Palladium nanoparticle formation on TiO2(110) by thermal decomposition of palladium(II) hexafluoroacetylacetonate

ACS Applied Materials and Interfaces

Volumn 6, Issue 16, 2014, Pages 14702-14711

  Gharachorlou, Amir ^a   Detwiler, Michael D ^a   Nartova, Anna V ^a,b,c   Lei, Yu ^d   Lu, Junling ^d   Elam, Jeffrey W ^d   Delgass, W Nicholas ^a   Ribeiro, Fabio H ^a   Zemlyanov, Dmitry Y ^a  

^a PURDUE UNIVERSITY   (United States)

^b BORESKOV INSTITUTE OF CATALYSIS   (Russian Federation)

^c NOVOSIBIRSK STATE UNIVERSITY   (Russian Federation)

^d ARGONNE NATIONAL LABORATORY   (United States)

Author keywords

atomic layer deposition; heterogeneous catalysis; nucleation delay; scanning tunneling microscopy; surface science; X ray photoelectron spectroscopy

Indexed keywords

ATOMIC LAYER DEPOSITION; ATOMS; BINDING ENERGY; CATALYSIS; CRYSTALLIZATION; DECOMPOSITION; LIGANDS; NANOPARTICLES; NUCLEATION; OXIDE MINERALS; PHOTOELECTRONS; PHOTONS; SCANNING TUNNELING MICROSCOPY; SINTERING; SYNTHESIS (CHEMICAL); THERMOLYSIS; TIO2 NANOPARTICLES; TITANIUM DIOXIDE; TITANIUM METALLOGRAPHY; X RAY PHOTOELECTRON SPECTROSCOPY;

AVERAGE HEIGHT; BRIDGING OXYGEN; NUCLEATION INHIBITION; PALLADIUM NANOPARTICLES; PD ATOMS; PD NANO PARTICLE; SURFACE SCIENCE; TIO2(110);

PALLADIUM COMPOUNDS;

EID: 84906807330     PISSN: 19448244     EISSN: 19448252     Source Type: Journal    
DOI: 10.1021/am504127k     Document Type: Article

References (42)

1. Biffis, A.; Zecca, M.; Basato, M. Palladium Metal Catalysts in Heck C-C Coupling Reactions J. Mol. Catal. A: Chem. 2001, 173, 249-274
2. Molnár, á.; Sárkány, A.; Varga, M. Hydrogenation of Carbon-Carbon Multiple Bonds: Chemo-, Regio- and Stereo-Selectivity J. Mol. Catal. A: Chem. 2001, 173, 185-221
3. Blaser, H.-U.; Indolese, A.; Schnyder, A.; Steiner, H.; Studer, M. Supported Palladium Catalysts for Fine Chemicals Synthesis J. Mol. Catal. A: Chem. 2001, 173, 3-18
4. Zhu, G.; Han, J.; Zemlyanov, D. Y.; Ribeiro, F. H. Temperature Dependence of the Kinetics for the Complete Oxidation of Methane on Palladium and Palladium Oxide J. Phys. Chem. B 2004, 109, 2331-2337
5. -3 mbar J. Catal. 2006, 242, 340-348
6. Newton, M. A.; Belver-Coldeira, C.; Martinez-Arias, A.; Fernandez-Garcia, M. Dynamic in Situ Observation of Rapid Size and Shape Change of Supported Pd Nanoparticles During CO/NO Cycling Nat. Mater. 2007, 6, 528-532
7. Feng, H.; Lu, J.; Stair, P.; Elam, J. Alumina Over-Coating on Pd Nanoparticle Catalysts by Atomic Layer Deposition: Enhanced Stability and Reactivity Catal. Lett. 2011, 141, 512-517
8. 3 Surfaces Thin Solid Films 2006, 515, 1664-1673
9. Lu, J.; Fu, B.; Kung, M. C.; Xiao, G.; Elam, J. W.; Kung, H. H.; Stair, P. C. Coking- and Sintering-Resistant Palladium Catalysts Achieved through Atomic Layer Deposition Science 2012, 335, 1205-1208
10. Feng, H.; Elam, J. W.; Libera, J. A.; Setthapun, W.; Stair, P. C. Palladium Catalysts Synthesized by Atomic Layer Deposition for Methanol Decomposition Chem. Mater. 2010, 22, 3133-3142
11. Lu, J.; Liu, B.; Greeley, J. P.; Feng, Z.; Libera, J. A.; Lei, Y.; Bedzyk, M. J.; Stair, P. C.; Elam, J. W. Porous Alumina Protective Coatings on Palladium Nanoparticles by Self-Poisoned Atomic Layer Deposition Chem. Mater. 2012, 24, 2047-2055
12. Feng, H.; Libera, J. A.; Stair, P. C.; Miller, J. T.; Elam, J. W. Subnanometer Palladium Particles Synthesized by Atomic Layer Deposition ACS Catal. 2011, 1, 665-673
13. Rikkinen, E.; Santasalo-Aarnio, A.; Airaksinen, S.; Borghei, M.; Viitanen, V.; Sainio, J.; Kauppinen, E. I.; Kallio, T.; Krause, A. O. I. Atomic Layer Deposition Preparation of Pd Nanoparticles on a Porous Carbon Support for Alcohol Oxidation J. Phys. Chem. C 2011, 115, 23067-23073
14. Hämäläinen, J.; Ritala, M.; Leskelä, M. Atomic Layer Deposition of Noble Metals and Their Oxides Chem. Mater. 2013, 26, 786-801
15. 2 and Formalin Thin Solid Films 2011, 519, 5339-5347
16. Lu, J.; Stair, P. C. Nano/Subnanometer Pd Nanoparticles on Oxide Supports Synthesized by AB-Type and Low-Temperature ABC-Type Atomic Layer Deposition: Growth and Morphology Langmuir 2010, 26, 16486-16495
17. 2 Plasmas J. Phys. Chem. C 2014, 118, 8702-8711
18. Anderson, V. R.; Leick, N.; Clancey, J. W.; Hurst, K. E.; Jones, K. M.; Dillon, A. C.; George, S. M. Atomic Layer Deposition of Platinum Nanoparticles on Titanium Oxide and Tungsten Oxide Using Platinum(II) Hexafluoroacetylacetonate and Formalin as the Reactants J. Phys. Chem. C 2014, 118, 8960-8970
19. 2 and hfacH on Pt(111) J. Phys. Chem. 1993, 97, 11530-11541
20. 2(110) Surf. Sci. 2008, 602, 2967-2974
21. Lei, Y.; Lu, J.; Zhao, H.; Liu, B.; Low, K.-B.; Wu, T.; Libera, J. A.; Greeley, J. P.; Chupas, P. J.; Miller, J. T.; Elam, J. W. Resolving Precursor Deligation, Surface Species Evolution, and Nanoparticle Nucleation During Palladium Atomic Layer Deposition J. Phys. Chem. C 2013, 117, 11141-11148
22. Zaera, F. The Surface Chemistry of Atomic Layer Depositions of Solid Thin Films J. Phys. Chem. Lett. 2012, 3, 1301-1309
23. Horcas, I.; Fernandez, R.; Gomez-Rodriguez, J. M.; Colchero, J.; Gomez-Herrero, J.; Baro, A. M. WSXM: A Software for Scanning Probe Microscopy and a Tool for Nanotechnology Rev. Sci. Instrum. 2007, 78, 013705-1-013705-8
24. 2(110) Surf. Rev. Lett. 2000, 7, 613-617
25. Fadley, C. S. Basic Concepts of X-Ray Photoelectron Spectroscopy. In Electron Spectroscopy: Theory, Techniques and Applications; Brundel, C. R.; Baker, A. D., Eds.; Academic Press: New York, 1978; Vol. 2, pp 1-156.
26. Scofield, J. H. Hartree-Slater Subshell Photoionization Cross-Sections at 1254 and 1487 eV J. Electron Spectrosc. Relat. Phenom. 1976, 8, 129-137
27. Yeh, J. J.; Lindau, I. Atomic Subshell Photoionization Cross Sections and Asymmetry Parameters: 1 Z 103 At. Data Nucl. Data Tables 1985, 32, 1-155
28. Powell, C. J.; Jablonski, A. NIST Electron Effective-Attenuation-Length Database-Version 1.3; National Institute of Standards and Technology: Gaithersburg, MD, 2011.
29. 2 Powders Chem. Mater. 2002, 14, 3808-3816
30. -1 mbar Range Surf. Sci. 2006, 600, 2980-2989
31. Lin, W. B.; Wiegand, B. C.; Nuzzo, R. G.; Girolami, G. S. Mechanistic Studies of Palladium Thin Film Growth from Palladium(II) Beta-Diketonates. 1. Spectroscopic Studies of the Reactions of Bis(hexafluoroacetylacetonato) palladium(II) on Copper Surfaces J. Am. Chem. Soc. 1996, 118, 5977-5987
32. Beamson, G.; Briggs, D. High Resolution XPS of Organic Polymers: The Scienta ESCA300 Database; Wiley: New York, 1992.
33. Cohen, S. L.; Liehr, M.; Kasi, S. Mechanisms of Copper Chemical Vapor Deposition Appl. Phys. Lett. 1992, 60, 50-52
34. Cohen, S. L.; Liehr, M.; Kasi, S. Selectivity in Copper Chemical Vapor Deposition Appl. Phys. Lett. 1992, 60, 1585-1587
35. Donnelly, V. M.; Gross, M. E. Copper Metalorganic Chemical Vapor Deposition Reactions of Hexafluoroacetylacetonate Cu(I) Vinyltrimethylsilane and Bis (Hexafluoroacetylacetonate) Cu(II) Adsorbed on Titanium Nitride J. Vac. Sci. Technol., A 1993, 11, 66-77
36. Lin, W. B.; Nuzzo, R. G.; Girolami, G. S. Mechanistic Studies of Palladium Thin Film Growth from Palladium(II) Beta-Diketonates. 2. Kinetic Analysis of the Transmetalation Reaction of Bis(hexafluoroacetylacetonato) palladium(II) on Copper Surfaces J. Am. Chem. Soc. 1996, 118, 5988-5996
37. Cheung, T. T. P. Lineshape Studies of the X-Ray Photoemission of Small Metal Clusters Surf. Sci. 1983, 127, L129-L134
38. Diebold, U. The Surface Science of Titanium Dioxide Surf. Sci. Rep. 2003, 48, 53-229
39. Horton, J. H.; Shapter, J. G.; Cheng, T.; Lennard, W. N.; Norton, P. R. STM Investigation of a Cu Organometallic Complex Adsorbed on Si(111)-(7 × 7) Surf. Sci. 1997, 375, 171-182
40. 2 from Copper(II) Hexafluoroacetylacetonate J. Vac. Sci. Technol., A 2012, 31, 01A121 1-01A121 5
41. Siedle, A. R.; Newmark, R. A.; Pignolet, L. H. Structure of Palladium Bis(hexafluoroacetylacetonate) and the Systematics of Its Acid-Base Chemistry Inorg. Chem. 1983, 22, 2281-2286
42. 2: STM Imaging of Spillover and a New Form of SMSI Catal. Lett. 1999, 59, 99-105