Separation and purification of α-glucosidase inhibitors from Polygonatum odoratum by stepwise high-speed counter-current chromatography combined with Sephadex LH-20 chromatography target-guided by ultrafiltration-HPLC screening

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 985, Issue , 2015, Pages 149-154

  Zhou, Xiaoling ^a,b   Liang, Junsheng ^a,b   Zhang, Yi ^a,b   Zhao, Huading ^c   Guo, Ying ^d   Shi, Shuyun ^c  

^a Hunan Academy of Forest Sciences   (China)

^b Key Laboratory of Hunan Tree Clones Breeding   (China)

^c CENTRAL SOUTH UNIVERSITY   (China)

^d CENTRAL SOUTH UNIVERSITY   (China)

Author keywords

HSCCC; Phenethyl cinnamide; Polygonatum odoratum; Sephadex LH 20; Ultrafiltration; Glucosidase inhibitor

Indexed keywords

COLLOIDS; DEXTRAN; ION EXCHANGE; LIQUID CHROMATOGRAPHY; ORGANIC SOLVENTS; PURIFICATION; SEPARATION; ULTRAFILTRATION;

GLUCOSIDASE INHIBITORS; HSCCC; PHENETHYL CINNAMIDE; POLYGONATUM ODORATUM; SEPHADEX LH-20;

CHROMATOGRAPHY;

5,7 DIHYDROXYL 3 (2',4' DIHYDROXYBENZYL) CHROMAN 4 ONE; 5,7 DIHYDROXYL 6 METHYL 3 (4' HYDROXYBENZYL) CHROMAN 4 ONE; 5,7 DIHYDROXYL 6 METHYL 8 METHOXY (4' HYDROXYBENZYL) CHROMAN 4 ONE; 5,7 DIHYDROXYL 6,8 DIMETHYL 3 (4' HYDROXYBENZYL) CHROMAN 4 ONE; ACETIC ACID ETHYL ESTER; ALCOHOL; ALPHA GLUCOSIDASE INHIBITOR; FLAVANONE DERIVATIVE; METHANOL; N CIS FERULOYLOCTOPAMINE; N TRANS FERULOYLOCTOPAMINE; N TRANS FERULOYLTYRAMINE; N TRANS P COUMAROYLOCTOPAMINE; N TRANS P COUMAROYLTYRAMINE; PETROLEUM ETHER; PLANT EXTRACT; SEPHADEX; UNCLASSIFIED DRUG; WATER; DEXTRAN; GLYCOSIDASE INHIBITOR;

ARTICLE; COUNTER CURRENT CHROMATOGRAPHY; DRUG PURIFICATION; DRUG SCREENING; DRUG STRUCTURE; ENZYME INHIBITION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH SPEED COUNTER CURRENT CHROMATOGRAPHY; IC50; LILIACEAE; MASS SPECTROMETRY; NONHUMAN; PARTITION COEFFICIENT; POLYGONATUM; POLYGONATUM ODORATUM; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; ULTRAFILTRATION; ULTRAVIOLET SPECTROPHOTOMETRY; CHEMISTRY; ENZYMOLOGY; ISOLATION AND PURIFICATION; PROCEDURES;

LILIACEAE; POLYGONATUM; POLYGONATUM ODORATUM;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; COUNTERCURRENT DISTRIBUTION; DEXTRANS; GLYCOSIDE HYDROLASE INHIBITORS; PLANT EXTRACTS; POLYGONATUM; ULTRAFILTRATION;

EID: 84922706800     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2015.01.030     Document Type: Article

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