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49
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57949093666
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1H NMR analysis was ∼80%.
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1H NMR analysis was ∼80%.
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The signals due to inner β-CH were observed at δ -3.82 ppm (minor) and -3.83 ppm (major), respectively. Because all signals were significantly overlapped, it was difficult to determine the product ratio accurately.
-
The signals due to inner β-CH were observed at δ -3.82 ppm (minor) and -3.83 ppm (major), respectively. Because all signals were significantly overlapped, it was difficult to determine the product ratio accurately.
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57
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57949087932
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The LANL2DZ basis set was used for the rhodium atoms and the 6-31G** basis set for the rest.
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The LANL2DZ basis set was used for the rhodium atoms and the 6-31G** basis set for the rest.
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58
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2, 47.1 mg of the residue was obtained.
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2, 47.1 mg of the residue was obtained.
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