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Under analogous conditions, 1,4, and 6 afforded 15 % (A/K = 0.22), 3% (A/K = 2), and 13% (A/K = 0.44) yields respectively.
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Under analogous conditions, 1,4, and 6 afforded 15 % (A/K = 0.22), 3% (A/K = 2), and 13% (A/K = 0.44) yields respectively.
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A third addition resulted in lower yields, presumably because of product overoxidation
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70349845969
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6, 3, and 6 can be found as Figure S4 in the Supporting Information.
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6, 3, and 6 can be found as Figure S4 in the Supporting Information.
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Deactivation of 2 via formation of oligomeric species has been recently proposed; N. A. Vermeulen, M. S. Chen, M. C. White, Tetrahedron 2009, 65, 3078-3084.
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Deactivation of 2 via formation of oligomeric species has been recently proposed; N. A. Vermeulen, M. S. Chen, M. C. White, Tetrahedron 2009, 65, 3078-3084.
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