Modern analytical supercritical fluid chromatography using columns packed with sub-2μm particles: A tutorial

Analytica Chimica Acta

Volumn 824, Issue , 2014, Pages 18-35

  Nováková, Lucie ^a   Grand Guillaume Perrenoud, Alexandre ^b   Francois, Isabelle ^c   West, Caroline ^d   Lesellier, Eric ^d   Guillarme, Davy ^b  

^a Charles University in Prague Faculty of Pharmacy   (Czech Republic)

^b UNIVERSITY OF GENEVA   (Switzerland)

^c Waters NV/SA   (Belgium)

^d UNIVERSITÉ D'ORLÉANS   (France)

Author keywords

Column selection; Mobile phase selection; Sub 2 m particles; Supercritical fluid chromatography; Tutorial; Ultra high performance supercritical fluid chromatography

Indexed keywords

ANALYTICAL GEOCHEMISTRY; CHEMICAL ANALYSIS; CHEMISTRY;

ANALYTICAL CONDITIONS; COLUMN SELECTIONS; LIPOPHILIC COMPOUNDS; MOBILE-PHASE SELECTION; ORGANIC MODIFIER; STATIONARY PHASE; SUPER CRITICAL FLUID CHROMATOGRAPHY; TUTORIAL;

GAS CHROMATOGRAPHY;

CARBON DIOXIDE; FATTY ACID; LIPID; SOLVENT; TRIACYLGLYCEROL;

CHEMICAL ANALYSIS; CHROMATOGRAPH; COLUMN CHROMATOGRAPHY; DISSOLUTION; DRUG ANALYSIS; FLOW RATE; HYDROPHILICITY; LIGHT SCATTERING; LIPID ANALYSIS; MASS SPECTROMETRY; PARTICLE SIZE; PRESSURE; PRIORITY JOURNAL; REVIEW; SUPERCRITICAL FLUID; SUPERCRITICAL FLUID CHROMATOGRAPHY; TEMPERATURE; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; ULTRAVIOLET RADIATION; CHEMISTRY; PROCEDURES;

CHROMATOGRAPHY, SUPERCRITICAL FLUID; PARTICLE SIZE; SOLVENTS;

EID: 84899079126     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2014.03.034     Document Type: Review

References (123)

1. Tarafder A., Kaczmarski K., Ranger M., Poe D.P., Guiochon G. Journal of Chromatography A 2012, 1238:132-145.
2. Poe D.P., Veit D., Ranger M., Kaczmarski K., Tarafder A., Guiochon G. Journal of Chromatography A 2012, 1250:105-114.
3. Tarafder A., Kaczmarski K., Poe D.P., Guiochon G. Journal of Chromatography A 2012, 1258:136-151.
4. Huetz A., Klesper E. Journal of Chromatography 1992, 607:79-89.
5. Lauer H.H., McManigill D., Board R.D. Analytical Chemistry 1983, 55:1370-1375.
6. Rosset R., Caude M., Jardy A. Chromatographie en Phase Liquide et Supercritique 1991, Ed. Masson, Paris.
7. Span R., Wagner W. Journal of Physical and Chemical Reference Data 1996, 25:1509-1596.
8. Berger T.A. Packed Column SFC 1995, Royal Society of Chemistry, Cambridge.
9. Deye J.F., Berger T.A., Anderson A.G. Analytical Chemistry 1990, 62:615-622.
10. Berger T.A., Deye J.F. Analytical Chemistry 1990, 62:1181-1185.
11. Olesik S.V., Woodruff J.L. Analytical Chemistry 1991, 63:670-676.
12. Sandra P., Pereira A., Dunkle M., Brunelli C., David F. LC-GC Europe 2010, 23:396-405.
13. Klesper E., Corwin A.H., Turner D.A. Journal of Organic Chemistry 1962, 27:700-701.
14. Springston S.R., Novotny M. Chromatographia 1981, 14:679-684.
15. Peaden P.A., Lee M.L. Journal of Chromatography 1983, 259:1-16.
16. Kuei J.C., Tarbet B.J., Jackson W.P., Bradshaw J.S., Markides K.E., Lee M.L. Chromatographia 1985, 20:25-30.
17. Gere D.R., Board R., McManigill D. Analytical Chemistry 1982, 54:736-740.
18. Wheeler J.R., McNally M.E. Journal of Chromatography 1987, 410:343-353.
19. Schoenmakers P.J., Uunk L.G.M. Chromatographia 1987, 24:51-57.
20. Schwartz H.E. LC-GC 1987, 5:14-22.
21. Crowther J.B., Henion J.D. Analytical Chemistry 1985, 57:2711-2716.
22. Anacleto J.F., Ramaley L., Boyd R.K., Pleasance S., Quilliam M.A., Sim P.G., Benoit F.M. Rapid Communications in Mass Spectrometry 1991, 5:149-155.
23. Strode J.T.B., Taylor L.T., Howard A.L., Ip D. Journal of Pharmaceutical and Biomedical Analysis 1999, 20:137-143.
24. Giddings J.C. A critical evaluation of the theory of gas chromatography. Gas Chromatography. 1964 1965, 3-24. Elsevier, Amsterdam. A. Goldup (Ed.).
25. Fairchild J.N., Hill J.F., Iraneta P.C. LC-GC North America 2013, 31:326-333.
26. Abrahamsson V., Sandahl M. Journal of Chromatography A 2013, 1306:80-88.
27. Gurdale K., Lesellier E., Tchapla A. Journal of Chromatography A 2000, 866:241-251.
28. Fekete S., Kohler I., Rudaz S., Veuthey J.L. Journal of Pharmaceutical and Biomedical Analysis 2014, 87:105-119.
29. Grand-Guillaume Perrenoud A., Hamman C., Goel M., Veuthey J.L., Guillarme D., Fekete S. Journal of Chromatography A 2013, 1314:288-297.
30. Grand-Guillaume Perrenoud A., Veuthey J.L., Guillarme D. Journal of Chromatography A 2012, 1266:158-167.
31. Lesellier E. Journal of Chromatography A 2009, 1216:1881-1890.
32. Lesellier E. Journal of Separation Science 2008, 31:1238-1251.
33. West C., Lesellier E. Journal of Chromatography A 2006, 1110:181-190.
34. West C., Lesellier E. Journal of Chromatography A 2006, 1115:233-245.
35. West C., Lesellier E., Tchapla A. Journal of Chromatography A 2004, 1048:99-109.
36. West C., Lesellier E. Journal of Chromatography A 2005, 1087:64-76.
37. West C., Lesellier E. Journal of Chromatography A 2006, 1110:200-213.
38. West C., Khater S., Lesellier E. Journal of Chromatography A 2012, 1250:182-195.
39. West C., Lesellier E. Journal of Chromatography A 2006, 1110:191-199.
40. West C., Lesellier E. Journal of Chromatography A 2007, 1169:205-219.
41. Khater S., West C., Lesellier E. Journal of Chromatography A 2013, 1319:148-159.
42. Yip H.S.H., Ashraf-Khorassani M., Taylor L.T. Chromatographia 2007, 65:655-665.
43. Cazenve-Gassiot A., Boughtflower R., Caldwell J., Coxhead R., Hitzel L., Lane S., Oakley P., Holyoak C., Pullen F., Langley G.J. Journal of Chromatography A 2008, 1189:254-265.
44. Alexander A.J., Hooker T.F., Tomasella F.P. Journal of Pharmaceutical and Biomedical Analysis 2012, 70:77-86.
45. Lundgreen J., Salomonsson J., Gyllenhaal O., Johansson E. Journal of Chromatography A 2007, 1154:360-367.
46. Lesellier E. Journal of Chromatography A 2012, 1228:89-98.
47. Lesellier E., Latos A., Lopes de Oliveira A. Journal of Chromatography A 2014, 1327:141-148.
48. Lesellier E. Journal of Chromatography A 2012, 1266:34-42.
49. West C., Lesellier E. Journal of Chromatography A 2008, 1203:105-114.
50. Berger T.A. Journal of Chromatography A 1997, 785:3-33.
51. Berger T.A. Analytical Chemistry 1990, 62:1181-1187.
52. Cantrell G.O., Stringham R.W., Blackwell J.A., Weckwerth J.D., Carr P.W. Analytical Chemistry 1996, 68:3645-3650.
53. Blackwell J.A., Stringham R.W., Weckwerth J.D. Analytical Chemistry 1997, 69:409-415.
54. Brunelli C., Zhao Y., Brown M.-H., Sandra P. Journal of Chromatography A 2008, 1185:263-272.
55. Zou W., Dorsey J.G., Chester T. Analytical Chemistry 2000, 72:3620-3626.
56. Brunelli C., Zhao Y., Brown M.-H., Sandra P. Journal of Separation Science 2008, 31:1299-1306.
57. Saito M. Journal of Bioscience and Bioengineering 2013, 115:590-599.
58. Smith R.M. Journal of Chromatography A 1999, 856:83-115.
59. Pinkston J.D., Stanon D.T., Wen D. Journal of Separation Science 2004, 27:115-123.
60. Geiser F., Schultz M., Beltz L., Shaimi M., Lee J., Champion W. Journal of Chromatography A 1999, 865:227-233.
61. Zheng J., Taylor L.T., Pinkston J.D., Mangels M.L. Journal of Chromatography A 2005, 1082:220-229.
62. Cazenave-Gassiot A., Boughtflower R., Caldwell J., Hitzel L., Holyoak C., Lane S., Oakley P., Pullen F., Richardson S., Langley G.J. Journal of Chromatography A 2009, 1216:6441-6450.
63. Cazenve-Gassiot A., Boughtflower R., Caldwell J., Coxhead R., Hitzel L., Lane S., Oakley P., Holyoak C., Pullen F., Langley G.J. Journal of Chromatography A 2008, 1189:254-265.
64. Hamman C., Schmidt D.E., Wong M., Hayes M. Journal of Chromatography A 2011, 1218:7886-7894.
65. Grand-Guillaume Perrenoud A., Boccard J., Veuthey J.-L., Guillarme D. Journal of Chromatography A 2012, 1262:205-213.
66. Coan C.R., King A.D. Journal of the American Chemical Society 1971, 93:1857-1858.
67. Wang S., Elshani S., Wai C.M. Analytical Chemistry 1995, 67:919-923.
68. Taylor L.T. Journal of Chromatography A 2012, 1250:196-204.
69. Ashraf-Khorassani M., Taylor L.T. Journal of Separation Science 2010, 33:1682-1691.
70. Lou X., Janssen H.-G., Cramers C.A. Journal of Chromatography A 1997, 785:57-68.
71. Berger T.A. Journal of High Resolution Chromatography 1991, 14:312-316.
72. Tarafder A., Kaczmarski K., Poe D.P., Guiochon G. Journal of Chromatography A 2012, 1258:136-145.
73. Harris C.M. Analytical Chemistry 2002, 74:87A-91A.
74. Lesellier E., Valarche A., West C., Dreux M. Journal of Chromatography A 2012, 1250:220-226.
75. Takashi K., Kinugasa S., Senda M., Kimizuka K., Fukushima K., Matsumoto T., Shibata Y., Christensen J. Journal of Chromatography A 2008, 1193:151-155.
76. Deschamps F.S., Gaudin K., Lesellier E., Tchapla A., Ferrier D., Baillet A., Chaminade P. Chromatographia 2001, 54:607-611.
77. Lesellier E., Gaudin K., Chaminade P., Tchapla A., Baillet A. Journal of Chromatography A 2003, 1016:111-121.
78. Takahashi K., Kinugasa S., Yoshihara R., Nakanishi A., Mosing R.K., Takahashi R. Journal of Chromatography A 2009, 1216:9008-9013.
79. Brunelli C., Gorecki T., Zhao Y., Sandra P. Analytical Chemistry 2007, 79:2472-2482.
80. Li F., Hsieh Y. Journal of Separation Science 2008, 31:1231-1237.
81. Pinkston J.D. European Journal of Mass Spectrometry 2005, 11:189-197.
82. Chen R. Chromatography Today 2009, 4:11-13.
83. Bolaños B., Greig M., Ventura M., Farrell W., Ch.Aurigemma M., Li H., Quenzer T.L., Tivel K., Bylund J.M.R., Tran P., Pham C., Phillipson D. International Journal of Mass Spectrometry 2004, 238:85-97.
84. Berger T.A., Berger B.K. Journal of Chromatography A 2011, 1218:2320-2326.
85. Wang Z., Zhang H., Liu O., Donovan B. Journal of Chromatography A 2011, 1218:2311-2319.
86. Ruiz-Samblás C., González-Casado A., Cuadros-Rodriguez L., Rodriguez García F.P. Talanta 2010, 82:255-260.
87. Purcaro G., Tranchida P.Q., Dugo P., Camera E.L., Bisignano G., Conte L., Mondello L. Journal of Separation Science 2010, 33:2334-2340.
88. Lísa M., Netusilová K., Franek L., Dvoráková H., Vrkoslav V., Holcapek M. Journal of Chromatography A 2011, 1218:7499-7510.
89. Camera E., Ludovici M., Galante M., Sinagra J., Picardo M. Journal of Lipid Research 2010, 51:3377-3388.
90. Pang L.Q., Liang Q.L., Wang Y.M., Ping L., Luo G.A. Journal of Chromatography B 2008, 869:118-125.
91. Lísa M., Holcapek M. Journal of Chromatography A 2008, 1198-1199:115-130.
92. Ikeda K., Oike Y., Shimizu T., Taguchi R. Journal of Chromatography B 2009, 877:2639-2647.
93. Bernal J.L., Martin M.T., Toribio L. Journal of Chromatography A 2013, 1313:24-36.
94. Senorans F.J., Ibanez E. Analytica Chimica Acta 2002, 465:131-144.
95. G. Isaac, M.D. Jones, B. Bajrami, W. Obeid, J. Langridge, P. Hatcher, Fast and Simple Free Fatty Acids Analysis Using UPC2/MS, Waters Application Note 720004763en.
96. Taguchi K., Fukusaki E., Bamba T. Journal of Chromatography A 2013, 1299:103-109.
97. Lesellier E., Tchapla A. Analytical Chemistry 1999, 71:5372-5378.
98. Lesellier E., Bleton J., Tchapla A. Analytical Chemistry 2000, 72:2573-2580.
99. Lee J.W., Uchikata T., Matsubara A., Nakamura T., Fukusaki E., Bamba T. Journal of Bioscience and Bioengineering 2012, 113:262-268.
100. M.N. Dunkle, F. David, P. Sandra, Analysis of triglycerides in vegetable oils using the Agilent 1260 Infinity Analytical SFC System with evaporative light scattering detection, Agilent Application Note 5991-0987EN.
101. Zhou Q., Gao B., Zhang X., Xu Y., Shi H., Yu L. Food Chemistry 2014, 143:199-204.
102. Sandra P., Medvedovici A., Zhao Y., David F. Journal of Chromatography A 2002, 974:231-241.
103. Sandra P., Medvedovici A., Kot A., David F. Supercritical Fluid Chromatography with Packed Columns 1997, 161-194. Marcel Decker, New York. K. Anton, C. Berger (Eds.).
104. Dermaux A., Medvedovici A., Ksir M., Van Hove E., Talbi M., Sandra P. Journal of Microcolumn Separations 1999, 11:451-459.
105. François I., Sandra P. Journal of Chromatography A 2009, 1216:4005-4012.
106. François I., dos Santos-Pereira A., Sandra P. Journal of Separation Science 2010, 33:1504-1512.
107. Hirata Y., Hashiguchi T., Kawata E. Journal of Separation Science 2003, 26:531-535.
108. Hirata Y., Sogabe I. Analytical and Bioanalytical Chemistry 2004, 378:1999-2003.
109. M.D. Jones, G. Isaac, G. Astarita, A. Aubin, J. Shockor, V. Shulaev, Lipid Class Separation Using UPC2/MS, Waters Application Note 720004579en.
110. Lesellier E., Krstulovic A.M., Tchapla A. Chromatographia 1993, 36:275-282.
111. Lesellier E., Gurdale K., Tchapla A. Journal of Chromatography A 1999, 844:307-320.
112. R. Chen, J. Yang, J. McCauley, A Single-Injection UPC2 Method for Fast and Simultaneous Separation of Nine Fat-Soluble Vitamins, Waters Application Note 720004551en.
113. McCalley D.V. Journal of Chromatography A 1999, 844:23-38.
114. Cai S.S., Hanold K.A., Syage J.A. Analytical Chemistry 2007, 79:2491-2498.
115. Karu N., Dicinoski G.W., Haddad P.R. Trends in Analytical Chemistry 2012, 40:119-132.
116. Periat A., Grand-Guillaume Perrenoud A., Guillarme D. Journal of Separation Science 2013, 36:3141-3151.
117. Patel M.A., Riley F., Ashraf-Khorassani M., Taylor L.T. Journal of Chromatography A 2012, 1233:85-90.
118. Ashraf-Khorassani M., Taylor L.T., Seest E. Journal of Chromatography A 2012, 1229:237-248.
119. West C., Metogo M.M., Lesellier E. Poster: investigations on the measurement of pH of supercritical mobile phases. HPLC International Symposium 2009.
120. Dijkstra Z.J., Doornbos A.R., Weyten H., Ernsting J.M., Elsevier C.J., Keurentjes J.T.F. Journal of Supercritical Fluids 2007, 41:109-114.
121. Zheng J., Glass T., Taylor L.T., Pinkston J.D. Journal of Chromatography A 2005, 1090:155-164.
122. Francois I., Dos Santos Pereira A., Lynen F., Sandra P. Journal of Separation Science 2008, 31:3473-3478.
123. Hudalla C.J., Tarafder A., Fountain K.J. Poster "development of a strategy for scaling SFC methods: applications for preparative chromatography". presented at SFC 2013 conference in Boston 2013.