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Diastereoselective carbomagnesation: (a) Hoveyda, A. H.; Xu, Z. J. Am. Chem. Soc. 1991, 113, 5079-5080. (b) Houri, A. F.; Didiuk, M. T.; Xu, Z.; Horan, N. R.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6614-6624. Enantioselective carbomagnesation: (c) Morken, J. P.; Didiuk, M. T.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6697-6698. (d) Visser, M. S.; Heron, N. M.; Didiuk, M. T.; Sagal, J. F.; Hoveyda, A. H. J. Am. Chem. Soc. 1996, 118, 4291-4298.
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10
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0000910153
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Diastereoselective carbomagnesation: (a) Hoveyda, A. H.; Xu, Z. J. Am. Chem. Soc. 1991, 113, 5079-5080. (b) Houri, A. F.; Didiuk, M. T.; Xu, Z.; Horan, N. R.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6614-6624. Enantioselective carbomagnesation: (c) Morken, J. P.; Didiuk, M. T.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6697-6698. (d) Visser, M. S.; Heron, N. M.; Didiuk, M. T.; Sagal, J. F.; Hoveyda, A. H. J. Am. Chem. Soc. 1996, 118, 4291-4298.
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Houri, A.F.1
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Horan, N.R.4
Hoveyda, A.H.5
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11
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-
85176720932
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-
Diastereoselective carbomagnesation: (a) Hoveyda, A. H.; Xu, Z. J. Am. Chem. Soc. 1991, 113, 5079-5080. (b) Houri, A. F.; Didiuk, M. T.; Xu, Z.; Horan, N. R.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6614-6624. Enantioselective carbomagnesation: (c) Morken, J. P.; Didiuk, M. T.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6697-6698. (d) Visser, M. S.; Heron, N. M.; Didiuk, M. T.; Sagal, J. F.; Hoveyda, A. H. J. Am. Chem. Soc. 1996, 118, 4291-4298.
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Morken, J.P.1
Didiuk, M.T.2
Hoveyda, A.H.3
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12
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17544377767
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Diastereoselective carbomagnesation: (a) Hoveyda, A. H.; Xu, Z. J. Am. Chem. Soc. 1991, 113, 5079-5080. (b) Houri, A. F.; Didiuk, M. T.; Xu, Z.; Horan, N. R.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6614-6624. Enantioselective carbomagnesation: (c) Morken, J. P.; Didiuk, M. T.; Hoveyda, A. H. J. Am. Chem. Soc. 1993, 115, 6697-6698. (d) Visser, M. S.; Heron, N. M.; Didiuk, M. T.; Sagal, J. F.; Hoveyda, A. H. J. Am. Chem. Soc. 1996, 118, 4291-4298.
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Hoveyda, A.H.5
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16
-
-
10544225452
-
-
note
-
At this point, the diastereomer derived from minor dihydroxylation enantiomer is separated from 3b.
-
-
-
-
17
-
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0000604066
-
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For the use of this chiral auxiliary in stereoselective reactions with O-silylketene acetals, see: Kita, Y.; Itoh, F.; Tamura, O.; Ke, Y. Y.; Tamura, Y. Tetrahedron Lett. 1987, 28, 1431-1434.
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18
-
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10544250742
-
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note
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This experiment was carried out by Mr. Daniel La of these laboratories.
-
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20
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0001326246
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Pozsgay, V. J. Am. Chem. Soc. 1995, 117, 6673-6681. Although the secondary amine of the unmasked carbohydrate (product of hydrogenation) could be protected, attempts to acylate the two secondary carbinols and the hemiacetal hydroxyl group, under a variety of conditions, led to the formation of complex mixtures of products.
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10544239636
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Reference 14
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Reference 14.
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0028013298
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For other macrocyclic ring syntheses through catalytic ring closing metathesis, see: (a) Martin, S. F.; Liao, Y.; Wong, Y.; Rein, T. Tetrahedron Lett. 1994, 35, 691-694. (b) Borer, B. C.; Deerenberg, S.; Bieraugel, H.; Pandit, U. K. Tetrahedron Lett. 1994, 35, 3191-3194. (c) Martin, S. F.; Liao, Y.; Chen, H.-J.; Patzel, M.; Ramser, M. N. Tetrahedron Lett. 1994, 35, 6005-6008. (d) Miller, S. J.; Grubbs, R. H. J. Am. Chem. Soc. 1995, 117, 5855-5856. (e) Clark, T. D.; Ghadiri, M. R. J. Am. Chem. Soc. 1995, 117, 12364-12365. (f) Furstner, A.; Langemann, K. J. Org. Chem. 1996, 61, 3942-3943. (g) McKervey, M. A.; Pitarch, M. J. Chem. Soc., Chem. Commun. 1996, 1689-1690.
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Martin, S.F.1
Liao, Y.2
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Rein, T.4
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33
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0028225084
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-
For other macrocyclic ring syntheses through catalytic ring closing metathesis, see: (a) Martin, S. F.; Liao, Y.; Wong, Y.; Rein, T. Tetrahedron Lett. 1994, 35, 691-694. (b) Borer, B. C.; Deerenberg, S.; Bieraugel, H.; Pandit, U. K. Tetrahedron Lett. 1994, 35, 3191-3194. (c) Martin, S. F.; Liao, Y.; Chen, H.-J.; Patzel, M.; Ramser, M. N. Tetrahedron Lett. 1994, 35, 6005-6008. (d) Miller, S. J.; Grubbs, R. H. J. Am. Chem. Soc. 1995, 117, 5855-5856. (e) Clark, T. D.; Ghadiri, M. R. J. Am. Chem. Soc. 1995, 117, 12364-12365. (f) Furstner, A.; Langemann, K. J. Org. Chem. 1996, 61, 3942-3943. (g) McKervey, M. A.; Pitarch, M. J. Chem. Soc., Chem. Commun. 1996, 1689-1690.
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Borer, B.C.1
Deerenberg, S.2
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Pandit, U.K.4
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34
-
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0028023345
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-
For other macrocyclic ring syntheses through catalytic ring closing metathesis, see: (a) Martin, S. F.; Liao, Y.; Wong, Y.; Rein, T. Tetrahedron Lett. 1994, 35, 691-694. (b) Borer, B. C.; Deerenberg, S.; Bieraugel, H.; Pandit, U. K. Tetrahedron Lett. 1994, 35, 3191-3194. (c) Martin, S. F.; Liao, Y.; Chen, H.-J.; Patzel, M.; Ramser, M. N. Tetrahedron Lett. 1994, 35, 6005-6008. (d) Miller, S. J.; Grubbs, R. H. J. Am. Chem. Soc. 1995, 117, 5855-5856. (e) Clark, T. D.; Ghadiri, M. R. J. Am. Chem. Soc. 1995, 117, 12364-12365. (f) Furstner, A.; Langemann, K. J. Org. Chem. 1996, 61, 3942-3943. (g) McKervey, M. A.; Pitarch, M. J. Chem. Soc., Chem. Commun. 1996, 1689-1690.
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Martin, S.F.1
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Ramser, M.N.5
-
35
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0029033474
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-
For other macrocyclic ring syntheses through catalytic ring closing metathesis, see: (a) Martin, S. F.; Liao, Y.; Wong, Y.; Rein, T. Tetrahedron Lett. 1994, 35, 691-694. (b) Borer, B. C.; Deerenberg, S.; Bieraugel, H.; Pandit, U. K. Tetrahedron Lett. 1994, 35, 3191-3194. (c) Martin, S. F.; Liao, Y.; Chen, H.-J.; Patzel, M.; Ramser, M. N. Tetrahedron Lett. 1994, 35, 6005-6008. (d) Miller, S. J.; Grubbs, R. H. J. Am. Chem. Soc. 1995, 117, 5855-5856. (e) Clark, T. D.; Ghadiri, M. R. J. Am. Chem. Soc. 1995, 117, 12364-12365. (f) Furstner, A.; Langemann, K. J. Org. Chem. 1996, 61, 3942-3943. (g) McKervey, M. A.; Pitarch, M. J. Chem. Soc., Chem. Commun. 1996, 1689-1690.
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Miller, S.J.1
Grubbs, R.H.2
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36
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0001073480
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For other macrocyclic ring syntheses through catalytic ring closing metathesis, see: (a) Martin, S. F.; Liao, Y.; Wong, Y.; Rein, T. Tetrahedron Lett. 1994, 35, 691-694. (b) Borer, B. C.; Deerenberg, S.; Bieraugel, H.; Pandit, U. K. Tetrahedron Lett. 1994, 35, 3191-3194. (c) Martin, S. F.; Liao, Y.; Chen, H.-J.; Patzel, M.; Ramser, M. N. Tetrahedron Lett. 1994, 35, 6005-6008. (d) Miller, S. J.; Grubbs, R. H. J. Am. Chem. Soc. 1995, 117, 5855-5856. (e) Clark, T. D.; Ghadiri, M. R. J. Am. Chem. Soc. 1995, 117, 12364-12365. (f) Furstner, A.; Langemann, K. J. Org. Chem. 1996, 61, 3942-3943. (g) McKervey, M. A.; Pitarch, M. J. Chem. Soc., Chem. Commun. 1996, 1689-1690.
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Clark, T.D.1
Ghadiri, M.R.2
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37
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0038206375
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For other macrocyclic ring syntheses through catalytic ring closing metathesis, see: (a) Martin, S. F.; Liao, Y.; Wong, Y.; Rein, T. Tetrahedron Lett. 1994, 35, 691-694. (b) Borer, B. C.; Deerenberg, S.; Bieraugel, H.; Pandit, U. K. Tetrahedron Lett. 1994, 35, 3191-3194. (c) Martin, S. F.; Liao, Y.; Chen, H.-J.; Patzel, M.; Ramser, M. N. Tetrahedron Lett. 1994, 35, 6005-6008. (d) Miller, S. J.; Grubbs, R. H. J. Am. Chem. Soc. 1995, 117, 5855-5856. (e) Clark, T. D.; Ghadiri, M. R. J. Am. Chem. Soc. 1995, 117, 12364-12365. (f) Furstner, A.; Langemann, K. J. Org. Chem. 1996, 61, 3942-3943. (g) McKervey, M. A.; Pitarch, M. J. Chem. Soc., Chem. Commun. 1996, 1689-1690.
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Furstner, A.1
Langemann, K.2
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38
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0000112278
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-
For other macrocyclic ring syntheses through catalytic ring closing metathesis, see: (a) Martin, S. F.; Liao, Y.; Wong, Y.; Rein, T. Tetrahedron Lett. 1994, 35, 691-694. (b) Borer, B. C.; Deerenberg, S.; Bieraugel, H.; Pandit, U. K. Tetrahedron Lett. 1994, 35, 3191-3194. (c) Martin, S. F.; Liao, Y.; Chen, H.-J.; Patzel, M.; Ramser, M. N. Tetrahedron Lett. 1994, 35, 6005-6008. (d) Miller, S. J.; Grubbs, R. H. J. Am. Chem. Soc. 1995, 117, 5855-5856. (e) Clark, T. D.; Ghadiri, M. R. J. Am. Chem. Soc. 1995, 117, 12364-12365. (f) Furstner, A.; Langemann, K. J. Org. Chem. 1996, 61, 3942-3943. (g) McKervey, M. A.; Pitarch, M. J. Chem. Soc., Chem. Commun. 1996, 1689-1690.
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McKervey, M.A.1
Pitarch, M.2
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39
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0001719584
-
-
Efforts to prepare more soluble derivatives of the macrolactam alcohol (e.g., the derived TMS ether) which would also be suitable for glycosylation by other methods (e.g., involving triacetate 7) were not successful. For an example, see: Mukaiyama, T.; Katsurada, M.; Takashima, T. Chem. Lett. 1991, 985-988.
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Mukaiyama, T.1
Katsurada, M.2
Takashima, T.3
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