Rapid and sensitive methodology for determination of ethyl carbamate in fortified wines using microextraction by packed sorbent and gas chromatography with mass spectrometric detection

Analytica Chimica Acta

Volumn 811, Issue , 2014, Pages 29-35

  Leça, João M ^a   Pereira, Vanda ^a,b   Pereira, Ana C ^c   Marques, José C ^a,b  

^a UNIVERSITY OF MADEIRA   (Portugal)

^b UNIVERSITY OF AVEIRO   (Portugal)

^c UNIVERSITY OF COIMBRA   (Portugal)

Author keywords

Ethyl carbamate; Gas chromatography mass spectrometric detection; Microextraction by packed sorbent; Wines

Indexed keywords

CHROMATOGRAPHIC ANALYSIS; DICHLOROMETHANE; MASS SPECTROMETERS; MASS SPECTROMETRY; SOLVENT EXTRACTION; SORBENTS; SORPTION; WINE;

ANALYTICAL PROCEDURE; COMBINING EFFICIENCY; ETHYL CARBAMATE; EXPENSIVE EQUIPMENTS; EXTRACTION SOLVENTS; LOW LIMITS OF DETECTIONS; MASS SPECTROMETRIC DETECTION; MICRO-EXTRACTION BY PACKED SORBENTS;

GAS CHROMATOGRAPHY;

DICHLOROMETHANE; SILICON DIOXIDE; SOLVENT; URETHAN;

ANALYTIC METHOD; ARTICLE; AUTOMATION; CALIBRATION; CONCENTRATION (PARAMETERS); EXTRACTION; FOOD ANALYSIS; FORTIFIED WINE; INTERMETHOD COMPARISON; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; MEASUREMENT REPEATABILITY; MICROEXTRACTION BY PACKED SORBENT; PRIORITY JOURNAL; PROCESS OPTIMIZATION; RAPID TEST; REPRODUCIBILITY; SENSITIVITY ANALYSIS; SYRINGE; VALIDATION PROCESS; VOLUMETRY; WINE;

BARREL INSERT NEEDLE; BIN; DOE; EC; ETHYL CARBAMATE; EXPERIMENTAL DESIGN; FORTIFIED WINE; FW; GAS CHROMATOGRAPHY-MASS SPECTROMETRIC DETECTION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GC-MS; INTERNAL STANDARD; IS; LIMIT OF DETECTION; LIMIT OF QUANTIFICATION; LOD; LOQ; MATRIX EFFECT; ME; MEPS; MICROEXTRACTION BY PACKED SORBENT; WINES;

AUTOMATION; CALIBRATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIMIT OF DETECTION; SOLID PHASE MICROEXTRACTION; SOLVENTS; URETHANE; WINE;

EID: 84892493404     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2013.12.018     Document Type: Article

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