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Sodium salt of acetyl acetone is more efficient than acetyl acetone for the synthesis of Fe(acac)3, see: L.A. Petrova, A.P. Borisov, V.V. Aleshin, and V.D. Makhaev Russ. J. Inorg. Chem. 45 2000 390
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The conversion of the transesterification reaction in cyclohexane was increased to 97% although prolonged reaction time (40 h) is required
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The conversion of the transesterification reaction in cyclohexane was increased to 97% although prolonged reaction time (40 h) is required.
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The optical purity of the transesterified products 3n, 3o, and 3p were analyzed by chiral HPLC analysis, and the absolute configuration was deduced according to literature reports
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The optical purity of the transesterified products 3n, 3o, and 3p were analyzed by chiral HPLC analysis, and the absolute configuration was deduced according to literature reports.
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3 and compound 4 of this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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3 and compound 4 of this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cma.ac./data-request/cif.
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