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Crystal data for dyad 3,4PF6. C188H170F48N26O28P8Zn2, M = 4531.99, triclinic, a = 13.471(19), b = 15.22(2), c = 28.60(4) A°, α = 100.70(3), β = 90.22(3), γ = 110.96(5)°, U = 5365(13) A°3, T = 100.01, space group P 1¯ (no. 2), Z = 1, μCuKa = 1.818, 13528 reflections measured, 9154 unique (Rint = 0.0352) which were used in all calculations. The final wR(F2) was 0.2435 (all data). CCDC-987726 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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