Development and validation of a high-performance liquid chromatography method for the determination of diacetyl in beer using 4-nitro-o- phenylenediamine as the derivatization reagent

Journal of Agricultural and Food Chemistry

Volumn 60, Issue 12, 2012, Pages 3013-3019

  Li, Pingliang ^a   Zhu, Yuncong ^a   He, Shun ^a   Fan, Jiqiao ^b   Hu, Qiongbo ^b   Cao, Yongsong ^a  

^a CHINA AGRICULTURAL UNIVERSITY   (China)

^b SOUTH CHINA AGRICULTURAL UNIVERSITY   (China)

Author keywords

4 nitro o phenylenediamine (NPDA); Determination; diacetyl; high performance liquid chromatography (HPLC); precolumn derivatization

Indexed keywords

4-NITRO-O-PHENYLENEDIAMINE (NPDA); ANALYTICAL METHOD; BEER SAMPLES; CHROMATOGRAPHIC SEPARATIONS; CONCENTRATION LEVELS; CORRELATION COEFFICIENT; DERIVATIZATION REACTION; DERIVATIZATION REAGENT; DERIVATIZATIONS; DETERMINATION; DIACETYL; HEALTH SAFETY; LIMIT OF DETECTION; PHENYLENEDIAMINES; PRECOLUMN DERIVATIZATIONS; RELATIVE STANDARD DEVIATIONS; ROOM TEMPERATURE; UNDESIRABLE EFFECTS;

CHROMATOGRAPHY; FOOD PRODUCTS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

BEER;

1,2-DIAMINO-4-NITROBENZENE; 2,3 BUTANEDIONE; 4 NITRO 1,2 PHENYLENEDIAMINE; DYES, REAGENTS, INDICATORS, MARKERS AND BUFFERS; PHENYLENEDIAMINE DERIVATIVE;

ARTICLE; BEER; CHEMISTRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METHODOLOGY; ODOR; REPRODUCIBILITY; VALIDATION STUDY;

BEER; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DIACETYL; INDICATORS AND REAGENTS; ODORS; PHENYLENEDIAMINES; REPRODUCIBILITY OF RESULTS;

EID: 84859147096     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf3007163     Document Type: Article

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