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85030208509
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note
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13C NMR spectra, as well as appropriate parent ion identificaton by high resolution mass spectrometry and/or elemental composition analysis.
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24
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85030207062
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note
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3) δ 26.6, 38.6, 55.7, 64.5, 66.1, 71.8, 71.9, 74.5, 94.6, 110.3, 111.7, 113.2, 141.9, 146.1, 151.9, 156.0, 177.8, 198.4
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29
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0001725065
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Danheiser, R.L.1
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Brisbois, R.G.3
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33845375462
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32
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0025324609
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33
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85030210618
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note
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(15) To date, we have found 50 mol% of the copper(I) complex to provide the optimal results in the conversion of 6 to 16. Greater, or lesser, amounts of the complex led to lower yields of 16.
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34
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0023693209
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(16) Feigelson, G.B.; Egbertson, M.; Danishefsky, S.J.; Schulte, G. J. Org. Chem. 1988, 53, 3390-3391.
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Schulte, G.4
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35
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85030203877
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note
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(17) Diol 17 is tentatively assigned the stereochemistry shown based on the presumption that osmylation occured from the side opposite the cyclic carbonate (6→17).
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36
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85030204781
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note
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13C NMR.
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