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33748991045
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The similarity of the retention time between dibenzalacetone (palladium ligand) and the final imino esters 5 made the purification of these compounds difficult, thus decreasing the yield of isolated products.
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33748997824
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The allyl zinc halide must be freshly prepared and used immediately in order to obtain the results indicated above.
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47
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33749010222
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note
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For the X-ray structure of (+)-10, see Supporting Information.
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