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0037921128
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note
-
mep=N, N′-dimethyl-N,N′-bis(2-pyridylmethyl)ethane-1,2-diamine. R,R-mcp = N,N′-dimethyI-N,N′ -bis(2-pyridylmethyl)cyclohexane-1R,2R-di-amine.
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12
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0039812510
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16
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0038597412
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note
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3, 3401 reflections (4° < 20 < 43.94°), R(Rw) = 0.036 (0.095).
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17
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0000224916
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18
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0028911267
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0001580728
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27
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0038258661
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note
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2 free.
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28
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0037921123
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note
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2 and HOAc using 1% sulfuric acid catalyst.
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29
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0037921124
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note
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2-. CDTA = trans-cyclobexyl-1,2-diamine tetraacetic acid.
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30
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0037921127
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note
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2 shows no reactivity under these conditions.
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31
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0037921125
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note
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This system does not exclusively provide the epoxide product for sensitive olefins such as styrene, ethyl acrylate, or α-pinene.
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32
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0037921126
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note
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2 salt and R,R-mcp. In addition, these reactions can be run in an identical manner when glacial acetic acid is used as the solvent.
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34
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0038258718
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note
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2+ have a similar scope of reactivity but require higher catalyst loadings. P. Hung, unpublished results.
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