Application of an analytical method for the simultaneous determination of the off-flavour volatiles geosmin, 4-ethylphenol and 4-ethylguaiacol and of target wine aroma volatiles

Italian Journal of Food Science

Volumn 22, Issue 1, 2010, Pages 15-27

  Lisanti, M T ^a   Genovese, A ^a   Piombino, P ^a   Gambuti, A ^a   Moio, L ^a  

^a UNIVERSITY OF NAPLES FEDERICO II   (Italy)

Author keywords

4 ethylguaiacol; 4 ethylphenol; Aroma; Geosmin; Off flavours; Wine

Indexed keywords

EID: 77952349769     PISSN: 11201770     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (50)

1. Aznar M., Lopez R., Cacho J.F. and Ferreira V. 2001. Identification of impact odorants of aged red wines from Rioja. GC-Olfactometry, Quantitative GC-MS, and odor evaluation of HPLC fractions. J. Agric. Food Chem. 49: 2924.
2. Caboni P., Sarais G., Cabras M. and Angioni A. 2007. Determination of 4-ethylphenol and 4-ethylguaiacol in wines by LC-MS-MS and HPLC-DAD- fluorescence. J. Agric. Food Chem. 55: 7288.
3. Chatonnet P. and Boidron J-N. 1988. Dosages de phenols volatils dan les vins par Chromatographie en phase gazeuse. Sci. Aliment. 8: 479.
4. Chatonnet P., Boidron J-N. and Pons M. 1990. Elevage des vins rouges en futs de chene: evolution de certains composes volatils et de leur impact aromatique. Sci. Aliment. 10: 565.
5. Chatonnet P., Dubourdieu D., Boidron J.N. and Pons M. 1992. The origin of ethylphenols in wines. J. Agric. Food Chem. 60: 165.
6. Chatonnet P., Dubourdieu D., Boidron J.N. and Lavigne V. 1993. Synthesis of volatile phenols by Saccharomyces cerevisiae in wines. J. Sci. Food Agric. 62: 191.
7. Chatonnet P., Dubourdieu D. and Boidron J.-N. 1995. The influence of Brettanomyces/Dekkera sp. yeast and lactic acid bacteria on the ethylphenol content of red wines. Am. J. Enol. Vitic. 46: 463.
8. Chisholm M.G., Guiher L.A., Vonah T.M. and Beaumont J.L. 1994. Comparison of some French-American hybrid wines with white Riesling using GC/O. Am. J. Enol. Vitic. 45: 201.
9. Cook D., Newcombe G. and Sztajnbok P. 2001. The application of powdered activated carbon for MIB and geos-min removal: predicting PAC doses in four raw waters. Water Res. 35: 1325.
10. Culleré L., Escudero A., Cacho J. and Ferreira V. 2004. Gas Chromatography-olfactometry and chemical quantitative study of the aroma of six "premium quality" Spanish aged red wines. J. Agric. Food Chem. 52: 1653.
11. Dabrowski A., Podkościelny P., Hubicki Z. and Barczak M. 2005. Adsorption of phenolics compounds by activated carbon-a critical review. 2005. Chemosphere 58: 1049.
12. Darriet P., Pons M., Lamy S. and Dubourdieu D. 2000. Identification and quantification of geosmin, an earthy odorant contaminating wines. J. Agric. Food Chem. 48: 4835.
13. Darriet P., Lamy S., La Guerche S., Pons M., Dubourdieu D., Blancard D., Steliopoulos P. and Mosandl A. 2001. Stereo differentiation of geosmin in wine. Eur. Food Res. Technol. 213: 122.
14. Darriet P., Pons M., Henry R., Dumont O., Findeling V., Cartolaro P., Calonnec A. and Dubourdieu D. 2002. Impact odorants contributing to the fungus type aroma from grape berries contaminated by powdery mildew (Uncinula necator); incedence of enzymatic activities of the yeast Saccharomyces cerevisiae. J. Agric. Food Chem. 50: 3277.
15. Díez J., Domínguez C., Guillén D.A., Veas R. and Barroso C.G. 2004. Optimisation of stir bar sorptive extraction for the analysis of volatile phenols in wines. J. Chromatogr. A 1025: 263.
16. Domínguez C., Guillén D.A. and Barroso C.G. 2002. Determination of volatile phenols in fino sherry wines. Anal. Chim. Acta 458: 95.
17. Dufour C. and Bayonove C.L. 1999. Interaction between polyphenols and aroma substances. An insight at the molecular level. J. Agric. Food Chem. 47: 678.
18. Dufour C. and Sauvaitre I. 2000. Interactions between an-thocyanins and aroma substances in a model system. Effect on the flavour of grape-derived beverages. J. Agric. Food Chem. 48: 1784.
19. Dumoulin M. and Riboulet J.M. 2004. Analyse de géosmine dans les vins: apport de la microextraction en phase solide (SPME) couplée à l'analyse par GC-MS. Rev. Fr. Oenol. 208: 28.
20. Escudero A., Cacho J.F. and Ferreira V. 2000. Isolation and identification of odorants generated in wine during its oxidation: a gas chromatography-olfactometric study. Eur. Food Res. Technol. 211: 105.
21. Etiévant P.X. 1991. Wine. In: "Volatile Compounds of Food and Beverages". H. Maarse (Ed.), p. 483. Marcel-Dekker, New York, Usa.
22. Fariña L., Boido E., Carrau F and Dellacassa E. 2007. Determination of volatile phenols in red wines by dispersive liquid-liquid microextraction and gas chromatography-mass spectrometry detection. J. Chromatogr. A 1157: 46.
23. Fernández M.J., Oliva J., Barba A. and Cámara M.A. 2005. Effects pf clarification and filtration processes on the removal of fungicide residues in red wines (var. Monastrell). J. Agric. Food Chem. 53: 6156.
24. Ferreira V., Lopez R., Aznar M. 2002. Olfactometry and aroma extract dilution analysis of wines. In: "Molecular Methods of Plant Analysis, Analysis of Taste and Aroma". Vol. 21. Jackson J.F. and Linskens H.F. (Ed.), p. 88. Springer Berlin.
25. Ferreira V., Lopez R. and Cacho J. F. 2000. Quantitative determination of the odorants of young red wines from different grape varieties. J. Sci. Food Agric. 80: 1659.
26. Flavours & Fragrances catalogue 2003-2004. Sigma-Aldrich, St. Louis, MO, Usa.
27. Genovese A., Lisanti M.T., Gambuti A., Piombino P. and Moio L. 2007. Relationship between sensory perception and aroma compounds of red wines. Acta Hortic. (ISHS) 754: 549.
28. Guth H. 1997. Quantitation and sensory studies of character impact odorants of different white wine varieties. J. Agric. Food Chem. 45: 3027.
29. nd Ed.
30. 1H NMR Spectroscopy J. Agric. Food Chem. 48: 407.
31. e Symposium International d'œnologie, A. Lonvaud (Ed.)., Tec et Doc, Lavoisier, Paris.
32. La Guerche S., Chamont S., Blancard D., Dubourdieu D. and Darriet P. 2005. Origin of (-)-geosmin on grapes: on the complementary action of two fungi, Botrytis cinerea and Penicillium expansion. Antonie Leeuwenhoek 88: 131.
33. La Guerche S., Dauphin B., Pons M., Blancard D. and Darriet P. 2006. Characterization of some mushroom and earthy off-odors microbially induced by the development of rot on grapes. J. Agric. Food Chem. 54: 9193.
34. Larcher R., Nicolini G., Puecher C., Bertoldi D., Moser S. and Favaro G. 2007. Determination of volatile phenols in wine using high-performance liquid chromatography with a coulometric array detector. Anal. Chim. Acta 582: 55.
35. Maarse H., Visscher CA., Willemsens L.C., Boelens M.H. 1992. Volatile Compounds in Food. Qualitative and Quantitative Data. Vol. 1. TNO-CtVO Biotechnology and Chemistry Institute: Zeist, The Netherland.
36. Martorell N., Marti M.P., Mestres M., Busto O. and Guasch J. 2002. Determination of 4-ethylguaiacol and 4-ethylphenol in red wines using headspace-solid-phase microex-traction-gas chromatography J. Chromatogr. A 975: 349.
37. Moio L., Chambellant E., Lesschaeve I., Issanchou S., Schlich P. and Etievant P.X. 1995. Production of representative wine extracts for chemical and olfactory analysis. Ital. J. Food Sci. 3: 265.
38. Moio L., Del Prete G., Diana M. and Valentino A. 1999. Influenza deH'origine geografica del legno di rovere impiega-to per la fabbricazione delie barrique e dell'intensità della tostatura del legno sull'aroma del vino rosso. Industria delle Bevande 158: 615.
39. Moio, L. Di Marzio L., Genovese A., Piombino P., Squillante E., Castellano L. and Mercurio V. 2002. I descrittori sensoriali ed i componenti volatili ad elevato impatto olfattivo deH'aroma del vino Fiano. Vignevini 4: 115.
40. Monje M.-C., Privat C., Gastine V. and Nepveu F. 2002. Determination of ethylphenol compounds in wine by head-space solid-phase microextraction in conjunction with gas chromatography and flame ionization detection. Anal. Chim. Acta 458: 111.
41. Nicolini G., Larcher R., Bertoldi D., Puecher C. and Magno F. 2007. Rapid quantification of 4-ethylphenol in wine using high-performance liquid chromatography with a fluorimetric detector. Vitis 46: 202.
42. Ortega-Heras M., Gonzáles-SanJosé M.L. and Beltrán S. 2002. Aroma composition of wine studied by different extraction methods. Anal. Chim. Acta 458: 85.
43. Perestrelo R., Fernandez A., Albuquerque F.F., Marques J.C. and Câmara J.S. 2006. Analytical characterization of the aroma of Tinta Negra Mole red wine: identification of the main odorants compounds. Anal. Chim. Acta 563: 154.
44. Pérez-Prieto L.J., López-Roca J.M., Martmez-Cutillas A., Pardo Mínguez F and Gómez-Plaza E. 2002. Maturing wines in oak barrels. Effect of origin, volume, and age of the barrel in the wine volatile composition. J. Agric. Food Chem. 50: 3272
45. Piombino P., Nicklaus S., Le Fur Y., Moio L. and Le Quere J.L. 2004. Selection of products presenting given flavor characteristics: An application to wine. Am. J. Enol. Vitic. 55: 27.
46. Pollnitz A.P., Pardon K.H. and Sefton M.A. 2000. Quantitative analysis of 4-ethylphenol and 4-ethylguaiacol in red wine. J. Chromatogr. A 874: 101.
47. Sejer Pedersen D., Capone D.L., Skouroumounis G.K., Pollnitz A.P. and Sefton M. A. 2003. Quantitative analysis of geraniol, nerol linalool, and α-terpineol in wine. Anal. Bioanal. Chem. 375: 517.
48. Suárez R., Suárez-Lepe J.A., Morata A. and Calderón F. 2007. The production of ethylphenols in wine by yeast of the genera Brettanomyces and Dekkera: a review. Food Chem. 102:10.
49. Versini G. 1985. Sull'aroma del vini Traminer Aromatico o Gewürztraminer. Vignevini 12: 57.
50. Versini G., Dalla Serra A., Falcetti M. and Sferlazzo G. 1992. Role du clone, du millesime et de l'epoque de la recolte sur le potentiel aromatique du raisin de Chardonnay. Rev. Oenol. 18:19.