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85069145054
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note
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+/MS). Experimental details of synthesis will be given in due course in a full account of this study.
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32
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85069140699
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note
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9 gave the imine 2 with 50-60 % yield in several experiments. It was very important to keep the reaction mixture at 0 °C. At 25 °C, a strong blue-green color slowly developed in the reaction mixture, and unidentified side products were mostly obtained after work-up.
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85069131657
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note
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Best yield of several experiments under various experimental conditions of base and solvent.
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37
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85069135540
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note
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2 by the acylazide method has been found to proceed efficiently.
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41
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0001554363
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