The use of solid-phase microextraction-gas chromatography in forensic analysis

Journal of Chromatographic Science

Volumn 38, Issue 7, 2000, Pages 297-306

  Furton, Kenneth G ^a   Wang, Jing ^a   Hsu, Ya Li ^a   Walton, John ^a   Almirall, José R ^a  

^a FLORIDA INTERNATIONAL UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

4 HYDROXYBUTYRIC ACID; ALCOHOL; EXPLOSIVE; NEUROLEPTIC AGENT; POISON;

ALCOHOL BLOOD LEVEL; ANALYTIC METHOD; ARTICLE; COST EFFECTIVENESS ANALYSIS; DRUG BLOOD LEVEL; EARLY DIAGNOSIS; FORENSIC PATHOLOGY; GAS CHROMATOGRAPHY; HUMAN; HUMAN CELL; HUMAN TISSUE; LIQUID CHROMATOGRAPHY; ODOR; RESIDUE ANALYSIS; SKIN; SOLID PHASE MICROEXTRACTION; TOXIN ANALYSIS; WATER CONTAMINATION;

EID: 0034236707     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/38.7.297     Document Type: Article

References (106)

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4. A novel method for the analysis of gasoline from fire debris using headspace solid-phase microextraction
5. A simple, inexpensive, rapid, sensitive and solventless method for the recovery of accelerants from fire debris based on SPME
6. Forensic application of the solid phase microextraction method to the analysis of gasoline and kerosene
7. Analysis of inflammable substances in blood using head space-solid phase microextraction and chemical ionization ion monitoring
8. A simple analysis of 5 thinner components in human body fluids by headspace solid-phase microextraction (SPME)
9. A novel method for the analysis of gasoline from fire debris using headspace solid-phase microextraction
10. The recovery of accelerants in aqueous samples from fire debris using solid phase microextraction (SPME)
11. Determination of liquid accelerants in arson suspected fire debris using headspace solid-phase microextraction
12. The detection and analysts of ignitable liquid residues extracted from human skin using SPME/GC
13. A comprehensive sample preparation scheme for accelerants in suspect arson cases
14. Contemporary sample preparation methods for the detection of ignitable liquids in suspect arson cases
15. Determination of the semi-volatile compounds nitrobenzene, isophorone, 2,4-dinitrotoluene and 2,6-dinitrotoluene in water using solid-phase microextraction with a polydimethylsiloxane-coated fiber
16. Application of solid-phase microextraction to the recovery of organic explosives
17. Trace explosives signatures from World War II unexploded undersea ordnance
18. Trace analysis of explosives in seawater using solid-phase microextraction and gas chromatography/ion trap mass spectrometry
19. Optimization of solid phase microextraction (SPME) for the recovery of explosives from aqueous and post-explosion debris followed by gas and liquid chromatographic analysis
20. The scientific foundations and efficacy of the use of canines as chemical detectors for explosives
21. The application of solid-phase microextraction to the recovery of explosives and ignitable liquids residues from forensic specimens
22. Trends in techniques for the extraction of drugs and pesticides from biological specimens prior to chromatographic separation and detection
23. Solid-phase microextraction (SPME) of drugs and poisons from biological samples
24. Determination of drugs of abuse using solid-phase microextraction
25. Detection of cocaine in human urine by solid-phase microextraction and capillary gas chromatography with nitrogenphosphorus detection
26. Aqueous phase hexyl chloroformate derivatization and SPME determination of benzoylecgonine in urine by GC-Quadrupole ion trap mass spectrometry
27. Determination of amphetamine, methamphetamine and dimethamphetamine in human urine by solid-phase microextraction (SPME)-gas chromatography/mass spectrometry
28. Simple clean-up of methamphetamine and amphetamine in human urine by direct-immersion solid phase micro extraction (DI-SPME)
29. Application of a solid-phase microextraction technique for the detection of urinary methamphetamine and amphetamine by gas chromatography
30. Detection of amphetamines and inflammable compounds in biological materials using GC/MS and SPME
31. Automated determination of ecstasy and amphetamines in urine by SPME and capillary GC after polylchloroformate derivatization
32. Detection of amphetamines in urine using headspace-solid phase microextraction and chemical ionization selected ion monitoring
33. Quantitative and qualitative analysis of MDMA, MDEA, MA, and amphetamine in urine by headspace/solid phase micro-extraction (SPME) and GC/MS
34. Method optimization for the analysis of amphetamines in urine by solid-phase microextraction
35. Screening procedure for 21 amphetamine-related compounds in urine using solid-phase microextraction and gas chromatography-mass spectrometry
36. Rapid analysis of amphetamine, methamphetamine, MDA, and MDMA in urine using solid-phase microextraction, direct on-fiber derivatization, and analysis by GC-MS
37. Gas chromatographic analysis of methadone in urine samples after solid phase microextraction
38. Rapid analysis of nicotine and cotinine in urine using headspace-solid phase microextraction and selected ion monitoring
39. Simple extraction of tricyclic antidepressants in human urine by headspace solid-phase microextraction (SPME)
40. Detection of meperidine (pethidine) in human blood and urine by headspace solid phase microextraction and gas chromatography
41. Detection of benzodiazepines in human urine by direct immersion SPME-GC
42. Determination of five benzodiazepines in aqueous solution and biological fluids using SPME with carbowax/DVB fiber coating
43. Solid-phase microextraction and GC-ECD of benzophenones for detection of benzodiazepines in urine
44. Determination benzophenone-3 and metabolites in water and human urine by SPME and quadrupole ion trap GC-MS
45. Determination of barbiturates by SPME and ion trap GC-MS
46. The confirmation of volatiles by solid-phase microextraction and GC-MS in the investigation of two traffic fatalities
47. Headspace solid-phase micro-extraction for the determination of BETX in urine
48. Method for analyzing urinary toluene and xylene by SPME and its application to workers using organic solvents
49. Application of SPME and GC-MS for the determination of chlorophenols in urine
50. Total 4-chlorophenol determination in urine samples of subjects exposed to chlorobenzene using SPME and GC-MS
51. Solid-phase microextraction for the determination of the free concentration of valproic acid in human plasma by capillary gas chromatography
52. Solid-phase microextraction with capillary gas-liquid chromatography and nitrogen-phosphorus selective detection for the assay of antidepressant drugs in human plasma
53. Detection of tricyclic antidepressants in whole blood by headspace solid-phase microextraction and capillary gas chromatography
54. Analysis of tricyclic antidepressant and that application blood and urine for fatal intoxication by headspace SPME
55. Simple analysis of tetracyclic antidepressants in blood using headspace-solid-phase microextraction and GC-MS
56. Rapid analysis of amphetamines in blood using headspace-solid phase microextraction and selected ion monitoring
57. Simple extraction of phencyclidine from human body fluids by headspace SPME
58. Use of SPME for the determination of methadone and its main metabolite, EDDP, in plasma by gas chromatography-mass spectrometry
59. Simple analysis of diphenylmethane antihistaminics and their analogous in bodily fluids by headspace solid-phase microextraction-capillary gas chromatography
60. Solvent-modified solidphase microextraction for the determination of diazepam in human plasma samples by capillary gas chromatography
61. Analysis of steroids from human serum by SPME with headspace derivatization and gas chromatography
62. Analysis of estrogens and anabolic steroids by SPME with on-fiber derivatization and GC-MS
63. Extraction of methylxanthines from human body fluids by SPME
64. Detection of ethanol in human body fluids by headspace solid-phase micro extraction (SPME)/capillary gas chromatography
65. Blood alcohol determination with automated solid phase microextraction (SPME): A comparison with static headspace sampling
66. Improved extraction of ethanol from human body fluids by headspace SPME with a Carboxen/PDMS fiber
67. Simple extraction of methanol in human whole blood by headspace SPME
68. Detection of organophosphorous pesticides in human body fluids by solid-phase microextraction (SPME) and capillary gas chromatography with nitrogen-phosphorus detection
69. Rapid analysis of malathion in blood using headspace solid-phase microextraction and selected ion monitoring
70. Determination of some carbamate pesticides in human body fluids by headspace solid phase microextraction and gas chromatography
71. Detection of some phenothiazines by headspace SPME and GC
72. SPME and GC-ECD determination of dinitroaniline herbicides in surface water and biological fluids
73. Rapid analysis of parathion in biological samples using headspace SPME and GC-MS
74. Simple and sensitive analysis of nereistoxin and its metabolites in human serum using headspace solid-phase microextraction and gas chromatography-mass spectrometry
75. Analysis of inflammable substances in blood using head space-solid phase microextraction and chemical ionization ion monitoring
76. A simple analysis of 5 thinner components in human body fluids by headspace solid-phase microextraction (SPME)
77. Detection of cresol isomers and phenol in human whole blood by headspace SPME and capillary GC
78. Biomonitoring of benzene and toluene in human blood by headspace SPME
79. SPME and GC-MS for determination of monoaromatic hydrocarbons in blood and urine. Application to people exposed to air pollutants
80. Tetrachloroethylene and trichloroethylene fatality: Case report and simple headspace SPME-capillary gas chromatographic determination in tissues
81. Detection of ten local anaesthetics in human blood using solid-phase microextraction (SPME) and capillary gas chromatography
82. Extraction of local anesthetics from human blood by direct immersion-SPME
83. Simple analysis of local anaesthetics in human blood using headspace SPME and GC-MS-electron impact ionization selected ion monitoring
84. Determination of methylmercury in fish and aqueous samples using solid-phase microextraction followed by gas chromatographyatomic fluorescence spectrometry
85. Simultaneous determination of Hg(III) and alkylated Hg, Pb, and Sn species in human body fluids using SPME-GC-MS-MS
86. Determination of methylmercury in biological samples and sediments by capillary GC coupled with atomic adsorption after hydride derivatization and SPME
87. Analysis of cyanide in blood by headspace SPME and capillary GC
88. Determination of lead in blood and urine by SPME-GC
89. Solid-phase microextraction for the analysis of human breath
90. Solid phase microextraction as a tool to determine membrane/water partition coefficients and bioavailable concentrations in vitro systems
91. Headspace SPME method optimization for residual solvent analysis
92. SPME/Capillary GC for the profiling of confiscated ecstasy and amphetamine
93. Determination of cannabinoids in water and human saliva by SPME and quadrupole ion trap GC-MS
94. Determination of amphetamine and methamphetamine in human hair by headspace SPME and GC-NPD
95. Solid-phase microextraction for cannabinoids analysis in hair and its possible application to other drugs
96. Classification of the botanical origin of cinnamon by SPME-GC
97. Characterization of commercial vodkas by SPME-GC-MS
98. Characterization of roasted coffee and coffee beverages by SPME-GC and principal component analysis
99. Qualitative and quantitative analysis of flavor additives on tobacco products using SPME-GC-MS
100. Identification of gamma-hydroxybutyric acid (GHB) by headspace SPME followed by chemical ionization-mass spectrometry