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We found that benzene evaporated too quickly under these conditions making stirring difficult. In addition, toluene was also tested but it was less effective than chlorobenzene.
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We found that benzene evaporated too quickly under these conditions making stirring difficult. In addition, toluene was also tested but it was less effective than chlorobenzene.
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An 8% NMR yield was obtained when the reaction was performed without DDQ.
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An 8% NMR yield was obtained when the reaction was performed without DDQ.
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The crude reaction mixture showed approximately 30% of unreacted 3-flourophenylacetylene remaining after the reaction. Increasing the reaction time to 30 h did not improve the yield.
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The crude reaction mixture showed approximately 30% of unreacted 3-flourophenylacetylene remaining after the reaction. Increasing the reaction time to 30 h did not improve the yield.
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