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Volumn , Issue 31, 2007, Pages 5212-5225

Oxidative nucleophilic substitution (SNOX) of the benzylic position as a tunable synthesis of tetrahydroisoquinoline natural alkaloid analogues

Author keywords

Alkaloids; Donor acceptor systems; Nucleophilic substitution; Oxidation

Indexed keywords


EID: 35948949906     PISSN: 1434193X     EISSN: 10990690     Source Type: Journal    
DOI: 10.1002/ejoc.200700366     Document Type: Article
Times cited : (24)

References (111)
  • 11
    • 0036558479 scopus 로고    scopus 로고
    • For a review, see
    • For a review, see: J. Scott, R. M. Williams, Chem. Rev. 2002, 102, 1669-1730.
    • (2002) Chem. Rev , vol.102 , pp. 1669-1730
    • Scott, J.1    Williams, R.M.2
  • 20
    • 35948935683 scopus 로고    scopus 로고
    • th Annual Meeting, New Orleans, 20-23 May, 2000, Abstract number 2182;
    • th Annual Meeting, New Orleans, 20-23 May, 2000, Abstract number 2182;
  • 40
    • 0000890076 scopus 로고
    • Ed, J. S. Pizey, Wiley, New York
    • b) A. B. Turner, Synthetic Reagents (Ed.: J. S. Pizey), Wiley, New York, 1977, vol. 3, pp. 193-225.
    • (1977) Synthetic Reagents , vol.3 , pp. 193-225
    • Turner, A.B.1
  • 65
    • 4243241249 scopus 로고
    • For a review, see
    • a) For a review, see: E. D. Cox, J. M. Cook, Chem. Rev. 1995, 95, 1797;
    • (1995) Chem. Rev , vol.95 , pp. 1797
    • Cox, E.D.1    Cook, J.M.2
  • 68
    • 35948965688 scopus 로고    scopus 로고
    • 13C: 100 MHz).
    • 13C: 100 MHz).
  • 69
    • 35949000939 scopus 로고    scopus 로고
    • -3. CCDC-628764 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
  • 73
    • 35948952458 scopus 로고    scopus 로고
    • X-ray crystal structure analysis of 26: Colourless crystal from CH2Cl2; size [mm, 0.50 x 0.40 x 0.25; formula C 15H17NO7, M, 323.30; data set collected with a Nonius-KappaCCD diffractometer; orthorhombic; space group: P212121; a, 7.7550(2, b, 11.9840(5, c, 16.0200(7) Å; V, 1488.8(1) Å3; Z, 4; ρ, 1.442 g cm-3; 2σmax, 55.8°; λ(Mo-Kα, 0.71073 Å; T, 291 K; 3432 measured reflections; 2970 [I > 2σ(I, μMo-Kα, 0.116 mm-1; Tmin, 0.945, Tmax, 0.971; SHELXTL; 209 parameters; alcoholic hydrogen atom clearly evidenced on Fourier difference map; all other hydrogen atoms calculated and refined as riding atoms; R, 0.044, wR, 0.115; refinem
    • -3. CCDC-628658 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data_request/cif.
  • 82
    • 35948982646 scopus 로고    scopus 로고
    • X-ray crystal structure analysis of 33a: Colourless crystal from CH2Cl2; size [mm, 0.60 x 0.50 x 0.40; formula C 18H21NO8S, M, 411.42; data set collected with a Nonius-KappaCCD diffractometer; monoclinic; space group: P21; a, 4.8190(1, b, 16.8130(7, c, 11.8460(5) Å; β, 96.707(2)°; V, 953.22(6) Å3; Z, 2; ρ, 1.433 g cm-3; 2θmax, 55.6°; λ(Mo-Kα, 0.71073 Å; T, 294 K; 3747 measured reflections; 3597 [I > 2σ(I, μMo-Kα, 0.216 mm -1; Tmin, 0.881, Tmax, 0.918; SHELXTL; 252 parameters; hydrogen atoms calculated and refined as riding atoms; R, 0.030, wR, 0.085; refinement of F2 against all reflections; Δρ
    • -3. CCDC-641202 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data_request/cif.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.