.J.1
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Comparison between charged aerosol detection and light scattering detection for the analysis of Leishmania membrane phospholipids
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This is a thorough report on the comparison of these two common mass detectors for polar lipids. Detector sensitivity and response for various types of phospholipids are described.
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Ramos, R.G., Libong, D., Rakotomanga, M., Gaudin, K., Loiseau, P.M., Chaminade, P., Comparison between charged aerosol detection and light scattering detection for the analysis of Leishmania membrane phospholipids. J Chromatogr A 1209 (2008), 88–94 This is a thorough report on the comparison of these two common mass detectors for polar lipids. Detector sensitivity and response for various types of phospholipids are described.
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Hazotte, A., Libong, D., Matoga, M., Chaminade, P., Comparison of universal detectors for high-temperature micro liquid chromatography. J Chromatogr A 1170 (2007), 52–61.
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A new liquid chromatography method with charge aerosol detector (CAD) for the determination of phospholipid classes. Application to milk phospholipids
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Kielbowicz, G., Micek, P., Wawrzenczyk, C., A new liquid chromatography method with charge aerosol detector (CAD) for the determination of phospholipid classes. Application to milk phospholipids. Talanta 105 (2013), 28–33.
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Kielbowicz, G.1
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Comparison of dairy phospholipid preparative extraction protocols in combination with analysis by high performance liquid chromatography coupled to a charged aerosol detector
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Barry, K.M., Dinan, T.G., Murray, B.A., Kelly, P.M., Comparison of dairy phospholipid preparative extraction protocols in combination with analysis by high performance liquid chromatography coupled to a charged aerosol detector. Int Dairy J 56 (2016), 179–185.
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Barry, K.M.1
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Separation and quantification of phospholipid and neutral lipid classes by HPLC–CAD: application to egg yolk lipids
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Kielbowicz, G., Trziszka, T., Wawrzenczyk, C., Separation and quantification of phospholipid and neutral lipid classes by HPLC–CAD: application to egg yolk lipids. J Liquid Chromatogr Relat Technol 2015 38 (2015), 898–903.
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31P NMR spectroscopy
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This review focuses on the basic physicochemical properties that determine the quality of phospholipid spectra, and describes an optimization strategy. It states that the following parameters should to be controlled for systematic optimization for phospholipid quantification by P NMR (1) extract concentration, (2) concentration of chelating agent, (3) pH value of the aqueous component of the solvent system, and (4) temperature of the NMR measurement.
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31P NMR spectroscopy. Biophys Rev 5 (2013), 295–304 This review focuses on the basic physicochemical properties that determine the quality of phospholipid spectra, and describes an optimization strategy. It states that the following parameters should to be controlled for systematic optimization for phospholipid quantification by P NMR (1) extract concentration, (2) concentration of chelating agent, (3) pH value of the aqueous component of the solvent system, and (4) temperature of the NMR measurement.
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1H NMR as a release methodology for the analysis of phospholipids and other constituents in infant nutrition. Anal Methods 8 (2016), 7493–7499.
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Simple and rapid quantification of phospholipids for supramolecular membrane transport assays
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Hein, R., Uzundal, C.B., Hennig, A., Simple and rapid quantification of phospholipids for supramolecular membrane transport assays. Org Biomol Chem 14 (2016), 2182–2185.
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Monakhova, Y.B., Diehl, B.W.K., Quantitative analysis of sunflower lecithin adulteration with soy species by NMR spectroscopy and PLS regression. J Am Oil Chem Soc 93 (2016), 27–36.
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Analysis of phospholipids in infant formulas using high performance liquid chromatography–tandem mass spectrometry
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This article is a good example of direct quantification of phospholipid class using hydrophilic interaction chromatography-triple quadrupole tandem mass spectrometry (HILIC-TQ-MS/MS) method.
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Fong, B., Ma, L., Norris, C., Analysis of phospholipids in infant formulas using high performance liquid chromatography–tandem mass spectrometry. J Agric Food Chem 61 (2013), 858–865 This article is a good example of direct quantification of phospholipid class using hydrophilic interaction chromatography-triple quadrupole tandem mass spectrometry (HILIC-TQ-MS/MS) method.
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Ultra-high-performance liquid chromatography-ion trap mass spectrometry characterisation of milk polar lipids from dairy cows fed different diets
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This paper discusses the quantification of phospholipid molecular species and phospholipid class by high performance liquid chromatography–mass spectrometry (HPLC–MS) method with a standard curve within a PL class.
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Craige Trenerry, V., Akbaridoust, G., Plozza, T., Rochfort, S., Wales, W.J., Auldist, M., Ajlouni, S., Ultra-high-performance liquid chromatography-ion trap mass spectrometry characterisation of milk polar lipids from dairy cows fed different diets. Food Chem 141 (2013), 1451–1460 This paper discusses the quantification of phospholipid molecular species and phospholipid class by high performance liquid chromatography–mass spectrometry (HPLC–MS) method with a standard curve within a PL class.
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Accurate quantification of lipid species by electrospray ionization mass spectrometry—meets a key challenge in lipidomics
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Comprehensive polar lipid identification and quantification in milk by liquid chromatography–mass spectrometry
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Liu, Z., Moate, P., Cocks, B., Rochfort, S., Comprehensive polar lipid identification and quantification in milk by liquid chromatography–mass spectrometry. J Chromatogr B 978 (2015), 95–102.
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This article thoroughly reviewed the application of single-point internal standard method in quantification of phospholipid molecular species by HPLC–MS method.
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Cajka, T., Fiehn, O., Comprehensive analysis of lipids in biological systems by liquid chromatography-mass spectrometry. Trend Anal Chem 61 (2014), 192–206 This article thoroughly reviewed the application of single-point internal standard method in quantification of phospholipid molecular species by HPLC–MS method.
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A study of inter-species ion suppression in electrospray ionization-mass spectrometry of some phospholipid classes
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Khoury, S., Banna, N.E., Tfaili, S., Chaminade, P., A study of inter-species ion suppression in electrospray ionization-mass spectrometry of some phospholipid classes. Anal Bioanal Chem 408 (2016), 1453–1465.
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A review of current trends and advances in modern bio-analytical methods: chromatography and sample preparation
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A review of chromatographic methods for the assessment of phospholipids in biological samples
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Peterson, B.L., Cummings, B.S., A review of chromatographic methods for the assessment of phospholipids in biological samples. Biomed Chromatogr 20 (2006), 227–243.
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Microquantification of phospholipid classes by stable isotope dilution and nanoESI mass spectrometry
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Safian, M.F., Zinn, N., Seidler, J., Lehmann, W.D., Microquantification of phospholipid classes by stable isotope dilution and nanoESI mass spectrometry. Anal Bioanal Chem 408 (2016), 7663–7667.
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NMR of polar lipids
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Diehl, B.W.K., NMR of polar lipids. Ahmad, M.U., Xu, X., (eds.) Polar lipids: biology, chemistry, and technology, 2015, AOCS Press, Urbana IL, 391–438.
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Keltti, J., Evaluation Report on the Analytical Methods submitted in connection with the Application for Authorisation of a Feed Additive according to Regulation (EC) No 1831/2003. Ares (2015)1043062 - 09/03/2015, 2015.
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