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0344551625
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note
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(±)-1,3-Butadiene diepoxide 2c was purchased from commercial sources.
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119
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0344119985
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note
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18
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120
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0344982635
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note
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27 yielded eater 18 having complete inversion of configuration. Hydrolysis of 18 followed by alkylation of alcohol 19 afforded 9b. For experimental details and analytical data, see the Experimental Section.
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122
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0344551621
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note
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18
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123
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0344982632
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note
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10a was isolated as a mixture of diastereoisomers.
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0344119982
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note
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The reviewers had very helpful comments concerning the reaction mechanism and the involved intermediates.
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125
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0344551597
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note
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D was isolated and identified when the RCM reaction was stopped before complete consumption of the starting material. Analytical data are reported in the Experimental Section.
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