A new method for the determination of carbonyl compounds in wines by headspace solid-phase microextraction coupled to gas chromatography-ion trap mass spectrometry

Journal of Agricultural and Food Chemistry

Volumn 58, Issue 24, 2010, Pages 12976-12985

  Pérez Olivero, Sergio J ^a   Pérez Trujillo, Juan P ^a  

^a UNIVERSIDAD DE LA LAGUNA   (Spain)

Author keywords

Carbonyl compounds; gas chromatography ion trap mass spectrometry; solid phase microextraction; wines

Indexed keywords

5-METHYLFURFURAL; ACETOIN; ACETOPHENONES; ANALYTES; ANALYTICAL METHOD; AUTOMATED HEADSPACE; DESORPTION TIME; DETECTION LIMITS; EXTRACTION TEMPERATURES; GAS CHROMATOGRAPHY-ION TRAP MASS SPECTROMETRIES; GAS CHROMATOGRAPHY-ION TRAP MASS SPECTROMETRY; HEAD-SPACE SOLID-PHASE MICROEXTRACTION; HEXANAL; PHENYLACETALDEHYDE; QUANTITATIVE ANALYSIS; REAL SAMPLES; REPRODUCIBILITIES; SOLID-PHASE MICROEXTRACTION;

ALDEHYDES; CARBONYLATION; CHEMICAL ANALYSIS; DESORPTION; EXTRACTION; ION CHROMATOGRAPHY; IONIC STRENGTH; KETONES; MASS SPECTROMETRY; OPTIMIZATION; SUGAR (SUCROSE); WINE;

GAS CHROMATOGRAPHY;

ORGANIC COMPOUND;

ARTICLE; EVALUATION; MASS FRAGMENTOGRAPHY; METHODOLOGY; SOLID PHASE MICROEXTRACTION; WINE;

GAS CHROMATOGRAPHY-MASS SPECTROMETRY; ORGANIC CHEMICALS; SOLID PHASE MICROEXTRACTION; WINE;

EID: 78650347753     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf1034064     Document Type: Article

References (44)

1. Etiévant, P. X. Wine. In Volatile compounds in foods and beverages; Maarse, H., Ed.; Dekker: New York, 1991; pp 483-544.
2. Ribéreau-Gayon, P.; Glories, Y.; Maujean, A.; Dubourdieu, D. In Tratado de enología. Vol.n 2: Química del vino. Estabilización y tratamiento de los vinos; Hemisferio Sur: Buenos Aires, 2002.
3. Spillman, P. J. I.; Sefton, M. A. Accumulation of volatile oak compounds in a model wine stored in American and Limousin barrels Aust. J. Grape Wine Res. 1998, 4, 67-73
4. Henschke, P. A.; Jiranek, V. Yeast-metabolism of nitrogen compounds. In Microbiology and Biotechnology; Fleet, G. H., Ed.; Harwood Academic Publishers: Graubünden, Switzerland, 1994; Chapter 4.
5. Hashizume, K.; Samuta, T. Green odorants of grape cluster stem and their ability to cause a wine stemmy flavor J. Agric. Food Chem. 1997, 45, 1333-1337
6. Baro, J. A. L.; Quiros Carrasco, J. M. Les conditions de formation des aldéhydes dans les vins: relation et importance en rapport avec les phénomènes d'oxidation et les caractéristiques organoleptiques Bull. O.I.V. 1977, 50 (554) 253-267
7. Escudero, A.; Asensio, E.; Cacho, J.; Ferreira, V. Sensory and chemical changes of young white wines stored under oxygen. An assessment of the role played by aldehydes and some other important odorants Food Chem. 2002, 77, 325-331
8. 8 aldehydes through the determination of their O-(2,3,4,5,6-pentafluorobenzyl)oximes formed directly in the solid phase extraction cartridge Anal. Chim. Acta 2004, 524, 201-206
9. Sarrazin, E.; Dubourdieu, D.; Darriet, P. Characterization of key-aroma compounds of botrytized wines, influence of grape botrytization Food Chem. 2007, 103, 536-545
10. Etievant, P.; Issanchou, S. N.; Bayonove, C. L. The flavour of Muscat wine: The sensory contribution of somo volatile compounds J. Sci. Food Agric. 1983, 34, 497-504
11. Nagy, S.; Randall, V. Use of furfural content as index of storage temperature abuse in commercially processed orange juice J. Agric. Food Chem. 1973, 21, 272-275
12. Escudero Carra, A. Estudio analítico del aroma del vino oxidado. Identificación, cuantificación y significación sensorial de sus componentes activos. Tesis Doctoral, Universidad de Zaragoza, Zaragoza, Spain, 1994.
13. Singleton, V. L. Maturation of wines and spirits: Comparisons, facts and hypotheses Am. J. Enol. Vitic. 1995, 46, 98-115
14. Simpson, R. F.; Miller, G. C. Aroma composition of Chardonnay wine Vitis 1984, 23, 143-158
15. Strauss, C. R.; Wilson, B.; Anderson, R.; Williams, P. J. Development of precursors of C13 norisoprenoid flavorants in Riesling grapes Am. J. Enol. Vitic. 1987, 38, 23-27
16. Ferreira, V.; Cacho, J.; Escudero, A.; Peña, C.; Fernández, P. Method for the HPLC prefractionation of wine flavor extracts. Part I. Analytical aspects. EuroFood Chem VIII; Progress in Food Fermentation; Valencia, Spain, 1993.
17. Ferreira, V.; Cacho, J.; Escudero, A.; Peña, C.; Fernández, P. Method for the HPLC prefractionation of wine flavor extracts. Part II. Sensorial aspects. EuroFood Chem VIII; Progress in Food Fermentation; Valencia, Spain, 1993.
18. Lasekan, O.; Buettner, A.; Christlbauer, C. Investigation of important odorants of palm wine (Elaeis guineensis) Food Chem. 2007, 105, 15-23
19. Genovese, A.; Gambuti, A.; Piombino, P.; Moio, L. Sensory properties and aroma compounds of sweet Fiano wine Food Chem. 2007, 103, 1228-1236
20. Cancilla, D. A.; Que Hee, S. S. O-(2,3,4,5,6-Pentafluorophenyl) methylhydroxylamine hydrochloride: A versatile reagent for the determination of carbonyl-containing compounds J. Chromatogr., A 1992, 627, 1-16
21. Nishikawa, H.; Sakai, T. Derivatization and chromatographic determination of aldehydes in gaseous and air samples J. Chromatogr., A 1995, 710, 159-165
22. Lehmpuhl, D. W.; Birks, J. W. New gas chromatographic-electron-capture detection method for the determination of atmospheric aldehydes and ketones based on cartridge sampling and derivatization with 2,4,6- trichlorophenylhydrazine J. Chromatogr., A 1996, 740, 71-81
23. Stashenko, E. E.; Ferreira, M. C.; Sequeda, L. G.; Martínez, J. R.; Wong, J. W. Comparison of extraction methods and detection systems in the gas chromatographic analysis of volatile carbonyl compounds J. Chromatogr., A 1997, 779, 360-369
24. Dong, J. Z.; Moldoveanu, S. C. Gas chromatography-mass spectrometry of carbonyl compounds in cigarette mainstream smoke after derivatization with 2,4-dinitrophenylhydrazine J. Chromatogr., A 2004, 1027, 25-35
25. Wanikawa, A.; Hosoi, K.; Kato, T.; Nagakawa, K. Identification of green note compounds in malt whiskey using multidimensional gas chromatography Flavour Fragrance J. 2002, 17, 207-211
26. Cardoso, D.; Bettin, S.; Reche, R.; Lima-Neto, B.; Franco, D. HPLC-DAD analysis of ketones as their 2,4-dinitrophenylhydrazone in Brazilian sugar-cane spirits and rum J. Food Compos. Anal. 2003, 16, 563-573
27. Ledauphin, J.; Basset, B.; Cohen, S.; Payot, T.; Barillier, D. Identification of trace volatile compounds in freshly distilled Calvados and Cognac: Carbonyl and sulphur compounds J. Food Compos. Anal. 2006, 19, 28-40
28. Ojala, M.; Kotiaho, T.; Siirila, J.; Sihvonen, M. L. Analysis of aldehydes and ketones from beer as o-(2,3,4,5,6-pentafluorobenzyl) hydroxylamine derivatives Talanta 1994, 41 (8) 1297-1309
29. Ferreira, V.; Culleré, L.; López, R.; Cacho, J. Determination of important odor-active aldehydes of wine through gas-chromatography-mass spectrometry of their O-(2,3,4,5,6-pentafluorobenzyl) oximes formed directly in the solid phase extraction cartridge used for selective isolation J. Chromatogr., A 2004, 1028, 339-345
30. Ferreira, V.; Culleré, L.; Loscos, N.; Cacho, J. Critical aspects of the determination of pentafluorobenzyl derivatives of aldehydes by gas chromatography with electron-capture or mass spectrometric detection. Validation of an optimized strategy for the determination of oxygen-related odor-active aldehydes in wine J. Chromatogr., A 2006, 1122, 255-265
31. Saison, D.; De Schutter, D. P.; Delvaux, F.; Delvaux, F. R. Determination of carbonyl compounds in beer by derivatisation and headspace solid-phase microextraction in combination with gas chromatography and mass spectrometry J. Chromatogr., A 2009, 1216, 5061-5068
32. Iglesias, J.; Gallardo, J. M.; Medina, I. Determination of carbonyl compounds in fish species samples with solid-phase microextraction with on-fibre derivatization Food Chem. 2010, 123, 771-778
33. Zapata, J.; Mateo-Vivaracho, L.; Cacho, J.; Ferreira, V. Comparison of extraction techniques and mass spectrometric ionization modes in the analysis of wine volatile carbonyls Anal. Chim. Acta 2010, 660, 197-205
34. Wang, Q.; O'Reilly, J.; Pawliszyn, J. Determination of low-molecular mass aldehydes by automated headspace solid-phase microextraction with in-fiber derivatisation J. Chromatogr., A 2005, 1071, 147-154
35. Hudson, E. D.; Okuda, K.; Ariya, P. A. Determination of acetone in seawater using derivatization solid-phase microextraction Anal. Bioanal. Chem. 2007, 388, 1275-1282
36. Rodríguez Bencomo, J. J.; Conde, J. E.; Rodriguez, M. A.; García, F.; Pérez Trujillo, J. P. Determination of esters in dry and sweet white wines by headspace solid-phase microextraction and gas chromatography J. Chromatogr., A 2002, 963, 213-223
37. Rodríguez Bencomo, J. J.; Conde, J. E.; García, F.; Pérez Trujillo, J. P. Determination of major compounds in sweet wines by headspace solid-phase microextraction and gas chromatography J. Chromatogr., A 2003, 991, 13-22
38. Mestres, M.; Martí, M. P.; Busto, O.; Guasch, J. Simultaneous analysis of thiols, sulphides and disulphides in wine aroma by headspace solid-phase microextraction-gas chromatography J. Chromatogr., A 1999, 849, 293-297 (Pubitemid 29301677)
39. Mestres, M.; Martí, M. P.; Busto, O.; Guasch, J. Analysis of low-volatility organic sulphur compounds in wines by solid-phase microextraction and gas chromatography J. Chromatogr., A 2000, 881, 583-590
40. Câmara, J. S.; Alves, M. A.; Marques, J. C. Development of headspace solid-phase microextraction-gas chromatography-mass spectrometry methodology for analysis of terpenoids in Madeira wines Anal. Chim. Acta 2006, 555, 191-200
41. Noguerol-Pato, R.; González-Barreiro, C.; Cancho-Grande, B.; Simal-Gándara, J. Quantitative determination and characterisation of the main odourants of Mencía monovarietal red wines Food Chem. 2009, 117, 473-484
42. Gómez-Míguez, M. J.; Cacho, J. F.; Ferreira, V.; Vicario, I. M.; Heredia, F. J. Volatile components of Zalema white wines Food Chem. 2007, 100, 1464-1473
43. Moreno, J. A.; Zea, L.; Moyano, L.; Medina, M. Aroma compounds as markers of the changes in sherry wines subjected to biological ageing Food Control 2005, 16, 333-338
44. Aznar, M.; Arroyo, T. Analysis of wine volatile profile by purge-and-trap-gas chromatography-mass spectrometry. Application to the analysis of red and white wines from different Spanish regions J. Chromatogr., A 2007, 1165, 151-157