Derivatization followed by gas chromatography-mass spectrometry for quantification of ethyl carbamate in alcoholic beverages

Journal of Separation Science

Volumn 35, Issue 7, 2012, Pages 804-810

  Xu, Xuejiao ^a   Gao, Yihan ^a   Cao, Xiujun ^b   Wang, Xiang ^c   Song, Guoxin ^a   Zhao, Jianfeng ^a   Hu, Yaoming ^a  

^a FUDAN UNIVERSITY   (China)

^b Shanghai Delco Electronics and Instrumentation Co Ltd   (China)

^c Shanghai Institute of Occupational Disease for Chemical Industry   (China)

Author keywords

Alcoholic beverages; Derivatization; Ethyl carbamate; Gas chromatography mass; Liquid liquid extraction; spectrometry

Indexed keywords

ALCOHOLIC BEVERAGES; ANALYTICAL METHODOLOGY; DERIVATIZATION REACTION; DERIVATIZATIONS; ETHYL ACETATES; ETHYL CARBAMATE; EXTRACTION CONDITIONS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; INTERNAL STANDARDS; LIMIT OF DETECTION; LIMIT OF QUANTIFICATIONS; LIQUID-LIQUID EXTRACTION; METHOD VALIDATIONS; OPTIMAL CONDITIONS; QUANTITATIVE DETERMINATIONS; REGRESSION COEFFICIENT; SAMPLE EXTRACTION; TIME DURATION; TOXIC CONTAMINANTS; TRIFLUOROACETAMIDES; TRIMETHYLSILYL; VALIDATION STUDY;

BEVERAGES; GAS CHROMATOGRAPHY; LIQUIDS; OPTIMIZATION; SPECTROMETRY;

SOLVENT EXTRACTION;

ACETIC ACID ETHYL ESTER; CARBAMIC ACID DERIVATIVE; SOLVENT; TRIFLUOROACETAMIDE DERIVATIVE; URETHAN;

ALCOHOLIC BEVERAGE; ARTICLE; DERIVATIZATION; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID LIQUID EXTRACTION; MASS FRAGMENTOGRAPHY; PH; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REACTION TIME; SILYLATION; TEMPERATURE; TIME;

ALCOHOLIC BEVERAGES; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIQUID-LIQUID EXTRACTION; URETHANE;

EID: 84860326194     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201100526     Document Type: Article

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