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Volumn 17, Issue 9, 2015, Pages 2122-2125

Fe-Catalyzed Direct α C-H Amination of Carbonyl Compounds

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EID: 84928902630     PISSN: 15237060     EISSN: 15237052     Source Type: Journal    
DOI: 10.1021/acs.orglett.5b00710     Document Type: Article
Times cited : (24)

References (66)
  • 42
    • 0000480449 scopus 로고
    • J. Org. Chem. 1995, 60, 5979.
    • (1995) J. Org. Chem. , vol.60 , pp. 5979
  • 51
    • 84928918750 scopus 로고    scopus 로고
    • note
    • Check the general procedure in the Supporting Information.
  • 52
    • 84928918751 scopus 로고    scopus 로고
    • note
    • To minimize the side product formation, we have used a syringe pump for slow delivery of a phenylhydroxylamine solution.
  • 66
    • 84928918752 scopus 로고    scopus 로고
    • note
    • We observed the absorbance peak at 260 nm for the 2-methyl ethylacetoacetate which disappeared upon addition of FeCl3. IR analysis indicates shifting of the carbonyl-ester peak from 1736 to 1743 cm-1 upon addition of FeCl3.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.