Rapid analysis of amphetamines in blood using head space-solid phase microextraction and selected ion monitoring

Forensic Science International

Volumn 78, Issue 2, 1996, Pages 95-102

  Nagasawa, Nobuyuki ^a   Yashiki, Mikio ^a   Iwasaki, Yasumasa ^a   Hara, Kenji ^b   Kojima, Tohru ^a  

^a HIROSHIMA UNIV SCHOOL OF MEDICINE   (Japan)

^b FUKUOKA UNIVERSITY SCHOOL OF MEDICINE   (Japan)

Author keywords

Amphetamine; Blood; Gas chromatography mass spectrometry; Head space; Methamphetamine; Solid phase microextraction

Indexed keywords

ACID ANHYDRIDE; AMPHETAMINE; DEUTERIUM; METHAMPHETAMINE; SODIUM HYDROXIDE;

ARTICLE; BLOOD ANALYSIS; BLOOD SAMPLING; CALIBRATION; CONTROLLED STUDY; DRUG DETERMINATION; GAS CHROMATOGRAPHY; HUMAN; HUMAN TISSUE; ION MONITORING; MASS SPECTROMETRY; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; STANDARD; TECHNIQUE;

EID: 0029870343     PISSN: 03790738     EISSN: None     Source Type: Journal    
DOI: 10.1016/0379-0738(95)01874-3     Document Type: Article

References (12)

1. R.B. Bruce and W.R. Maynard, Jr, Determination of amphetamine and related amines in blood by gas chromatography. Anal. Chem., 41 (1969) 977-979.
2. K. Hara, T. Nagata and K. Kimura, Forensic toxicologic analysis of methamphetamine and amphetamine in body materials by gas chromatography/mass spectrometry. Z. Rechtsmed., 96 (1986) 93-104.
3. R. Taylor, S. Le, S. Philip and N. Jain, Simultaneous identification of amphetamine and methamphetamine using solid-phase extraction and gas chromatography/nitrogen phosphorous. J. Anal. Toxicol., 13 (1989) 293-295
4. H. Brandenberger, Can gas chromatography-mass spectrometry influence trends in drug abuse? In A. Frigerio and E.L. Ghisalberti (eds.), Mass Spectrometry in Drug Metabolism, New York, 1977, pp. 379-402.
5. H. Tsuchihashi, K. Nakajima, M. Nishikawa, S. Suzuki, K. Shiomi and S. Takahashi, Determination of methamphetamine and amphetamine in urine by head space gas chromatography/mass spectrometry. Anal Sci., 7 (1991) 19-22.
6. C. Arthur and J. Pawliszyn, Solid phase microextraction with fused silica-optical fibers. Anal. Chem., 62 (1990) 2145-2148.
7. C. Arthur, D. Potter, K. Buchholz, S. Motlagh and J. Pawliszyn, Theory and practice of solid phase microextraction for the direct analysis of water. LC-GC, 10 (1992) 656-661.
8. C. Arthur, L. Killam, S. Motlagh, M. Lim, D. Potter and J. Pawliszyn, Analysis of substituted benzene compounds in groundwater using SPME. Environ. Sci. Technol., 26 (1992) 979-983.
9. S. Hawthorne, D. Miller, J. Pawlizyn and C. Arthur, Solventless detection of caffeine in beverage using solid phase microextraction with fused silica fibers. J. Chromatogr., 603 (1992) 185-191.
10. M. Yashiki, T. Kojima, T. Miyazaki, N. Nagasawa, Y. Iwasaki and K. Hara, Detection of amphetamines in urine using head space-solid phase microextraction and chemical ionization selected ion monitoring. Forensic. Sci. Int., (1995) in press.
11. M. Yashizki, N. Nagasawa, T. Kojima, T. Miyazaki and Y. Iwasaki, Rapid analysis of nicotine and cotinine in urine using head space-solid phase microextraction and selected ion monitoring. Jpn. J. Forensic Toxicol., 13 (1995) 17-24
12. T. Miyazaki, T. Kojima, M. Yashiki, H. Wakamoto, Y. Iwasaki and T. Taniguchi, Site dependence of methamphetamine concentrations in blood samples collected from cadavers of people who had been methamphetamine abusers. Am. J. Forensic Med. Pathol., 14 (1993) 121-124.