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Crystallographic data for 4·CHCl3: C 79H49Cl3N12Zn3, Mr, 1468.84, monoclinic, space group P1, a, 15.225(3, b, 15.442(3, c, 16.500(2) Å, α, 91.865(7)°, β, 109.600(7)°, γ, 115.960(8)°, V, 3211(1) A°3, Z, 2, ρcalcd, 1.519 gcm -3, T, 140°C, 107414 measured reflections, 14666 unique reflections (Rint, 0.066, 8269 with I ≥ 3σ(I) used in refinement, R, 0.065, Rw, 0.095, GOF, 1.062. CCDC 622718 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge @Crystallographic Data Centre via
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w = 0.095, GOF = 1.062. CCDC 622718 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge @Crystallographic Data Centre via @www.ccdc.cam.ac.uk/data_request/cif.
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