Analysis of Estrogens and Anabolic Steroids by SPME with On-Fiber Derivatization and GC/MS

Journal of Microcolumn Separations

Volumn 10, Issue 7, 1998, Pages 551-556

  Okeyo, Pius D ^a,b   Snow, Nicholas H ^a  

^a SETON HALL UNIVERSITY   (United States)

^b DUPONT COMPANY   (United States)

Author keywords

Anabolic steroids; BSTFA; Derivatization; Estrogens; Gas chromatography mass spectrometry (GC MS); Solid phase microextraction (SPME)

Indexed keywords

EID: 0000932555     PISSN: 10407685     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1520-667X(1998)10:7<551::AID-MCS1>3.0.CO;2-F     Document Type: Article

References (19)

1. S-H. Hsu, R.H. Eckerlein, and J.D. Henion, J. Chromatogr. 573, 183 (1992).
2. C.L. Arthur and J. Pawliszyn, Anal. Chem. 62, 2145 (1990).
3. D. Louch, S. Matlagh, and J. Pawliszyn, Anal. Chem. 64, 1187 (1992).
4. A. Boyd-Boland and J. Pawliszyn, Anal. Chem. 68, 1521 (1996).
5. J.R. Berg, in Proceedings of the Eighteenth International Symposium on Capillary Chromatography (A. Huethig, Heidelberg, 1996), p. 592.
6. 1996 Catalog (Supelco, Inc., Bellfonte, PA, 1996).
7. T. Gorecki, R. Mindrup, and J. Pawliszyn, Proceedings of the Eighteenth International Symposium on Capillary Chromatography (A. Huethig, Heidelberg, 1996), p. 163-172.
8. D.W. Potter and J. Pawliszyn, J. Chromatogr. 625, 247 (1992).
9. B.D. Page and G. Lacroix, J. Chromatogr. 648, 199 (1993).
10. X.P. Lee, T. Kumazawa, K. Sato, and O. Suzuki, Chromatographia 42, 135 (1996).
11. M. Yashiki, T. Kojima, T. Miyazaki, N. Nagasawa, Y. Iwzsaki, and K. Hara, Forensic Sci. Int. 76, 169 (1995).
12. T. Kumazawa, X.P. Lee, M.C. Tsai, H. Seno, A. Ishii, and K. Sato, Japan J. Forensic Toxicol. 13, 207 (1995).
13. 1996-1997 NCAA Manual (National Collegiate Athletic Association, Overland Park, KS, 1996), pp. 495-500.
14. D.R. Knapp, Handbook of Analytical Derivatization Reactions (Wiley, New York, 1979) pp. 449-514.
15. P. Okeyo, S.M. Rentz, and N.H. Snow, J. High Resolut. Chromatogr. 20, 171 (1997).
16. L. Pan and J. Pawliszyn, Anal. Chem. 69, 196 (1997).
17. S.K. Yap, G.A.R. Johnston, and R. Kazlauskas, J. Chromatogr. 573, 183 (1992).
18. D.L. Pavia, G.M. Lampman, and G.S. Kriz, Introduction to Organic Laboratory Techniques (Saunders College Publishing, Philadelphia, 1988), pp. 541-550.
19. P. Okeyo, "Solid Phase Microextraction: Optimization and Interface with GC/MS for Trace Analysis of Steroids in Biological Fluids," Ph.D. Dissertation, Seton Hall University, 1997.