Simple and sensitive analysis of nereistoxin and its metabolites in human serum using headspace solid-phase microextraction and gas chromatography-mass spectrometry

Journal of Chromatographic Science

Volumn 37, Issue 3, 1999, Pages 77-82

  Namera, Akira ^a   Watanabe, Tomohiko ^a   Yashiki, Mikio ^a   Kojima, Tohru ^a   Urabe, Toshima ^b  

^a HIROSHIMA UNIV SCHOOL OF MEDICINE   (Japan)

^b Sera Central Hospital   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

MARINE TOXIN; NEREISTOXIN;

ADULT; AGED; ARTICLE; BIOTRANSFORMATION; BLOOD; FEMALE; HUMAN; MALE; MASS FRAGMENTOGRAPHY; REPRODUCIBILITY; STANDARD; SUICIDE;

ADULT; AGED; AGED, 80 AND OVER; BIOTRANSFORMATION; FEMALE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; MALE; MARINE TOXINS; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SUICIDE;

EID: 0033088842     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/37.3.77     Document Type: Article

References (27)

1. S. Nitta. Ueber Nereistoxin, einen, gifftgen Bestandteil von Lumbriconereis heteropoda Marenz. Yakugaku Zasshi 54: 648-50 (1934).
2. H. Hirano, M. Sakai, and M. Numata. Researches on Nereistoxin (a marine annelid toxin). Annu. Rep. Takeda Res. Lab. 28: 272-94 (1969).
3. Y. Nagawa, Y. Saji, S. Chiba, and T. Yui. Neuromuscular blocking actions of nereistoxin and its derivatives and antagonism by sulfhydryl compounds. Jpn. J. Pharmacol. 21: 185-97 (1971).
4. National Research Institute of Police Science. Annual Case Reports of Drug and Toxic Poisoning in Japan 39: 55 (1997).
5. K. Nishi, Y. Ashida, N. Tan, and N. Sugita. Gas chromatographic and polarographic determination of nereistoxin and nereistoxin monooxide. Bunseki Kagaku 28: 137-42 (1979).
6. T. Mitsui and Y. Fujimura. Spectrophotometric determination of agricultural chemical cartap by ion association reagent. Bunseki Kagaku 32: 416-19 (1983).
7. T. Mitsui and Y. Fujimura. Extraction of agricutural chemical cartap in human blood. Eisei Kagaku 32: 305-307 (1986).
8. K. Kiyota, M. Honma, M. Shigeki, Y. Miyake, T. Sakamoto, and T. Aruga. Carrap intoxicationpharmacokinetics analysis. Jpn. J. Clin. Toxicol. 7: 263-70 (1994).
9. C.L. Arthur and J. Pawliszyn. Solid phase microextraction with thermal desorption using fused silica optical fibers. Anal. Chem. 62: 2145-48 (1990).
10. M. Yashiki, N. Nagasawa, T. Kojima, T. Miyazaki, and Y. Iwasaki. Rapid analysis of nicotine and cotinine in urine using headspace-solid phase microextraction and selected ion monitoring. Jpn. J. Forensic Toxicol. 13: 17-24 (1995).
11. M. Yashiki, T. Kojima, T. Miyazaki, N. Nagasawa, Y. Iwasaki, and K. Kara. Detection of amphetamines in urine using head space-solid phase microextraction and chemical ionization selected ion monitoring. Forensic Sci. Int. 76: 169-77 (1995).
12. N. Nagasawa, M. Yashiki, Y. Iwasaki, K. Hara, and T. Kojima. Rapid analysis of amphetamines in blood using head space-solid phase microextraction and selected ion monitoring. Forensic Sci. Int. 78: 95-102 (1996).
13. A. Namera, M. Yashiki, N. Nagasawa, Y. Iwasaki, and T. Kojima. Rapid analysis of malathion in blood using head space-solid phase microextraction and selected ion monitoring. Forensic Sci. Int. 88: 125-31 (1997).
14. T. Watanabe, A. Namera, M. Yashiki, Y. Iwasaki, K. Hara, and T. Kojima. Simple analysis of local anaesthetics in human blood using headspace-solid phase microextraction and gas chromatography-mass spectrometer/electron impact ionization-selected ion monitoring. J. Chromatogr. B 709: 225-32 (1998).
15. A. Namera, T. Watanabe, M. Yashiki, Y. Iwasaki, and T. Kojima. Simple analysis of tetracyclic antidepressants in blood head-space-solid phase microextraction and CC-MS. J. Anal. Toxicol. 22: 396-400 (1998).
16. X.-P. Lee, T. Kumazawa, K. Sato, and O. Suzuki. Detection of organophosphate pesticides in human body fluids by headspace solid-phase microextraction (SPME) and capillary gas chro-matography with nitrogen-phosphorus detection. Chromatographia 42: 135-40 (1996).
17. H. Seno, T. Kumazawa, A. Ishii, M. Nishikawa, K. Watanabe, H. Hattori, and O. Suzuki. Determination of some carbamate pesticides in human body fluids by headspace solid phase microextraction and gas chromatography. Jpn. J. Forensic Toxicol. 14: 199-203 (1996).
18. M.T. Sng, F.K. Lee, and H.A. Lakso. Solid-phase microextraction of organophosphorus pesticides from water. J. Chromatogr. A 759: 225-30 (1997).
19. Y. Luo, L. Pan, and J. Pawliszyn. Determination of five benzodiazepines in aqueous solution and biological fluids using solid-phase microextraction with Carbowax/DVB fiber coating. J. Micro. Sep. 10: 193-201 (1998).
20. V. Ferreira, M. Sharman, J.F. Cacho, and J. Dennis. New and efficient microextraction/solid-phase extraction method for the gas chromatography/mass spectrometry. Anal. Sci. 7: 19-22 (1991).
21. H.L. Lord and J. Pawliszyn. Method optimization for the analysis of amphetamines in urine by solid-phase microextraction. Anal. Chem. 69: 3899-3906 (1997).
22. L. DeBruin, R. Josephy, and J. Pawliszyn. Solid-phase microextraction of monocyclic aromatic amines from biological fluids. Anal. Chem. 70: 1986-92 (1998).
23. Z. Zhang and J. Pawliszyn. Quantitative extraction using an internally coiled solid-phase microextraction device. Anal. Chem. 67: 34-43 (1993).
24. Z. Zhang and J. Pawliszyn. Headspace solid-phase microextraction. Anal. Chem. 65: 1842-52 (1993).
25. X.-P. Lee, T. Kumazawa, and K. Sato. A simple analysis of 5 thinner components in human body fluids by headspace solid-phase microextraction (SPME). Int. J. Legal Med. 107: 310-13 (1995).
26. Y. Iwasaki, M. Yashiki, N. Nagasawa, T. Miyazaki, and T. Kojima. Analysis of inflammable substances in blood using head space-solid phase microextraction and chemical ionization selected ion monitoring. Jpn. J. Forensic Toxicol. 13: 189-94 (1995).
27. E. Degel. Comparison of new solid-phase extraction methods for chromatographic identification of drugs in clinical toxicological analysis. Clin. Biochem. 29: 529-40 (1996).